SampleIdent,909C 9R-3 11-15DROP,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 4-sep-1993 10:49,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 106, 86, 98, 102, 102, 102, 106, 106 104, 117, 119, 98, 262, 112, 106, 104 98, 92, 96, 106, 90, 102, 102, 112 365, 117, 100, 104, 102, 106, 98, 112 94, 108, 102, 119, 104, 94, 102, 98 117, 119, 100, 108, 121, 132, 128, 98 98, 90, 102, 121, 132, 106, 117, 106 106, 123, 108, 132, 102, 114, 114, 114 108, 110, 108, 128, 108, 112, 102, 112 102, 106, 128, 123, 123, 114, 112, 117 125, 90, 130, 130, 123, 117, 121, 130 130, 132, 112, 106, 130, 132, 108, 114 96, 130, 121, 123, 128, 142, 135, 132 110, 104, 112, 123, 114, 123, 121, 123 114, 119, 106, 114, 128, 119, 102, 119 104, 144, 119, 119, 117, 121, 125, 108 117, 151, 112, 139, 125, 110, 149, 123 121, 137, 144, 121, 117, 121, 135, 121 137, 125, 119, 128, 125, 144, 144, 110 114, 130, 117, 119, 130, 137, 144, 128 121, 142, 125, 149, 130, 159, 123, 139 142, 135, 151, 130, 144, 142, 154, 137 142, 135, 164, 132, 137, 112, 137, 139 135, 139, 125, 132, 123, 139, 130, 130 125, 112, 121, 117, 119, 106, 102, 104 96, 114, 100, 119, 112, 106, 90, 100 102, 98, 125, 119, 88, 102, 110, 98 85, 108, 106, 92, 114, 106, 81, 94 94, 100, 112, 110, 100, 106, 88, 128 86, 110, 83, 106, 102, 102, 90, 92 102, 100, 94, 100, 102, 79, 88, 106 110, 100, 85, 98, 77, 96, 76, 85 106, 79, 100, 104, 92, 100, 102, 106 119, 88, 92, 104, 112, 88, 94, 100 106, 94, 88, 94, 94, 114, 88, 98 85, 90, 98, 79, 79, 100, 98, 92 104, 92, 100, 88, 98, 85, 106, 94 69, 90, 83, 86, 79, 88, 102, 90 90, 104, 98, 94, 88, 98, 71, 85 104, 74, 94, 90, 76, 102, 100, 92 74, 83, 83, 81, 94, 98, 94, 110 102, 76, 79, 88, 85, 79, 94, 77 98, 85, 114, 98, 88, 98, 104, 119 100, 100, 108, 98, 94, 86, 125, 117 119, 102, 123, 130, 135, 123, 123, 151 154, 137, 159, 139, 130, 137, 110, 114 119, 104, 112, 94, 94, 81, 102, 92 94, 83, 76, 85, 83, 90, 86, 88 83, 90, 86, 83, 85, 86, 72, 83 86, 94, 98, 83, 102, 83, 88, 83 79, 72, 92, 81, 86, 74, 77, 94 81, 77, 85, 86, 67, 100, 72, 77 85, 66, 72, 79, 90, 79, 74, 90 85, 86, 96, 83, 96, 90, 77, 76 94, 76, 83, 92, 85, 79, 76, 90 85, 102, 72, 77, 85, 86, 76, 77 83, 77, 71, 74, 94, 76, 85, 71 86, 69, 83, 85, 76, 74, 56, 64 90, 74, 88, 72, 72, 74, 72, 92 67, 85, 81, 83, 86, 79, 88, 62 71, 67, 58, 83, 71, 94, 94, 79 85, 69, 90, 83, 85, 76, 71, 72 74, 71, 72, 72, 77, 71, 81, 67 98, 88, 77, 79, 72, 62, 79, 77 67, 69, 85, 92, 76, 69, 81, 83 86, 88, 77, 77, 77, 77, 72, 81 90, 86, 85, 83, 74, 56, 76, 66 59, 96, 76, 74, 85, 90, 85, 76 81, 85, 72, 83, 71, 86, 81, 96 90, 72, 74, 72, 88, 83, 62, 90 86, 77, 86, 83, 79, 83, 71, 79 85, 85, 76, 77, 76, 86, 74, 76 83, 83, 67, 88, 76, 77, 61, 83 83, 86, 67, 96, 96, 66, 88, 88 86, 92, 64, 79, 86, 74, 71, 83 79, 83, 66, 90, 100, 77, 98, 92 67, 85, 90, 72, 76, 83, 79, 83 85, 83, 81, 72, 83, 96, 74, 85 96, 104, 88, 96, 85, 83, 76, 90 85, 100, 90, 100, 79, 71, 94, 88 85, 74, 88, 92, 74, 85, 104, 76 88, 88, 71, 79, 86, 77, 81, 83 86, 66, 83, 76, 72, 67, 86, 94 72, 79, 64, 79, 62, 81, 77, 56 88, 62, 77, 98, 83, 88, 64, 81 79, 74, 83, 69, 72, 79, 72, 83 85, 66, 55, 61, 74, 76, 96, 53 81, 67, 79, 96, 72, 79, 79, 61 76, 72, 71, 66, 83, 71, 96, 85 77, 92, 104, 94, 88, 98, 69, 85 96, 100, 102, 112, 117, 112, 110, 130 130, 156, 135, 139, 149, 164, 156, 151 161, 161, 174, 135, 121, 123, 125, 132 130, 123, 110, 92, 102, 114, 119, 83 114, 98, 96, 88, 88, 104, 110, 100 90, 114, 100, 88, 96, 106, 81, 90 100, 112, 100, 77, 98, 96, 79, 100 98, 94, 108, 114, 114, 104, 139, 159 159, 210, 174, 193, 213, 240, 207, 159 151, 128, 123, 112, 114, 92, 100, 108 90, 86, 98, 90, 88, 102, 83, 88 85, 110, 85, 100, 83, 72, 90, 88 83, 90, 88, 94, 90, 69, 69, 72 77, 79, 74, 67, 86, 79, 106, 79 85, 76, 69, 85, 72, 94, 74, 94 77, 62, 85, 72, 85, 62, 81, 88 79, 86, 102, 92, 72, 86, 67, 72 77, 69, 81, 76, 72, 79, 66, 66 86, 90, 79, 85, 67, 79, 72, 72 67, 66, 59, 83, 76, 67, 79, 76 88, 76, 85, 85, 77, 83, 74, 98 79, 74, 88, 108, 92, 85, 86, 85 79, 85, 79, 86, 92, 71, 77, 72 74, 81, 77, 94, 76, 85, 85, 69 66, 79, 88, 98, 92, 94, 94, 77 86, 79, 92, 81, 76, 100, 83, 102 102, 98, 104, 88, 96, 90, 90, 92 85, 88, 83, 79, 88, 86, 88, 92 88, 96, 96, 85, 104, 104, 102, 94 102, 100, 88, 110, 104, 100, 102, 94 96, 98, 119, 130, 137, 119, 144, 135 149, 137, 159, 161, 164, 202, 193, 240 231, 222, 222, 228, 250, 234, 256, 276 231, 219, 234, 216, 234, 250, 199, 207 196, 188, 154, 154, 151, 144, 125, 123 112, 106, 117, 104, 112, 108, 108, 110 110, 108, 112, 128, 108, 104, 117, 135 108, 108, 100, 104, 119, 85, 104, 81 79, 88, 102, 83, 100, 98, 72, 85 86, 79, 94, 86, 90, 79, 92, 83 92, 96, 88, 88, 83, 83, 77, 94 83, 104, 94, 92, 98, 83, 85, 90 86, 110, 108, 94, 117, 94, 135, 110 128, 166, 169, 231, 231, 296, 365, 416 462, 534, 502, 600, 645, 640, 666, 620 534, 449, 600, 313, 240, 199, 172, 149 164, 119, 154, 117, 121, 100, 144, 110 106, 94, 110, 92, 86, 104, 79, 108 96, 79, 106, 77, 83, 108, 85, 83 90, 100, 104, 106, 88, 106, 69, 83 92, 117, 102, 100, 96, 96, 88, 102 79, 81, 100, 90, 90, 86, 96, 100 100, 92, 106, 94, 104, 98, 88, 85 88, 83, 83, 92, 92, 98, 85, 94 90, 71, 92, 76, 86, 64, 72, 71 72, 86, 77, 77, 86, 83, 88, 76 94, 76, 92, 62, 90, 92, 72, 71 72, 86, 79, 83, 76, 85, 76, 69 58, 88, 66, 77, 72, 85, 62, 71 76, 71, 77, 81, 74, 72, 79, 85 66, 67, 86, 56, 79, 71, 56, 61 79, 86, 72, 62, 79, 77, 90, 67 83, 71, 77, 72, 69, 83, 67, 81 79, 72, 62, 76, 77, 79, 81, 86 79, 81, 81, 76, 77, 117, 100, 86 104, 85, 100, 76, 67, 79, 100, 77 85, 79, 86, 86, 90, 98, 86, 86 90, 77, 83, 96, 85, 88, 96, 86 85, 79, 77, 88, 67, 86, 83, 86 88, 72, 81, 92, 96, 90, 104, 86 98, 102, 104, 102, 94, 100, 108, 119 108, 110, 121, 121, 125, 96, 123, 132 112, 108, 100, 104, 132, 108, 128, 130 137, 137, 154, 137, 149, 149, 164, 151 144, 151, 169, 177, 188, 188, 177, 193 207, 216, 262, 253, 250, 259, 292, 328 342, 335, 388, 392, 420, 445, 471, 506 529, 610, 625, 660, 605, 676, 620, 660 650, 635, 630, 640, 630, 620, 635, 610 600, 562, 529, 552, 488, 428, 392, 372 350, 289, 253, 246, 182, 182, 185, 174 156, 119, 117, 117, 106, 98, 85, 100 86, 85, 79, 86, 83, 83, 72, 67 66, 66, 79, 83, 86, 81, 92, 106 85, 100, 98, 100, 112, 110, 94, 94 71, 85, 71, 71, 58, 76, 79, 77 55, 71, 64, 56, 66, 62, 58, 74 71, 72, 59, 59, 55, 56, 53, 44 58, 66, 62, 53, 61, 62, 55, 67 45, 53, 67, 64, 50, 62, 53, 50 59, 59, 59, 55, 61, 59, 58, 50 58, 58, 48, 56, 56, 55, 49, 66 83, 59, 76, 86, 66, 62, 62, 67 85, 85, 88, 86, 98, 85, 72, 94 100, 108, 104, 112, 108, 130, 128, 130 119, 110, 139, 114, 139, 139, 144, 135 139, 151, 146, 123, 149, 139, 144, 125 128, 130, 142, 125, 132, 114, 123, 110 94, 88, 86, 88, 98, 88, 62, 94 79, 76, 88, 81, 72, 72, 77, 77 81, 66, 76, 69, 96, 64, 62, 76 67, 67, 71, 66, 64, 76, 83, 66 66, 67, 83, 62, 67, 77, 74, 76 83, 86, 74, 66, 61, 69, 69, 62 69, 83, 79, 69, 61, 67, 56, 83 67, 92, 79, 79, 76, 96, 98, 77 112, 130, 102, 123, 119, 125, 117, 121 112, 123, 83, 85, 88, 83, 94, 76 79, 74, 66, 88, 79, 102, 88, 114 94, 83, 104, 104, 90, 90, 102, 100 86, 104, 100, 86, 90, 96, 94, 106 85, 90, 88, 74, 81, 81, 85, 88 85, 83, 85, 88, 96, 76, 79, 85 112, 104, 102, 104, 90, 96, 110, 110 102, 108, 125, 117, 110, 106, 108, 128 112, 106, 125, 114, 117, 128, 112, 132 130, 128, 159, 144, 154, 159, 182, 164 169, 180, 185, 193, 188, 199, 177, 199 182, 204, 204, 177, 172, 169, 137, 128 144, 144, 130, 108, 106, 108, 77, 94 86, 90, 76, 66, 72, 83, 67, 74 64, 67, 66, 69, 67, 69, 50, 67 76, 76, 59, 52, 38, 53, 61, 53 56, 61, 56, 58, 74, 62, 67, 66 74, 77, 100, 79, 94, 114, 83, 104 96, 102, 67, 86, 76, 79, 53, 56 56, 59, 50, 42, 46, 56, 55, 48 62, 55, 53, 48, 56, 71, 376, 71 50, 85, 58, 50, 76, 59, 62, 71 53, 67, 74, 77, 66, 79, 90, 83 83, 79, 108, 69, 88, 77, 59, 62 76, 72, 55, 71, 69, 83, 64, 77 72, 62, 88, 92, 94, 94, 92, 79 66, 79, 76, 69, 59, 59, 61, 59 76, 52, 67, 71, 59, 66, 64, 67 67, 56, 83, 86, 71, 74, 71, 74 64, 69, 66, 76, 76, 67, 55, 76 66, 76, 55, 53, 77, 67, 76, 77 55, 76, 71, 83, 76, 85, 96, 88 98, 79, 90, 112, 108, 106, 114, 110 130, 110, 132, 132, 128, 146, 164, 172 164, 146, 188, 199, 204, 193, 216, 237 225, 210, 196, 225, 246, 231, 222, 222 269, 269, 259, 243, 276, 276, 259, 246 207, 219, 196, 159, 161, 159, 139, 114 114, 110, 104, 85, 123, 83, 72, 77 79, 76, 56, 72, 71, 50, 71, 72 56, 59, 76, 62, 59, 53, 50, 64 66, 59, 53, 64, 59, 44, 61, 55 38, 56, 52, 46, 49, 40, 59, 59 50, 67, 52, 58, 56, 50, 56, 37 53, 59, 48, 48, 53, 62, 41, 50 50, 48, 61, 56, 76, 71, 79, 77 72, 66, 72, 56, 71, 76, 61, 67 79, 62, 59, 67, 53, 67, 58, 67 72, 53, 61, 61, 69, 71, 66, 59 59, 61, 67, 102, 85, 92, 94, 110 98, 108, 94, 94, 86, 71, 81, 81 71, 83, 88, 59, 56, 62, 72, 66 71, 74, 67, 49, 62, 77, 98, 62 71, 76, 76, 62, 71, 86, 83, 83 59, 90, 81, 96, 88, 106, 85, 92 94, 102, 102, 119, 100, 108, 110, 88 104, 110, 117, 110, 112, 112, 117, 142 123, 142, 130, 151, 154, 154, 159, 166 149, 177, 169, 182, 177, 159, 174, 182 193, 182, 193, 188, 172, 185, 180, 149 174, 154, 169, 164, 188, 177, 177, 169 142, 130, 164, 137, 125, 121, 123, 121 90, 94, 83, 86, 88, 79, 48, 72 72, 50, 62, 76, 67, 72, 62, 62 59, 46, 52, 52, 55, 58, 46, 61 55, 49, 56, 56, 40, 56, 61, 42 53, 42, 55, 46, 69, 67, 67, 77 61, 71, 67, 58, 59, 55, 62, 58 77, 50, 62, 56, 62, 50, 55, 45 53, 49, 48, 52, 48, 46, 55, 58 56, 41, 49, 56, 62, 49, 53, 48 50, 48, 46, 46, 62, 50, 52, 46 52, 46, 46, 38, 61, 50, 49, 38 48, 49, 44, 48, 44, 40, 35, 49 41, 53, 42, 48, 35, 42, 48, 50 50, 46, 45, 42, 41, 48, 48, 40 49, 48, 56, 49, 44, 49, 49, 55 37, 49, 41, 50, 50, 44, 42, 37 36, 42, 59, 35, 58, 55, 62, 55 46, 48, 56, 45, 62, 56, 48, 44 53, 59, 67, 50, 45, 59, 58, 58 52, 44, 53, 50, 59, 62, 64, 61 50, 45, 55, 45, 66, 55, 66, 67 64, 55, 59, 90, 71, 106, 110, 102 123, 125, 151, 159, 193, 154, 154, 137 156, 142, 106, 128, 128, 114, 98, 90 85, 85, 86, 67, 83, 92, 88, 100 112, 114, 121, 90, 112, 121, 119, 96 121, 112, 110, 114, 106, 102, 114, 130 114, 102, 112, 108, 114, 112, 110, 130 114, 112, 96, 108, 110, 128, 96, 100 98, 88, 85, 83, 88, 71, 88, 79 83, 67, 90, 76, 74, 76, 88, 79 76, 77, 58, 83, 77, 61, 72, 71 85, 83, 83, 96, 85, 94, 88, 86 98, 85, 90, 121, 104, 96, 121, 114 112, 119, 102, 100, 135, 128, 137, 130 149, 132, 128, 151, 174, 172, 164, 177 174, 177, 190, 207, 202, 228, 213, 219 253, 216, 231, 262, 246, 286, 282, 243 292, 272, 292, 282, 266, 289, 292, 296 299, 289, 299, 306, 279, 289, 299, 317 292, 292, 292, 296, 296, 303, 306, 310 266, 296, 276, 292, 256, 219, 228, 219 174, 180, 188, 177, 164, 149, 119, 149 121, 135, 104, 98, 108, 112, 106, 102 104, 81, 88, 83, 77, 104, 85, 81 88, 71, 90, 66, 92, 77, 71, 67 77, 86, 86, 69, 71, 79, 72, 71 71, 66, 85, 79, 46, 62, 67, 83 59, 66, 76, 67, 53, 61, 56, 85 66, 62, 59, 79, 72, 67, 62, 67 71, 64, 67, 59, 67, 67, 62, 58 71, 72, 62, 79, 83, 67, 98, 85 90, 117, 90, 102, 88, 79, 88, 85 90, 88, 77, 85, 79, 98, 77, 77 71, 72, 77, 77, 85, 77, 59, 98 86, 88, 79, 62, 76, 88, 56, 72 79, 98, 77, 67, 64, 77, 83, 56 83, 67, 71, 69, 72, 67, 88, 90 83, 83, 66, 72, 76, 74, 58, 76 72, 71, 92, 85, 77, 85, 90, 88 100, 100, 106, 108, 142, 114, 117, 102 117, 112, 108, 79, 88, 76, 59, 77 90, 62, 66, 53, 69, 59, 66, 85 66, 66, 53, 45, 40, 61, 50, 50 55, 50, 58, 52, 45, 49, 49, 52 55, 46, 42, 71, 62, 53, 66, 53 41, 44, 52, 52, 41, 44, 53, 53 36, 50, 56, 44, 55, 42, 58, 41 44, 48, 58, 58, 46, 49, 49, 44 41, 48, 45, 52, 50, 46, 49, 38 44, 58, 53, 59, 53, 53, 50, 52 48, 50, 50, 36, 41, 56, 50, 53 44, 62, 55, 52, 55, 53, 40, 44 40, 38, 56, 50, 48, 38, 50, 45 45, 44, 44, 46, 38, 35, 59, 50 48, 49, 53, 41, 44, 42, 24, 44 38, 53, 45, 46, 53, 59, 56, 61 50, 40, 53, 44, 50, 42, 56, 59 46, 50, 53, 32, 53, 66, 62, 50 53, 58, 52, 48, 49, 49, 56, 38 56, 66, 53, 46, 56, 55, 64, 56 59, 66, 61, 56, 59, 48, 55, 53 61, 59, 62, 62, 62, 72, 83, 67 110, 76, 100, 112, 135, 128, 149, 125 174, 130, 137, 123, 121, 104, 98, 110 106, 86, 94, 94, 96, 79, 88, 79 85, 85, 74, 77, 86, 86, 74, 94 79, 88, 71, 88, 88, 71, 85, 81 86, 74, 85, 88, 92, 88, 81, 81 77, 92, 86, 90, 102, 86, 90, 100 86, 96, 83, 88, 94, 94, 121, 100 102, 110, 125, 112, 137, 112, 123, 123 130, 137, 154, 149, 119, 142, 137, 125 130, 149, 137, 132, 166, 135, 144, 188 164, 196, 180, 169, 193, 174, 174, 196 180, 164, 182, 164, 172, 190, 139, 159 172, 154, 142, 146, 128, 144, 125, 128 114, 121, 108, 112, 106, 81, 96, 96 71, 100, 96, 96, 90, 77, 67, 72 77, 77, 83, 77, 64, 71, 72, 83 64, 67, 58, 56, 71, 71, 67, 50 67, 53, 49, 62, 56, 41, 53, 48 50, 50, 56, 53, 62, 61, 59, 53 67, 44, 53, 53, 49, 46, 50, 53 45, 48, 53, 55, 41, 55, 48, 48 32, 66, 48, 59, 59, 46, 53, 42 38, 66, 48, 55, 55, 64, 55, 46 36, 52, 59, 52, 56, 59, 44, 59 66, 49, 58, 53, 67, 48, 59, 71 62, 66, 59, 71, 81, 71, 74, 76 64, 83, 76, 79, 85, 71, 74, 77 67, 72, 66, 76, 79, 77, 59, 71 67, 76, 67, 77, 79, 81, 67, 61 53, 72, 64, 66, 66, 71, 71, 66 66, 77, 81, 83, 71, 92, 86, 96 117, 94, 102, 108, 102, 104, 98, 125 112, 117, 125, 130, 125, 132, 132, 125 112, 123, 119, 98, 123, 102, 96, 114 110, 119, 121, 121, 104, 125, 102, 121 112, 92, 112, 108, 110, 128, 100, 102 106, 100, 114, 74, 110, 85, 104, 98 88, 77, 79, 83, 79, 72, 81, 76 74, 61, 67, 62, 67, 66, 72, 59 72, 64, 56, 48, 53, 53, 59, 53 72, 69, 56, 62, 55, 53, 44, 66 76, 64, 59, 77, 67, 71, 77, 62 58, 92, 69, 72, 74, 67, 55, 72 62, 67, 74, 72, 71, 62, 67, 71 62, 62, 56, 71, 71, 81, 71, 90 69, 72, 83, 90, 79, 85, 76, 90 86, 94, 66, 104, 86, 88, 94, 72 85, 92, 76, 112, 86, 104, 90, 100 114, 96, 135, 106, 117, 123, 98, 125 117, 125, 121, 106, 117, 110, 114, 102 104, 137, 114, 117, 121, 156, 144, 159 159, 193, 193, 159, 137, 172, 142, 144 137, 180, 164, 137, 154, 135, 106, 128 100, 106, 106, 88, 104, 123, 90, 86 76, 85, 83, 85, 85, 85, 100, 77 83, 83, 102, 100, 86, 100, 83, 106 92, 102, 85, 100, 108, 108, 100, 98 119, 110, 117, 108, 106, 104, 119, 110 125, 106, 130, 100, 137, 128, 130, 144 117, 102, 114, 130, 112, 112, 112, 121 123, 128, 114, 114, 123, 137, 123, 96 130, 114, 106, 88, 106, 94, 83, 88 85, 61, 90, 98, 67, 67, 83, 86 66,/