SampleIdent,911A 40X-5 23 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-aug-1993 21:05,/ DataAngleRange, 5.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 159, 149, 166, 137, 166, 169, 159, 156 151, 156, 169, 196, 161, 172, 156, 169 177, 182, 169, 199, 177, 190, 159, 193 193, 185, 207, 199, 185, 185, 222, 207 207, 185, 213, 190, 250, 202, 196, 222 219, 190, 228, 216, 213, 231, 222, 210 240, 231, 222, 231, 256, 250, 246, 240 272, 243, 253, 266, 269, 234, 237, 276 237, 219, 286, 272, 276, 266, 279, 282 276, 299, 303, 266, 299, 269, 279, 303 292, 292, 299, 292, 266, 313, 292, 313 306, 310, 324, 313, 320, 282, 335, 292 317, 313, 306, 282, 335, 276, 292, 296 339, 306, 299, 299, 303, 299, 328, 317 306, 289, 313, 296, 303, 303, 282, 259 279, 262, 296, 262, 289, 282, 250, 253 266, 276, 256, 246, 240, 246, 272, 222 225, 231, 228, 243, 222, 237, 231, 234 225, 177, 225, 228, 219, 231, 185, 202 216, 177, 190, 204, 222, 219, 180, 169 193, 180, 161, 190, 196, 174, 164, 199 174, 207, 177, 177, 174, 169, 202, 174 185, 193, 188, 169, 161, 196, 202, 177 180, 190, 196, 161, 166, 177, 172, 166 164, 164, 172, 130, 159, 121, 130, 161 135, 121, 151, 137, 117, 117, 149, 128 121, 137, 112, 130, 102, 119, 90, 125 119, 125, 121, 108, 117, 104, 130, 110 98, 156, 108, 117, 100, 102, 114, 106 100, 125, 121, 139, 100, 106, 108, 90 110, 106, 114, 128, 110, 110, 100, 117 72, 104, 98, 96, 104, 112, 100, 96 92, 104, 106, 108, 106, 86, 106, 106 90, 106, 94, 102, 117, 98, 85, 106 104, 104, 100, 100, 94, 114, 104, 94 96, 104, 100, 88, 86, 108, 94, 94 114, 100, 102, 83, 98, 92, 102, 121 98, 102, 79, 100, 121, 100, 106, 106 77, 94, 98, 106, 96, 102, 102, 106 100, 114, 102, 90, 106, 86, 86, 96 90, 96, 94, 106, 92, 85, 86, 88 76, 108, 92, 92, 96, 104, 114, 86 81, 76, 106, 90, 100, 94, 104, 121 92, 88, 77, 98, 86, 88, 100, 112 90, 72, 102, 83, 119, 92, 92, 125 110, 88, 104, 119, 114, 117, 121, 112 90, 132, 146, 137, 112, 108, 123, 112 123, 104, 114, 94, 94, 83, 81, 112 86, 79, 102, 88, 86, 110, 86, 90 104, 121, 112, 100, 96, 85, 92, 108 102, 119, 102, 125, 102, 94, 100, 104 85, 92, 94, 88, 76, 100, 102, 92 90, 94, 106, 92, 119, 102, 94, 88 88, 112, 112, 94, 112, 83, 79, 96 85, 90, 81, 92, 104, 98, 83, 102 106, 119, 104, 83, 114, 94, 106, 100 96, 117, 98, 98, 112, 108, 92, 110 85, 110, 94, 104, 102, 104, 100, 112 106, 102, 123, 106, 96, 121, 110, 92 98, 88, 92, 96, 104, 114, 102, 102 90, 88, 90, 86, 108, 106, 106, 102 114, 121, 119, 117, 92, 98, 102, 125 98, 104, 104, 110, 104, 106, 90, 106 114, 100, 119, 96, 106, 102, 88, 94 92, 85, 102, 130, 92, 96, 98, 92 104, 117, 79, 94, 96, 77, 100, 114 94, 106, 86, 114, 110, 102, 117, 112 102, 108, 119, 110, 106, 106, 98, 104 76, 119, 102, 98, 104, 112, 104, 98 90, 86, 104, 86, 90, 90, 92, 85 108, 114, 106, 92, 100, 96, 108, 100 86, 102, 121, 96, 106, 90, 94, 114 110, 106, 117, 100, 117, 110, 121, 114 121, 81, 92, 119, 94, 104, 108, 112 96, 119, 102, 110, 100, 114, 96, 102 92, 98, 106, 106, 100, 88, 96, 86 92, 121, 114, 104, 121, 112, 119, 125 110, 110, 117, 104, 114, 137, 117, 98 121, 128, 130, 123, 125, 144, 149, 125 135, 119, 156, 149, 125, 137, 132, 121 125, 132, 132, 119, 100, 125, 104, 108 123, 117, 104, 98, 135, 121, 117, 123 102, 117, 114, 106, 119, 119, 117, 112 112, 121, 110, 119, 119, 117, 117, 119 123, 117, 108, 130, 104, 98, 125, 114 96, 114, 132, 119, 125, 130, 139, 137 130, 130, 130, 121, 121, 125, 119, 114 112, 121, 117, 98, 102, 139, 130, 117 121, 130, 144, 130, 132, 123, 123, 117 130, 146, 146, 121, 154, 146, 149, 142 151, 161, 172, 188, 169, 190, 199, 196 213, 228, 216, 228, 213, 231, 231, 246 279, 243, 262, 262, 237, 228, 213, 210 231, 246, 234, 225, 234, 237, 216, 253 243, 225, 250, 210, 237, 253, 256, 289 253, 250, 256, 246, 299, 276, 292, 262 282, 296, 335, 306, 357, 310, 328, 342 365, 357, 342, 339, 342, 380, 350, 369 369, 416, 369, 408, 380, 369, 392, 353 404, 350, 369, 400, 328, 376, 342, 331 388, 365, 324, 365, 380, 384, 400, 404 361, 372, 400, 458, 420, 462, 445, 441 484, 529, 480, 557, 566, 538, 571, 534 635, 650, 645, 660, 610, 586, 630, 660 620, 650, 566, 666, 595, 581, 548, 576 571, 552, 529, 484, 511, 497, 458, 441 441, 458, 445, 404, 404, 353, 376, 412 346, 339, 361, 357, 353, 339, 324, 320 328, 331, 328, 357, 346, 286, 286, 303 276, 292, 272, 269, 250, 279, 279, 282 296, 262, 292, 250, 269, 262, 262, 250 256, 272, 259, 222, 250, 234, 276, 225 243, 256, 231, 234, 256, 240, 216, 219 228, 234, 225, 228, 225, 219, 213, 237 213, 193, 219, 188, 228, 199, 228, 219 202, 190, 225, 193, 190, 213, 202, 193 213, 231, 196, 177, 216, 188, 174, 182 199, 193, 182, 196, 182, 190, 193, 188 199, 177, 210, 188, 204, 161, 199, 199 185, 196, 188, 193, 185, 207, 177, 204 151, 346, 180, 190, 174, 199, 149, 172 169, 174, 166, 180, 193, 174, 182, 196 180, 199, 350, 180, 493, 166, 193, 188 193, 190, 174, 185, 190, 177, 180, 177 182, 182, 174, 182, 190, 182, 190, 204 190, 213, 228, 202, 243, 202, 234, 228 231, 202, 216, 202, 188, 231, 213, 202 199, 202, 188, 199, 210, 213, 190, 234 199, 204, 199, 190, 188, 188, 202, 169 202, 216, 196, 190, 199, 202, 190, 193 182, 166, 193, 188, 210, 185, 199, 219 222, 177, 228, 182, 207, 204, 182, 207 174, 204, 210, 199, 210, 193, 216, 204 243, 225, 262, 253, 296, 292, 237, 331 384, 433, 420, 488, 484, 605, 640, 708 681, 818, 562, 538, 428, 388, 412, 342 361, 350, 331, 335, 299, 299, 296, 246 286, 299, 269, 237, 243, 243, 253, 228 256, 246, 256, 246, 259, 240, 282, 250 250, 266, 279, 259, 276, 269, 286, 266 289, 269, 253, 276, 269, 266, 243, 253 299, 272, 276, 266, 256, 262, 289, 286 269, 286, 282, 317, 306, 292, 306, 310 310, 306, 339, 310, 303, 306, 331, 303 279, 272, 292, 296, 253, 250, 282, 246 250, 259, 240, 276, 279, 250, 276, 222 231, 243, 253, 237, 246, 259, 250, 231 225, 237, 250, 222, 256, 231, 237, 253 219, 234, 225, 207, 262, 225, 231, 240 210, 204, 225, 240, 237, 243, 231, 213 207, 222, 207, 193, 228, 210, 240, 199 193, 216, 202, 213, 207, 177, 228, 188 180, 196, 177, 196, 190, 180, 182, 196 172, 196, 177, 213, 199, 204, 207, 182 216, 207, 193, 222, 204, 216, 207, 219 202, 207, 216, 213, 199, 202, 188, 207 210, 213, 213, 185, 225, 204, 185, 202 169, 180, 169, 182, 174, 190, 199, 199 202, 213, 156, 182, 169, 164, 207, 199 199, 207, 180, 154, 193, 180, 185, 174 196, 177, 164, 182, 193, 190, 174, 185 185, 199, 182, 180, 169, 185, 182, 193 180, 216, 185, 169, 193, 174, 188, 174 182, 161, 182, 159, 174, 182, 193, 193 182, 210, 185, 188, 172, 177, 156, 180 177, 177, 182, 172, 196, 177, 202, 204 174, 174, 180, 193, 199, 177, 193, 166 202, 185, 199, 182, 144, 161, 185, 174 149, 185, 154, 182, 164, 182, 177, 190 156, 172, 151, 156, 169, 169, 146, 154 159, 177, 159, 151, 146, 149, 156, 177 188, 324, 172, 156, 146, 154, 177, 149 159, 164, 149, 169, 174, 151, 149, 156 161, 154, 156, 185, 164, 146, 156, 166 144, 164, 130, 156, 154, 182, 159, 172 174, 125, 144, 154, 159, 146, 149, 149 161, 177, 144, 149, 132, 146, 149, 137 159, 154, 164, 156, 132, 146, 156, 146 139, 149, 166, 159, 169, 159, 137, 139 151, 144, 151, 146, 154, 146, 164, 137 166, 137, 142, 156, 164, 154, 149, 164 149, 137, 156, 149, 172, 149, 159, 159 159, 154, 151, 174, 149, 166, 169, 182 161, 142, 139, 159, 154, 193, 185, 169 188, 185, 161, 182, 180, 193, 188, 207 182, 204, 210, 222, 180, 207, 185, 216 199, 182, 202, 219, 213, 202, 199, 199 234, 207, 202, 213, 207, 204, 207, 222 199, 202, 216, 202, 213, 202, 219, 210 213, 219, 185, 199, 202, 202, 210, 219 202, 199, 216, 202, 228, 190, 228, 231 237, 237, 246, 234, 246, 282, 259, 292 279, 213, 299, 246, 246, 289, 286, 243 266, 262, 243, 296, 259, 240, 256, 259 231, 231, 228, 240, 250, 237, 219, 199 193, 204, 204, 188, 207, 219, 225, 199 216, 210, 188, 193, 196, 199, 222, 216 222, 222, 202, 202, 193, 193, 182, 196 172, 188, 177, 182, 166, 182, 164, 185 180, 174, 164, 159, 169, 182, 159, 182 310, 182, 174, 185, 156, 164, 174, 159 177, 166, 154, 166, 166, 132, 149, 154 169, 166, 161, 169, 144, 182, 144, 172 177, 144, 151, 172, 169, 172, 169, 185 159, 174, 159, 185, 174, 144, 149, 169 177, 177, 154, 151, 154, 156, 144, 149 130, 142, 137, 121, 146, 137, 154, 151 130, 156, 142, 159, 159, 169, 177, 149 185, 185, 174, 149, 166, 166, 144, 149 121, 137, 144, 139, 130, 130, 144, 123 135, 154, 119, 137, 151, 139, 128, 137 139, 121, 128, 125, 130, 130, 121, 121 146, 144, 149, 135, 135, 137, 121, 130 130, 114, 119, 119, 132, 139, 114, 132 130, 135, 146, 128, 144, 144, 177, 161 169, 135, 188, 139, 164, 154, 137, 139 149, 132, 121, 128, 144, 119, 144, 128 135, 159, 139, 135, 137, 123, 137, 121 135, 154, 135, 135, 135, 144, 139, 156 149, 146, 137, 149, 149, 146, 146, 139 130, 151, 121, 149, 151, 130, 144, 117 151, 121, 130, 125, 154, 130, 132, 123 146, 114, 121, 135, 110, 144, 110, 125 135, 117, 137, 117, 130, 112, 110, 146 117, 144, 128, 128, 128, 130, 159, 144 144, 137, 144, 125, 139, 137, 132, 125 135, 121, 142, 149, 110, 128, 125, 144 146, 146, 142, 149, 137, 135, 149, 142 144, 137, 142, 164, 154, 128, 139, 146 144, 144, 159, 132, 149, 169, 125, 137 174, 146, 144, 144, 135, 144, 128, 159 128, 125, 144, 151, 130, 128, 128, 151 142, 130, 174, 156, 137, 166, 139, 161 161, 164, 169, 166, 169, 177, 190, 174 196, 149, 169, 144, 164, 177, 161, 154 161, 169, 159, 161, 135, 144, 146, 169 161, 154, 159, 142, 137, 149, 159, 154 123, 159, 144, 156, 149, 137, 132, 137 159, 166, 169, 139, 128, 144, 156, 139 137, 130, 142, 130, 132, 154, 139, 144 137, 159, 161, 135, 125, 166, 159, 172 154, 156, 142, 154, 135, 154, 154, 159 154, 154, 156, 159, 146, 174, 156, 135 182, 193, 159, 185, 174, 182, 156, 164 166, 159, 151, 161, 151, 159, 182, 154 151, 164, 177, 166, 144, 154, 164, 174 166, 196, 199, 177, 196, 199, 182, 228 225, 210, 185, 188, 193, 174, 193, 164 156, 180, 174, 156, 161, 172, 164, 142 166, 166, 130, 164, 166, 146, 146, 137 151, 159, 137, 166, 166, 177, 166, 174 149, 193, 166, 177, 188, 182, 196, 174 196, 185, 202, 188, 210, 164, 210, 196 169, 199, 166, 164, 149, 193, 166, 172 156, 177, 156, 156, 180, 166, 130, 149 161, 130, 156, 159, 151, 149, 169, 149 146, 132, 135, 139, 139, 137, 149, 130 137, 149, 128, 149, 151, 144, 130, 128 117, 137, 142, 119, 137, 108, 130, 106 137, 142, 139, 130, 154, 139, 128, 128 132, 142, 121, 135, 110, 123, 139, 144 149, 135, 125, 121, 151, 104, 128, 128 119, 121, 142, 137, 156, 130, 137, 137 121, 125, 130, 128, 130, 117, 121, 137 110, 137, 117, 125, 146, 119, 114, 132 128, 125, 106, 135, 112, 149, 130, 117 137, 108, 130, 121, 149, 139, 130, 121 110, 108, 114, 132, 142, 114, 142, 137 137, 137, 142, 149, 125, 137, 146, 137 135, 130, 119, 130, 161, 132, 119, 142 123, 121, 119, 114, 125, 139, 125, 130 125, 119, 149, 130, 135, 137, 112, 137 106, 135, 128, 137, 117, 135, 100, 123 121, 125, 132, 114, 135, 123, 119, 110 142, 108, 110, 132, 121, 137, 114, 144 119, 125, 106, 123, 123, 117, 121, 128 117, 149, 108, 144, 104, 132, 132, 114 144, 130, 139, 125, 114, 123, 137, 125 119, 121, 128, 112, 142, 121, 121, 137 128, 125, 119, 146, 114, 114, 130, 128 132, 128, 117, 137, 128, 125, 121, 159 144, 135, 156, 172, 177, 164, 188, 182 180, 180, 172, 137, 149, 164, 121, 125 125, 128, 132, 112, 117, 137, 135, 119 130, 128, 119, 121, 125, 112, 130, 144 121, 121, 144, 144, 125, 108, 139, 125 132, 123, 139, 114, 125, 121, 125, 128 96, 128, 135, 121, 121, 146, 110, 164 110, 121, 106, 114, 125, 159, 114, 125 106, 104, 125, 117, 119, 128, 104, 121 104, 98, 144, 125, 104, 110, 121, 117 112, 130, 130, 121, 125, 117, 154, 130 125, 130, 117, 130, 114, 130, 102, 125 130, 144, 96, 132, 112, 121, 119, 123 135, 135, 125, 123, 146, 110, 130, 128 135, 123, 142, 137, 114, 123, 142, 128 121, 130, 146, 144, 130, 132, 130, 123 135, 117, 137, 119, 121, 128, 128, 130 156, 132, 132, 110, 130, 135, 135, 123 144, 128, 146, 132, 112, 132, 130, 125 144, 142, 132, 125, 130, 139, 119, 130 146, 142, 132, 156, 110, 132, 128, 130 128, 130, 137, 142, 146, 164, 161, 154 154, 125, 156, 151, 159, 132, 123, 130 154, 142, 159, 130, 132, 156, 142, 130 149, 132, 159, 177, 185, 149, 130, 139 169, 123, 161, 159, 154, 130, 151, 146 144, 154, 142, 149, 169, 151, 139, 164 149, 154, 132, 154, 142, 151, 139, 149 161, 137, 144, 159, 169, 161, 135, 146 164, 154, 164, 159, 154, 130, 177, 149 174, 166, 190, 182, 174, 169, 159, 161 149, 146, 156, 159, 174, 161, 149, 159 161, 166, 164, 169, 154, 161, 159, 154 156, 169, 169, 154, 169, 151, 164, 154 169, 156, 156, 174, 166, 182, 151, 151 149, 174, 156, 169, 149, 182, 144, 151 149, 144, 159, 182, 151, 151, 154, 180 169, 193, 169, 144, 164, 142, 169, 144 149, 154, 159, 169, 166, 164, 159, 174 156, 164, 169, 180, 161, 164, 169, 169 154, 154, 161, 177, 169, 177, 174, 159 149, 159, 182, 180, 177, 180, 174, 174 180, 199, 196, 174, 159, 174, 174, 156 166, 137, 164, 164, 172, 169, 156, 156 169, 166, 161, 164, 154, 174, 151, 161 164, 180, 180, 174, 146, 159, 172, 144 156, 161, 142, 151, 174, 159, 142, 161 144, 164, 164, 151, 142, 159, 164, 146 149, 154, 154, 169, 172, 154, 130, 154 149, 188, 172, 169, 142, 146, 146, 151 159, 139, 159, 144, 151, 151, 164, 156 137, 161, 149, 151, 132, 139, 154, 151 156, 172, 139, 137, 146, 159, 144, 156 151, 161, 159, 132, 174, 149, 182, 159 159, 119, 164, 149, 146, 149, 154, 132 154, 139, 156, 154, 156, 156, 154, 128 132, 156, 174, 180, 159, 135, 172, 151 154, 169, 174, 156, 174, 169, 159, 159 161, 156, 151, 164, 139, 149, 169, 182 149, 137, 151, 151, 164, 142, 156, 154 159, 144, 159, 159, 151, 159, 159, 169 151, 177, 169, 164, 161, 164, 185, 159 199, 210, 188, 216, 188, 185, 199, 156 202, 196, 172, 156, 164, 174, 154, 137 169, 177, 159, 172, 164, 166, 161, 161 174, 149, 149, 132, 137, 169, 130, 151 172, 161, 149, 146, 172, 154, 159, 180 146, 164, 144, 164, 151, 139, 161, 185 182, 164, 151, 159, 161, 159, 196, 154 164, 139, 154, 172, 164, 196, 213, 156 154, 199, 164, 180, 196, 161, 196, 185 174, 174, 182, 185, 164, 172, 199, 177 190, 207, 202, 202, 185, 188, 199, 199 193, 207, 190, 196, 188, 185, 185, 204 172, 180, 177, 182, 196, 190, 202, 188 180, 177, 199, 188, 154, 177, 204, 185 190, 190, 161, 188, 182, 190, 185, 204 169, 185, 196, 210, 169, 169, 177, 188 169, 169, 154, 146, 169, 166, 161, 159 156, 169, 177, 190, 164, 169, 169, 154 164, 169, 156, 159, 159, 154, 159, 159 146, 146, 159, 164, 169, 154, 146, 161 149, 172, 151, 156, 137, 144, 161, 149 144, 156, 151, 159, 161, 151, 159, 159 154, 180, 182, 161, 154, 182, 146, 146 149, 154, 164, 137, 156, 154, 151, 286 154, 154, 156, 161, 164, 172, 159, 159 159, 139, 169, 164, 177, 188, 156, 174 159, 164, 180, 190, 174, 177, 196, 166 164, 180, 182, 154, 161, 151, 164, 151 174, 164, 144, 174, 174, 169, 154, 188 182, 159, 188, 185, 159, 169, 159, 166 164, 177, 174, 156, 190, 185, 164, 166 172, 190, 190, 182, 174, 177, 180, 188 182, 169, 169, 154, 182, 159, 169, 188 159, 156, 193, 172, 174, 154, 180, 180 174, 185, 182, 180, 177, 156, 199, 164 188, 172, 174, 172, 169, 164, 174, 174 174, 174, 166, 177, 144, 164, 164, 190 144, 159, 159, 139, 177, 161, 169, 174 177, 164, 154, 190, 177, 144, 164, 151 172, 174, 159, 137, 174, 142, 154, 164 151, 161, 159, 161, 125, 149, 144, 151 137, 169, 156, 161, 151, 161, 149, 177 149, 182, 154, 151, 125, 137, 154, 156 154, 142, 142, 149, 139, 169, 164, 154 156, 174, 137, 151, 142, 149, 169, 161 156, 156, 161, 159, 149, 166, 159, 185 151, 164, 154, 159, 164, 169, 132, 164 154, 169, 180, 164, 149, 174, 188, 156 169, 154, 159, 188, 154, 146, 164, 182 182, 199, 180, 169, 164, 185, 156, 164 180, 164, 164, 166, 193, 182, 188, 193 166, 196, 193, 188, 207, 159, 180, 202 185, 182, 193, 172, 185, 199, 207, 210 161, 156, 164, 142, 169, 161, 174, 177 174, 180, 164, 169, 169, 164, 169, 159 164, 142, 188, 161, 159, 137, 144, 161 172, 166, 174, 166, 146, 161, 146, 174 128, 166, 188, 139, 130, 166, 139, 151 164, 190, 159, 172, 139, 156, 149, 159 169, 190, 151, 174, 172, 149, 177, 161 128, 159, 166, 174, 169, 151, 169, 154 182, 156, 154, 146, 149, 169, 144, 149 154, 151, 130, 169, 159, 154, 159, 164 149,/