SampleIdent,911C 6H-1 35 BULK,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,29-aug-1993 23:49,/ DataAngleRange, 2.0000, 69.9600,/ ScanStepSize, 0.020,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 85, 83, 96, 86, 98, 76, 77, 72 83, 102, 79, 88, 72, 85, 67, 77 76, 67, 71, 52, 58, 50, 74, 79 64, 77, 86, 62, 77, 66, 72, 66 67, 74, 77, 61, 69, 77, 74, 67 71, 71, 76, 66, 62, 67, 79, 86 50, 61, 86, 67, 66, 72, 59, 62 48, 69, 76, 67, 72, 59, 66, 62 71, 71, 72, 88, 77, 72, 59, 74 72, 74, 79, 66, 74, 72, 62, 76 83, 59, 79, 64, 76, 56, 76, 59 66, 69, 74, 77, 71, 72, 66, 71 72, 66, 66, 62, 72, 77, 67, 86 85, 69, 66, 83, 58, 77, 94, 81 77, 67, 81, 74, 76, 69, 76, 71 88, 90, 71, 64, 71, 71, 67, 83 83, 76, 92, 76, 92, 79, 85, 66 85, 76, 76, 74, 85, 81, 72, 77 71, 72, 74, 86, 94, 66, 88, 85 77, 88, 88, 85, 102, 76, 86, 76 86, 79, 94, 81, 90, 100, 90, 96 102, 77, 100, 74, 85, 90, 77, 102 85, 90, 98, 77, 92, 100, 102, 92 98, 104, 98, 100, 86, 79, 86, 104 112, 112, 92, 106, 90, 90, 98, 102 102, 94, 96, 100, 102, 121, 110, 86 139, 92, 117, 102, 98, 102, 106, 102 90, 110, 104, 121, 102, 104, 112, 112 102, 117, 128, 92, 104, 98, 100, 128 98, 123, 117, 114, 106, 128, 104, 94 110, 96, 86, 102, 96, 130, 106, 110 112, 104, 119, 135, 119, 106, 112, 119 96, 114, 102, 106, 121, 110, 106, 108 88, 110, 96, 104, 110, 108, 119, 108 92, 102, 104, 106, 108, 94, 94, 100 96, 114, 100, 132, 104, 98, 100, 106 106, 104, 108, 114, 125, 125, 104, 135 88, 112, 119, 112, 110, 102, 96, 106 125, 121, 102, 100, 98, 132, 106, 100 102, 112, 88, 110, 121, 106, 112, 119 117, 112, 112, 108, 108, 100, 106, 137 94, 121, 108, 121, 98, 125, 121, 130 137, 128, 125, 132, 130, 156, 146, 139 130, 132, 125, 121, 112, 121, 98, 114 125, 102, 102, 102, 108, 100, 100, 92 108, 86, 90, 100, 94, 77, 98, 100 106, 86, 108, 96, 96, 104, 86, 117 90, 92, 98, 83, 92, 100, 104, 66 94, 88, 94, 88, 100, 94, 88, 98 83, 98, 96, 88, 96, 86, 85, 90 104, 104, 88, 112, 90, 85, 100, 104 106, 100, 100, 79, 108, 79, 102, 100 90, 90, 85, 106, 100, 98, 96, 83 96, 94, 77, 96, 86, 106, 90, 92 90, 67, 77, 85, 94, 86, 96, 400 71, 96, 96, 94, 90, 94, 94, 88 106, 92, 90, 92, 92, 98, 94, 90 81, 108, 76, 92, 85, 76, 98, 90 102, 90, 96, 88, 94, 100, 102, 79 96, 96, 72, 86, 72, 79, 90, 77 88, 67, 77, 88, 71, 81, 90, 86 83, 85, 98, 83, 108, 108, 94, 83 92, 83, 96, 114, 88, 106, 114, 102 102, 100, 104, 106, 119, 104, 114, 112 130, 125, 117, 128, 137, 156, 156, 151 190, 172, 159, 174, 193, 193, 185, 207 182, 180, 137, 128, 114, 112, 106, 108 90, 106, 76, 85, 92, 100, 83, 90 86, 90, 85, 86, 88, 117, 69, 79 79, 88, 76, 76, 94, 96, 86, 83 88, 76, 83, 88, 69, 98, 79, 74 71, 71, 98, 88, 90, 90, 62, 81 85, 98, 83, 92, 94, 90, 79, 96 62, 76, 76, 86, 86, 90, 79, 77 72, 66, 96, 77, 77, 90, 86, 86 79, 88, 62, 96, 76, 71, 79, 81 79, 79, 86, 77, 83, 90, 76, 61 81, 67, 76, 81, 96, 90, 72, 71 83, 79, 79, 71, 72, 83, 67, 94 77, 71, 77, 77, 83, 67, 69, 85 72, 83, 72, 77, 77, 90, 72, 67 67, 85, 76, 100, 71, 83, 71, 72 83, 71, 86, 79, 88, 79, 69, 72 77, 79, 66, 71, 83, 66, 90, 76 62, 81, 62, 76, 67, 83, 86, 74 77, 83, 71, 94, 81, 69, 81, 76 86, 79, 67, 83, 79, 81, 81, 72 72, 71, 76, 81, 100, 69, 67, 71 81, 72, 76, 86, 77, 71, 72, 77 81, 59, 81, 81, 67, 62, 79, 64 72, 81, 79, 77, 72, 76, 67, 88 62, 79, 79, 83, 72, 58, 66, 77 62, 77, 88, 72, 59, 77, 58, 276 61, 102, 76, 69, 83, 85, 58, 83 77, 81, 83, 67, 76, 76, 71, 74 66, 76, 83, 81, 77, 76, 83, 83 71, 72, 79, 58, 83, 74, 100, 72 77, 71, 88, 76, 86, 72, 69, 94 114, 92, 88, 106, 98, 119, 108, 104 110, 114, 112, 94, 110, 88, 71, 90 83, 86, 85, 79, 71, 92, 76, 74 74, 98, 94, 85, 77, 83, 71, 74 74, 79, 90, 88, 100, 61, 98, 83 88, 86, 83, 83, 94, 77, 94, 94 96, 94, 85, 100, 100, 100, 108, 100 98, 102, 102, 119, 79, 88, 98, 94 94, 102, 92, 96, 66, 72, 72, 102 81, 94, 77, 72, 76, 79, 79, 74 72, 88, 92, 76, 92, 79, 92, 88 55, 86, 88, 81, 86, 100, 92, 76 94, 90, 104, 94, 96, 110, 108, 102 102, 112, 121, 121, 121, 114, 123, 110 108, 102, 96, 104, 100, 94, 86, 94 90, 88, 79, 90, 108, 83, 85, 106 102, 88, 90, 98, 96, 114, 85, 104 119, 85, 88, 98, 90, 94, 92, 90 83, 86, 88, 92, 96, 88, 112, 132 121, 130, 164, 185, 204, 228, 237, 272 279, 272, 299, 279, 237, 222, 166, 123 119, 392, 100, 85, 85, 112, 86, 96 96, 86, 77, 76, 69, 79, 94, 81 96, 92, 81, 98, 69, 83, 92, 104 77, 69, 100, 76, 79, 90, 76, 79 88, 83, 72, 94, 90, 90, 72, 98 83, 77, 79, 74, 96, 112, 86, 86 94, 117, 102, 96, 96, 102, 92, 119 79, 96, 86, 85, 83, 77, 86, 92 81, 88, 79, 86, 90, 79, 67, 92 90, 96, 83, 88, 98, 83, 88, 85 90, 102, 79, 83, 102, 85, 72, 106 83, 77, 77, 102, 106, 86, 121, 102 117, 110, 94, 128, 119, 128, 114, 128 156, 121, 128, 135, 169, 151, 144, 156 146, 125, 132, 130, 123, 130, 132, 114 128, 135, 142, 149, 121, 130, 139, 139 119, 130, 128, 128, 130, 132, 161, 135 114, 114, 114, 119, 130, 110, 125, 112 106, 117, 112, 104, 104, 102, 108, 106 96, 110, 119, 106, 104, 90, 117, 125 106, 119, 121, 117, 119, 121, 108, 114 90, 98, 112, 90, 114, 98, 100, 110 123, 104, 128, 94, 112, 110, 119, 123 108, 132, 114, 144, 130, 154, 151, 169 159, 164, 182, 174, 164, 174, 185, 172 196, 182, 177, 185, 259, 213, 240, 234 234, 253, 250, 222, 204, 207, 182, 182 161, 193, 139, 161, 144, 128, 156, 164 144, 164, 128, 135, 135, 130, 159, 128 117, 128, 130, 117, 96, 106, 108, 117 98, 121, 117, 110, 106, 114, 98, 100 92, 100, 112, 110, 98, 114, 108, 108 125, 119, 100, 142, 112, 128, 117, 135 130, 146, 156, 166, 159, 207, 202, 246 279, 365, 488, 702, 801, 961, 1089, 1176 1369, 1459, 1592, 1560, 1544, 1296, 1149, 906 666, 562, 471, 350, 320, 292, 256, 237 231, 207, 207, 174, 207, 169, 151, 135 159, 130, 135, 130, 142, 135, 130, 137 151, 144, 130, 159, 151, 182, 196, 177 199, 196, 222, 234, 299, 372, 380, 404 313, 276, 246, 207, 174, 164, 164, 166 172, 166, 169, 169, 169, 225, 204, 193 196, 222, 240, 246, 253, 196, 193, 213 166, 149, 121, 130, 139, 110, 125, 117 121, 130, 130, 123, 123, 137, 114, 104 104, 123, 112, 104, 110, 128, 416, 117 98, 123, 121, 114, 114, 94, 85, 114 100, 106, 100, 102, 102, 96, 98, 112 98, 119, 100, 108, 106, 92, 117, 110 128, 125, 104, 121, 132, 132, 135, 164 130, 182, 149, 139, 164, 185, 185, 207 237, 266, 296, 310, 369, 365, 445, 475 471, 552, 538, 581, 590, 620, 600, 620 671, 630, 605, 557, 576, 548, 552, 538 475, 471, 480, 408, 372, 380, 365, 346 350, 339, 310, 306, 313, 276, 262, 292 282, 269, 310, 282, 259, 306, 292, 303 313, 313, 331, 299, 328, 335, 353, 339 365, 404, 361, 353, 380, 372, 376, 335 320, 335, 339, 306, 266, 276, 303, 266 262, 276, 234, 216, 219, 228, 225, 188 188, 234, 225, 188, 169, 169, 159, 164 174, 159, 149, 137, 146, 123, 139, 123 154, 142, 135, 154, 121, 137, 110, 146 121, 119, 146, 132, 112, 142, 146, 161 149, 156, 156, 169, 164, 193, 172, 185 154, 177, 137, 154, 142, 159, 144, 135 142, 132, 128, 130, 144, 154, 130, 135 142, 142, 117, 128, 128, 114, 110, 132 102, 121, 98, 104, 117, 106, 92, 96 100, 114, 100, 94, 90, 100, 88, 85 92, 88, 83, 88, 76, 90, 74, 79 86, 96, 86, 92, 77, 77, 83, 90 86, 86, 85, 90, 104, 102, 104, 137 110, 137, 125, 117, 121, 110, 79, 92 94, 94, 96, 74, 85, 86, 96, 77 88, 81, 85, 92, 108, 81, 72, 88 88, 81, 96, 85, 86, 85, 76, 76 77, 72, 77, 85, 86, 83, 79, 77 79, 74, 86, 90, 67, 74, 79, 79 83, 92, 86, 94, 90, 86, 98, 79 79, 76, 90, 104, 77, 83, 83, 92 86, 92, 96, 98, 104, 108, 112, 106 108, 121, 112, 130, 119, 128, 108, 128 110, 96, 130, 117, 128, 114, 135, 149 125, 142, 123, 132, 135, 149, 161, 123 154, 149, 146, 166, 159, 135, 156, 159 144, 149, 142, 137, 125, 123, 123, 117 114, 114, 102, 125, 112, 106, 106, 92 90, 112, 102, 98, 90, 90, 100, 92 86, 110, 100, 83, 104, 102, 121, 114 121, 112, 112, 112, 121, 121, 123, 135 128, 149, 137, 144, 188, 161, 193, 161 196, 228, 207, 190, 174, 199, 196, 210 185, 216, 196, 185, 159, 177, 169, 177 174, 180, 204, 204, 228, 243, 269, 292 276, 317, 324, 292, 286, 243, 262, 222 193, 182, 193, 144, 137, 139, 169, 139 144, 142, 123, 193, 169, 146, 174, 180 166, 182, 199, 177, 177, 188, 174, 159 142, 166, 151, 149, 130, 121, 119, 104 132, 130, 119, 114, 110, 137, 128, 132 128, 119, 121, 137, 119, 123, 110, 121 121, 130, 119, 135, 119, 108, 123, 108 114, 114, 114, 119, 83, 102, 125, 98 83, 94, 94, 96, 88, 104, 102, 92 100, 85, 92, 88, 92, 108, 90, 104 98, 114, 88, 106, 100, 90, 108, 86 88, 92, 90, 77, 90, 94, 88, 85 83, 94, 79, 100, 90, 79, 85, 72 76, 77, 90, 71, 90, 71, 79, 61 76, 88, 92, 86, 88, 90, 81, 69 92, 94, 92, 96, 96, 104, 90, 81 119, 102, 121, 142, 137, 169, 177, 216 237, 246, 250, 266, 310, 292, 269, 303 276, 253, 246, 272, 237, 243, 210, 213 196, 202, 196, 204, 182, 185, 174, 169 196, 159, 154, 172, 161, 164, 169, 144 177, 169, 144, 156, 156, 144, 149, 164 169, 188, 188, 190, 185, 216, 202, 196 199, 174, 210, 172, 159, 154, 151, 159 132, 154, 177, 177, 164, 199, 172, 182 202, 196, 216, 188, 188, 202, 207, 193 149, 177, 159, 164, 146, 144, 149, 142 164, 159, 125, 108, 135, 132, 117, 130 125, 110, 119, 117, 102, 121, 102, 102 83, 108, 112, 98, 100, 88, 88, 94 110, 92, 86, 77, 112, 76, 96, 81 83, 88, 96, 98, 130, 90, 83, 119 110, 94, 114, 92, 90, 108, 98, 98 83, 83, 76, 85, 94, 94, 100, 104 85, 104, 102, 104, 104, 94, 100, 135 119, 104, 130, 137, 164, 169, 180, 177 193, 219, 202, 193, 169, 159, 137, 142 137, 137, 132, 121, 86, 83, 104, 86 112, 85, 94, 102, 117, 104, 102, 90 110, 100, 106, 104, 100, 104, 94, 135 117, 139, 151, 130, 154, 156, 180, 185 172, 202, 207, 210, 207, 196, 188, 207 207, 240, 210, 225, 207, 196, 182, 188 182, 161, 172, 174, 172, 182, 161, 164 169, 161, 161, 135, 149, 149, 164, 174 156, 177, 177, 159, 166, 169, 164, 142 139, 132, 149, 112, 174, 142, 149, 144 142, 135, 128, 156, 156, 159, 156, 169 156, 199, 180, 190, 210, 188, 207, 228 204, 231, 246, 234, 213, 193, 185, 185 180, 174, 174, 151, 161, 159, 132, 164 135, 137, 132, 149, 137, 142, 151, 144 139, 130, 114, 132, 149, 137, 121, 149 117, 146, 130, 144, 142, 144, 146, 193 156, 196, 159, 185, 166, 182, 190, 199 207, 161, 199, 144, 149, 164, 159, 137 139, 144, 156, 154, 169, 166, 177, 159 204, 210, 169, 172, 151, 139, 135, 156 121, 121, 139, 108, 90, 104, 83, 102 106, 79, 98, 102, 83, 100, 85, 90 100, 98, 96, 85, 96, 98, 79, 81 77, 90, 81, 100, 77, 72, 86, 86 98, 76, 88, 79, 76, 77, 83, 67 90, 96, 92, 98, 102, 85, 88, 90 72, 102, 86, 92, 98, 100, 106, 112 137, 102, 117, 117, 114, 110, 108, 119 146, 142, 149, 146, 137, 137, 146, 149 154, 156, 149, 174, 204, 159, 166, 174 154, 154, 151, 144, 149, 151, 169, 154 169, 172, 154, 166, 202, 193, 169, 185 177, 164, 180, 177, 169, 188, 180, 172 174, 219, 156, 169, 169, 177, 164, 164 174, 166, 159, 159, 164, 180, 156, 161 159, 159, 154, 151, 169, 193, 156, 154 174, 185, 199, 202, 164, 196, 210, 204 222, 219, 228, 202, 234, 213, 243, 231 222, 240, 222, 207, 196, 193, 202, 240 216, 199, 190, 193, 185, 188, 185, 177 177, 161, 164, 169, 159, 149, 142, 169 146, 174, 146, 159, 146, 156, 159, 156 169, 169, 135, 144, 128, 172, 144, 146 146, 132, 182, 164, 132, 159, 142, 164 166, 164, 154, 156, 169, 169, 169, 174 185, 202, 207, 225, 292, 346, 357, 388 437, 416, 392, 376, 380, 306, 310, 296 289, 276, 222, 202, 199, 169, 174, 159 149, 128, 149, 128, 164, 144, 142, 149 149, 144, 159, 146, 144, 174, 135, 121 130, 119, 139, 137, 146, 112, 121, 123 102, 119, 121, 119, 90, 98, 121, 114 92, 119, 94, 110, 98, 130, 104, 102 108, 94, 98, 90, 88, 83, 77, 86 77, 85, 66, 69, 72, 83, 85, 77 86, 72, 74, 81, 66, 76, 62, 77 83, 67, 76, 85, 72, 72, 79, 74 64, 79, 61, 66, 71, 67, 79, 66 72, 67, 94, 79, 74, 71, 71, 77 83, 76, 90, 64, 85, 74, 79, 76 86, 90, 88, 94, 86, 81, 74, 85 81, 81, 77, 74, 85, 88, 77, 62 94, 96, 74, 74, 88, 66, 94, 94 88, 83, 67, 83, 88, 72, 90, 85 72, 86, 83, 76, 74, 83, 67, 86 77, 83, 86, 94, 71, 86, 90, 85 83, 81, 79, 77, 74, 86, 83, 79 72, 79, 88, 76, 71, 86, 53, 74 69, 83, 74, 79, 71, 90, 79, 69 76, 71, 76, 90, 74, 77, 96, 94 72, 72, 102, 92, 88, 92, 62, 79 83, 79, 83, 83, 77, 79, 81, 83 77, 86, 106, 108, 86, 85, 77, 77 92, 79, 88, 90, 83, 69, 86, 85 92, 88, 85, 102, 102, 96, 92, 102 135, 146, 142, 164, 159, 196, 202, 219 202, 190, 182, 159, 149, 182, 149, 137 156, 135, 128, 125, 130, 119, 110, 119 114, 137, 137, 135, 125, 119, 119, 128 130, 119, 112, 132, 106, 142, 106, 108 104, 108, 121, 117, 100, 112, 114, 108 100, 110, 94, 102, 112, 119, 110, 100 100, 119, 110, 114, 102, 108, 102, 98 106, 86, 123, 112, 130, 132, 125, 130 135, 149, 169, 161, 128, 128, 119, 121 132, 149, 132, 114, 121, 102, 108, 117 104, 106, 86, 117, 98, 114, 102, 114 108, 104, 108, 112, 123, 104, 114, 110 104, 96, 94, 137, 121, 110, 100, 123 98, 112, 123, 102, 119, 100, 100, 100 106, 106, 142, 117, 119, 132, 128, 119 149, 125, 137, 128, 146, 164, 164, 161 132, 172, 156, 130, 135, 144, 139, 172 146, 182, 172, 161, 151, 159, 156, 169 169, 137, 130, 139, 144, 146, 139, 132 123, 135, 164, 137, 154, 130, 125, 130 146, 123, 135, 130, 108, 137, 125, 125 112, 137, 121, 130, 114, 130, 121, 104 135, 119, 106, 128, 130, 137, 110, 110 130, 154, 112, 102, 137, 121, 125, 139 146, 123, 121, 142, 139, 146, 108, 159 137, 119, 125, 130, 144, 130, 130, 135 135, 139, 137, 125, 146, 146, 135, 142 130, 123, 110, 130, 135, 125, 123, 125 121, 125, 130, 117, 137, 106, 125, 104 132, 128, 108, 130, 130, 128, 121, 132 135, 110, 144, 151, 135, 190, 182, 225 266, 306, 313, 335, 320, 346, 313, 279 210, 262, 222, 199, 219, 231, 196, 172 149, 137, 96, 100, 125, 104, 104, 100 119, 98, 110, 92, 85, 108, 119, 88 108, 117, 88, 112, 100, 110, 114, 123 123, 128, 146, 125, 135, 121, 135, 132 130, 130, 154, 146, 132, 151, 132, 137 139, 142, 142, 149, 137, 137, 149, 151 164, 121, 156, 130, 149, 135, 123, 135 144, 146, 177, 137, 161, 151, 151, 180 159, 139, 159, 161, 169, 166, 177, 169 164, 169, 154, 156, 174, 161, 161, 135 174, 139, 180, 154, 156, 142, 149, 139 137, 123, 137, 137, 123, 142, 114, 123 144, 121, 114, 130, 117, 123, 125, 123 146, 125, 98, 128, 117, 102, 137, 117 142, 125, 96, 132, 119, 108, 110, 104 117, 106, 125, 121, 112, 119, 119, 119 110, 114, 128, 130, 144, 102, 112, 108 114, 119, 114, 108, 110, 108, 114, 104 121, 98, 112, 110, 96, 130, 128, 112 102, 108, 112, 112, 114, 112, 110, 96 121, 119, 123, 114, 112, 112, 130, 119 128, 104, 114, 110, 104, 102, 142, 125 100, 130, 121, 100, 125, 125, 128, 119 94, 117, 144, 137, 156, 139, 139, 159 149, 164, 146, 110, 135, 132, 164, 117 130, 161, 154, 128, 146, 123, 106, 130 106, 119, 121, 119, 102, 121, 104, 117 125, 128, 121, 119, 110, 119, 132, 117 119, 112, 128, 137, 142, 137, 149, 149 128, 146, 156, 166, 156, 132, 161, 164 154, 139, 151, 154, 144, 139, 159, 149 159, 144, 130, 154, 144, 137, 146, 144 125, 135, 121, 117, 130, 139, 132, 137 135, 112, 144, 128, 121, 144, 110, 110 135, 125, 132, 144, 149, 112, 144, 130 117, 130, 144, 144, 130, 144, 130, 137 144, 123, 135, 125, 130, 121, 142, 137 117, 112, 135, 125, 123, 135, 98, 119 128, 123, 108, 108, 110, 104, 110, 108 112, 114, 114, 106, 96, 128, 112, 128 121, 117, 128, 117, 119, 108, 119, 130 110, 121, 121, 119, 108, 125, 117, 110 121, 104, 112, 130, 121, 130, 123, 121 128, 139, 121, 106, 104, 121, 114, 121 110, 117, 130, 110, 123, 132, 114, 104 106, 106, 142, 114, 112, 98, 121, 106 110, 151, 132, 174, 159, 169, 213, 222 259, 246, 246, 282, 202, 202, 174, 161 164, 204, 185, 196, 188, 185, 202, 196 188, 243, 219, 237, 240, 231, 276, 276 286, 310, 272, 234, 282, 272, 306, 289 253, 225, 231, 199, 204, 180, 185, 161 169, 144, 130, 114, 108, 106, 104, 100 92, 94, 117, 92, 85, 108, 98, 110 106, 92, 90, 112, 102, 77, 88, 98 96, 112, 106, 94, 112, 92, 112, 104 106, 100, 112, 123, 137, 94, 125, 104 125, 121, 114, 108, 110, 132, 117, 137 106, 125, 135, 128, 121, 100, 123, 110 123, 110, 117, 104, 104, 106, 90, 121 132, 112, 121, 90, 98, 108, 112,/