SampleIdent,925A 54R5 67-69 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,20-mar-1994 13:44,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 180, 185, 164, 166, 174, 185, 149, 159 142, 159, 149, 159, 164, 144, 166, 149 159, 159, 149, 164, 159, 185, 137, 172 164, 159, 139, 151, 146, 161, 146, 144 146, 169, 139, 159, 177, 142, 164, 159 144, 172, 139, 144, 144, 146, 144, 166 164, 156, 139, 132, 149, 132, 169, 161 159, 154, 137, 154, 151, 151, 139, 177 164, 159, 149, 156, 149, 154, 137, 185 154, 161, 135, 139, 149, 137, 151, 149 149, 166, 166, 146, 161, 137, 177, 130 151, 142, 156, 144, 137, 161, 164, 154 161, 159, 146, 154, 130, 159, 142, 149 159, 180, 146, 169, 154, 164, 135, 166 154, 142, 149, 151, 177, 130, 182, 146 182, 135, 164, 172, 190, 172, 164, 164 130, 161, 169, 169, 154, 154, 188, 177 164, 164, 196, 149, 164, 180, 169, 166 174, 185, 159, 154, 161, 154, 193, 169 166, 177, 188, 177, 177, 177, 161, 164 154, 166, 177, 172, 174, 159, 180, 174 182, 182, 193, 185, 172, 188, 177, 185 172, 204, 185, 190, 174, 172, 188, 213 196, 202, 185, 185, 188, 185, 199, 172 193, 177, 188, 169, 199, 213, 202, 219 193, 193, 190, 190, 228, 219, 196, 213 219, 219, 222, 207, 193, 188, 216, 213 228, 202, 159, 213, 213, 231, 213, 204 207, 234, 231, 199, 222, 231, 207, 231 216, 231, 228, 210, 231, 207, 219, 228 243, 219, 216, 250, 228, 231, 243, 246 253, 253, 234, 234, 225, 228, 256, 266 253, 246, 250, 250, 253, 246, 282, 240 240, 262, 253, 234, 246, 243, 266, 259 269, 259, 272, 272, 246, 279, 256, 272 276, 272, 276, 272, 243, 262, 276, 272 266, 286, 282, 306, 303, 279, 310, 292 286, 276, 272, 272, 282, 299, 276, 303 256, 276, 306, 306, 289, 289, 256, 246 276, 250, 259, 279, 269, 279, 292, 279 279, 250, 272, 250, 286, 266, 262, 282 269, 259, 272, 253, 240, 253, 253, 282 246, 237, 231, 234, 234, 225, 216, 213 210, 225, 225, 225, 228, 231, 240, 225 196, 204, 222, 210, 210, 188, 182, 185 193, 219, 185, 199, 246, 210, 180, 202 196, 225, 166, 196, 199, 185, 185, 193 169, 172, 216, 207, 202, 188, 193, 182 185, 185, 207, 177, 182, 169, 164, 188 182, 193, 156, 182, 174, 164, 193, 182 177, 199, 188, 154, 188, 169, 177, 159 185, 172, 174, 169, 161, 159, 154, 172 142, 190, 156, 151, 146, 174, 182, 169 180, 156, 169, 164, 174, 154, 156, 174 164, 156, 139, 151, 137, 159, 149, 166 149, 177, 135, 154, 144, 135, 172, 164 154, 161, 139, 182, 154, 169, 166, 174 142, 149, 156, 146, 164, 164, 137, 144 144, 164, 159, 132, 161, 154, 144, 130 144, 146, 154, 139, 154, 139, 149, 149 114, 135, 137, 130, 142, 119, 154, 144 164, 125, 142, 132, 114, 144, 142, 151 125, 110, 146, 137, 130, 161, 137, 130 149, 125, 151, 149, 137, 121, 135, 137 139, 144, 121, 112, 137, 137, 144, 123 142, 142, 144, 108, 130, 119, 146, 154 135, 130, 125, 137, 119, 139, 119, 135 110, 110, 123, 121, 130, 119, 110, 121 139, 144, 137, 146, 151, 144, 144, 121 130, 123, 125, 121, 117, 125, 135, 121 121, 123, 123, 108, 121, 128, 121, 125 128, 130, 128, 151, 137, 128, 137, 142 142, 119, 123, 139, 130, 151, 130, 130 123, 108, 121, 130, 130, 149, 130, 128 142, 144, 121, 135, 132, 132, 119, 128 144, 128, 142, 132, 112, 125, 117, 144 128, 128, 144, 125, 119, 125, 110, 123 146, 117, 130, 139, 110, 121, 132, 139 130, 137, 121, 125, 114, 104, 130, 137 119, 149, 119, 114, 135, 102, 139, 132 149, 130, 112, 132, 132, 130, 119, 151 146, 135, 128, 142, 137, 130, 130, 130 139, 139, 135, 110, 123, 135, 125, 137 132, 123, 128, 149, 121, 139, 130, 110 125, 125, 130, 135, 144, 139, 130, 142 128, 135, 139, 144, 149, 144, 125, 123 135, 117, 110, 123, 114, 139, 117, 130 128, 137, 123, 125, 112, 119, 146, 139 128, 112, 149, 108, 125, 114, 125, 135 123, 123, 117, 123, 130, 144, 106, 142 123, 128, 110, 121, 139, 132, 144, 106 123, 130, 121, 119, 132, 121, 123, 128 117, 130, 112, 112, 149, 135, 121, 123 132, 128, 121, 132, 121, 132, 130, 130 146, 112, 130, 135, 125, 102, 121, 119 144, 130, 121, 149, 135, 135, 146, 156 144, 149, 146, 146, 156, 177, 177, 156 182, 146, 164, 130, 159, 132, 159, 156 159, 156, 144, 142, 149, 137, 123, 139 142, 123, 128, 123, 119, 132, 110, 130 137, 121, 123, 130, 117, 110, 125, 125 119, 112, 117, 125, 135, 121, 125, 100 137, 130, 117, 121, 119, 88, 112, 137 151, 108, 108, 117, 106, 112, 112, 123 119, 130, 114, 119, 121, 117, 112, 94 130, 112, 121, 121, 121, 98, 102, 98 125, 110, 121, 112, 112, 130, 108, 104 104, 112, 102, 117, 119, 104, 114, 92 132, 92, 106, 121, 121, 132, 108, 102 98, 98, 112, 96, 110, 104, 94, 114 104, 98, 92, 104, 100, 85, 83, 102 110, 100, 104, 92, 104, 106, 104, 102 90, 117, 98, 108, 104, 98, 110, 117 92, 92, 104, 100, 106, 98, 114, 119 123, 137, 108, 112, 98, 110, 108, 104 128, 104, 92, 104, 96, 90, 106, 94 81, 108, 90, 108, 86, 106, 86, 90 85, 98, 114, 100, 85, 108, 94, 108 102, 100, 96, 98, 85, 81, 104, 106 102, 104, 96, 100, 100, 110, 90, 117 104, 108, 106, 132, 110, 86, 110, 76 92, 102, 96, 106, 119, 94, 106, 117 108, 123, 94, 119, 108, 121, 117, 102 117, 108, 121, 135, 123, 110, 135, 117 123, 119, 130, 144, 117, 137, 128, 132 121, 172, 154, 149, 144, 149, 149, 139 156, 139, 154, 174, 166, 156, 199, 199 154, 180, 177, 204, 219, 213, 213, 228 231, 240, 213, 202, 231, 222, 250, 213 213, 207, 216, 199, 202, 202, 182, 185 174, 146, 161, 159, 130, 149, 166, 135 119, 137, 142, 137, 135, 149, 128, 123 117, 132, 139, 121, 121, 110, 123, 117 100, 96, 114, 100, 104, 106, 108, 100 100, 96, 106, 98, 106, 114, 102, 110 112, 108, 100, 112, 98, 104, 85, 114 104, 106, 121, 98, 104, 88, 123, 94 94, 86, 96, 96, 88, 100, 104, 94 106, 90, 114, 106, 100, 94, 110, 94 108, 98, 100, 76, 76, 104, 108, 102 104, 94, 106, 112, 108, 88, 121, 94 85, 119, 100, 106, 92, 92, 104, 92 106, 90, 102, 86, 77, 96, 96, 90 112, 132, 92, 85, 106, 85, 96, 98 100, 98, 96, 110, 112, 108, 90, 104 92, 104, 108, 88, 108, 104, 102, 98 92, 100, 100, 96, 104, 112, 114, 90 104, 94, 74, 92, 98, 104, 96, 92 117, 90, 106, 85, 92, 92, 104, 90 104, 100, 86, 96, 83, 98, 106, 100 90, 106, 96, 100, 92, 83, 98, 102 96, 106, 98, 88, 132, 92, 106, 98 100, 88, 110, 92, 83, 86, 112, 86 94, 106, 81, 98, 85, 88, 100, 92 100, 85, 104, 86, 88, 85, 96, 104 119, 119, 88, 100, 94, 102, 117, 94 106, 76, 98, 100, 86, 102, 104, 90 106, 104, 110, 104, 100, 94, 90, 86 106, 96, 110, 100, 90, 98, 100, 117 110, 98, 100, 94, 94, 92, 100, 125 119, 108, 94, 98, 108, 110, 117, 94 85, 108, 100, 96, 114, 96, 98, 94 110, 114, 94, 112, 110, 117, 96, 96 106, 106, 112, 108, 110, 96, 112, 100 94, 98, 128, 117, 117, 94, 142, 98 121, 132, 102, 132, 83, 102, 119, 106 114, 117, 108, 114, 130, 117, 130, 119 123, 108, 102, 90, 90, 108, 100, 102 119, 130, 98, 128, 117, 112, 119, 106 123, 100, 125, 135, 137, 114, 110, 110 102, 121, 108, 119, 123, 117, 121, 121 114, 114, 128, 114, 108, 90, 130, 108 106, 139, 96, 128, 144, 114, 104, 128 119, 106, 117, 106, 90, 108, 132, 104 114, 110, 98, 125, 110, 108, 121, 132 112, 121, 102, 121, 106, 121, 98, 104 106, 110, 117, 121, 117, 121, 132, 92 119, 96, 110, 106, 94, 100, 114, 130 119, 100, 112, 128, 123, 125, 106, 110 110, 106, 125, 117, 106, 130, 104, 125 121, 96, 94, 121, 121, 130, 112, 121 110, 121, 104, 112, 94, 98, 149, 117 121, 110, 132, 117, 108, 121, 121, 121 125, 114, 128, 106, 121, 106, 110, 114 112, 114, 119, 114, 106, 108, 106, 137 102, 119, 132, 117, 96, 102, 112, 106 104, 108, 100, 110, 117, 117, 108, 110 123, 119, 106, 112, 117, 98, 106, 114 110, 112, 94, 110, 119, 110, 121, 114 128, 104, 119, 135, 106, 117, 121, 117 112, 110, 132, 130, 110, 123, 130, 144 130, 128, 128, 110, 135, 123, 130, 121 110, 106, 104, 121, 128, 121, 123, 123 128, 121, 139, 121, 112, 123, 130, 121 106, 112, 114, 114, 121, 121, 125, 132 121, 144, 108, 112, 142, 139, 108, 128 121, 130, 106, 106, 119, 144, 125, 132 132, 114, 130, 123, 121, 135, 135, 125 119, 132, 125, 123, 128, 130, 121, 94 130, 130, 121, 112, 130, 132, 123, 123 114, 154, 125, 125, 137, 123, 139, 119 128, 135, 139, 137, 135, 121, 149, 121 114, 119, 110, 123, 130, 128, 128, 130 130, 117, 149, 142, 121, 139, 125, 130 130, 114, 114, 132, 132, 106, 137, 123 132, 135, 132, 146, 135, 123, 117, 137 142, 123, 121, 139, 128, 123, 142, 112 139, 125, 130, 119, 142, 146, 146, 128 137, 137, 130, 123, 128, 135, 130, 144 119, 154, 121, 142, 146, 125, 154, 139 121, 137, 130, 137, 114, 149, 121, 137 128, 144, 130, 139, 130, 139, 132, 135 154, 142, 135, 121, 159, 132, 164, 149 135, 142, 146, 154, 144, 132, 151, 135 139, 166, 142, 135, 151, 142, 137, 135 137, 161, 137, 130, 151, 142, 149, 146 159, 137, 164, 144, 149, 137, 149, 142 172, 151, 149, 161, 156, 154, 144, 185 174, 164, 161, 202, 164, 185, 182, 159 174, 174, 207, 180, 193, 199, 188, 207 228, 196, 193, 210, 210, 210, 222, 213 219, 256, 237, 246, 272, 276, 256, 243 246, 286, 269, 253, 266, 276, 225, 256 253, 256, 266, 231, 231, 282, 262, 276 246, 272, 259, 256, 228, 246, 246, 246 231, 231, 234, 231, 256, 234, 225, 246 225, 231, 219, 234, 225, 225, 228, 246 225, 237, 231, 219, 240, 219, 240, 210 259, 237, 259, 253, 222, 228, 213, 228 216, 250, 234, 225, 202, 216, 225, 246 222, 225, 199, 256, 216, 234, 225, 246 222, 234, 225, 207, 262, 237, 256, 231 231, 210, 250, 213, 216, 256, 210, 266 246, 262, 237, 231, 253, 243, 259, 243 237, 262, 253, 279, 306, 276, 292, 276 272, 296, 296, 296, 282, 328, 279, 303 303, 286, 276, 272, 250, 259, 237, 234 237, 219, 246, 225, 231, 234, 210, 234 234, 228, 219, 246, 250, 250, 262, 228 246, 228, 246, 234, 196, 228, 225, 231 231, 240, 234, 213, 231, 216, 237, 237 228, 237, 253, 210, 234, 234, 246, 256 246, 246, 253, 228, 234, 231, 222, 234 240, 250, 276, 240, 243, 237, 222, 228 225, 262, 225, 269, 250, 213, 246, 272 246, 253, 253, 266, 225, 228, 240, 246 225, 246, 228, 222, 231, 246, 266, 237 259, 231, 246, 259, 240, 237, 256, 279 259, 234, 256, 243, 253, 237, 219, 262 240, 243, 266, 222, 256, 225, 272, 234 246, 234, 259, 234, 237, 234, 259, 234 216, 231, 259, 222, 256, 213, 250, 228 250, 213, 231, 240, 246, 234, 237, 237 262, 256, 231, 269, 243, 243, 250, 256 243, 228, 243, 219, 240, 250, 259, 237 240, 266, 250, 243, 228, 237, 234, 231 259, 243, 228, 234, 202, 246, 237, 225 234, 259, 243, 234, 216, 250, 225, 231 272, 222, 228, 219, 234, 228, 243, 253 225, 240, 216, 207, 246, 256, 231, 243 231, 216, 222, 222, 234, 246, 225, 253 243, 240, 237, 243, 225, 246, 228, 234 269, 225, 231, 231, 228, 222, 210, 243 240, 225, 231, 210, 231, 210, 237, 207 213, 222, 213, 199, 246, 231, 256, 228 210, 240, 234, 234, 219, 202, 188, 243 222, 219, 222, 202, 216, 234, 250, 231 202, 202, 222, 213, 246, 216, 240, 222 240, 228, 222, 222, 250, 199, 225, 231 199, 237, 213, 237, 250, 210, 228, 216 207, 237, 207, 231, 240, 207, 259, 266 240, 234, 256, 234, 259, 228, 207, 213 202, 228, 213, 213, 246, 228, 228, 231 246, 234, 237, 231, 243, 234, 231, 231 237, 243, 240, 202, 207, 207, 243, 234 237, 237, 231, 210, 259, 225, 213, 240 243, 222, 253, 234, 234, 246, 222, 210 279, 225, 237, 272, 210, 228, 219, 222 243, 234, 262, 240, 243, 228, 237, 256 237, 250, 237, 222, 228, 228, 231, 259 219, 225, 219, 276, 240, 276, 250, 253 228, 225, 253, 246, 256, 259, 256, 272 240, 262, 296, 240, 266, 276, 269, 292 269, 286, 324, 296, 310, 317, 353, 296 353, 365, 339, 369, 380, 380, 396, 400 392, 376, 380, 404, 376, 392, 396, 369 372, 376, 404, 365, 353, 346, 339, 346 320, 335, 310, 328, 296, 279, 279, 328 289, 282, 286, 292, 279, 306, 296, 286 289, 246, 320, 306, 253, 320, 289, 272 289, 259, 282, 279, 296, 279, 296, 262 306, 282, 279, 250, 299, 262, 286, 259 262, 269, 259, 240, 282, 289, 286, 246 256, 266, 259, 250, 240, 259, 269, 237 262, 243, 237, 276, 240, 269, 276, 269 286, 231, 266, 256, 262, 234, 272, 262 225, 279, 250, 282, 253, 303, 289, 266 253, 272, 256, 240, 259, 299, 243, 269 262, 279, 269, 279, 282, 276, 259, 269 286, 256, 279, 256, 266, 262, 262, 246 276, 266, 286, 272, 282, 272, 231, 259 282, 250, 286, 306, 286, 269, 266, 310 276, 272, 289, 303, 279, 282, 256, 276 276, 286, 256, 286, 266, 272, 266, 286 286, 272, 272, 306, 282, 324, 310, 313 299, 292, 346, 331, 353, 339, 328, 396 342, 420, 416, 471, 484, 502, 493, 548 605, 600, 625, 620, 681, 724, 697, 671 605, 692, 620, 590, 511, 506, 449, 441 445, 357, 376, 328, 328, 335, 317, 313 286, 286, 296, 296, 286, 286, 259, 272 286, 313, 276, 266, 286, 276, 250, 262 234, 269, 237, 272, 262, 256, 246, 253 246, 250, 259, 250, 234, 246, 272, 234 253, 222, 240, 246, 240, 231, 228, 231 234, 259, 253, 231, 259, 237, 246, 246 243, 246, 231, 237, 250, 222, 231, 272 234, 266, 256, 246, 250, 237, 286, 231 225, 231, 246, 253, 259, 246, 246, 228 240, 250, 225, 234, 225, 256, 250, 259 243, 240, 243, 250, 243, 243, 219, 234 246, 231, 237, 237, 222, 222, 222, 231 231, 225, 243, 231, 246, 250, 237, 231 243, 250, 234, 231, 222, 246, 259, 234 259, 253, 234, 219, 253, 196, 243, 228 207, 228, 231, 231, 207, 240, 228, 240 219, 225, 213, 177, 207, 219, 219, 237 210, 210, 234, 228, 225, 216, 225, 225 237, 243, 222, 225, 210, 216, 216, 228 219, 222, 199, 228, 231, 243, 202, 207 188, 216, 216, 222, 216, 213, 219, 213 213, 222, 213, 237, 231, 188, 225, 219 231, 222, 210, 210, 234, 219, 213, 210 199, 213, 210, 207, 196, 225, 222, 213 216, 219, 213, 185, 228, 204, 199, 204 231, 196, 199, 222, 222, 210, 202, 202 213, 204, 243, 210, 193, 222, 202, 207 204, 188, 213, 196, 204, 216, 216, 210 204, 234, 204, 196, 204, 193, 180, 207 207, 222, 188, 225, 210, 210, 216, 219 213, 199, 204, 193, 207, 210, 213, 196 210, 210, 202, 199, 193, 228, 188, 204 219, 222, 207, 188, 202, 243, 196, 202 188, 228, 210, 225, 246, 202, 219, 213 219, 190, 210, 234, 199, 182, 225, 204 210, 196, 219, 210, 199, 228, 193, 213 180, 246, 231, 207, 231, 219, 228, 210 202, 210, 202, 237, 202, 243, 222, 199 222, 219, 219, 207, 246, 196, 225, 237 213, 185, 225, 204, 213, 219, 210, 210 219, 216, 193, 228, 246, 225, 210, 182 185, 213, 231, 222, 202, 199, 210, 222 182, 222, 190, 213, 216, 204, 204, 196 207, 213, 207, 204, 237, 210, 219, 222 213, 213, 210, 202, 210, 225, 210, 177 185, 207, 204, 207, 199, 204, 207, 199 185, 237, 216, 174, 213, 202, 243, 196 204, 231, 207, 196, 182, 199, 213, 185 219, 213, 216, 202, 188, 213, 210, 202 210, 204, 202, 196, 190, 196, 185, 207 219, 216, 213, 202, 196, 219, 202, 207 216, 193, 185, 222, 185, 169, 225, 177 222, 196, 204, 222, 219, 213, 207, 202 188, 216, 182, 177, 185, 199, 204, 225 202, 202, 188, 196, 216, 196, 210, 210 190, 180, 180, 196, 190, 210, 210, 222 228, 199, 228, 196, 202, 190, 202, 199 188, 213, 202, 228, 202, 199, 202, 222 225, 213, 177, 185, 190, 161, 188, 196 204, 188, 185, 188, 213, 207, 231, 199 193, 202, 210, 190, 196, 188, 202, 193 190, 177, 202, 219, 177, 213, 199, 185 193, 207, 190, 185, 182, 196, 202, 180 213, 216, 190, 219, 216, 207, 219, 161 182, 193, 237, 219, 202, 185, 213, 188 202, 188, 193, 196, 188, 180, 196, 199 196, 182, 202, 172, 185, 182, 180, 190 193, 193, 188, 174, 185, 188, 182, 196 188, 188, 174, 156, 169, 196, 193, 190 185, 193, 172, 180, 193, 169, 156, 182 193, 185, 185, 174, 193, 199, 193, 169 180, 219, 166, 174, 188, 177, 202, 193 193, 190, 188, 196, 210, 188, 182, 156 210, 204, 166, 172, 177, 182, 193, 169 177, 164, 180, 185, 164, 204, 172, 196 196, 164, 174, 185, 169, 188, 190, 174 154, 199, 177, 193, 164, 185, 182, 159 216, 202, 180, 159, 188, 174, 196, 185 182, 190, 177, 166, 193, 166, 164, 161 182, 174, 182, 182, 185, 182, 172, 159 190, 169, 202, 156, 190, 174, 164, 159 164, 169, 216, 159, 182, 159, 156, 164 188, 185, 159, 156, 166, 164, 169, 156 156, 190, 182, 164, 156, 161, 177, 154 166, 159, 149, 159, 185, 169, 169, 188 172, 172, 166, 149, 169, 180, 172, 146 164, 166, 174, 156, 154, 180, 149, 159 161, 199, 188, 182, 185, 156, 174, 169 174, 159, 169, 182, 137, 193, 159, 149 185, 180, 159, 164, 164, 164, 177, 164 164, 190, 149, 154, 174, 164, 169, 164 166, 172, 188, 177, 161, 164, 161, 161 174, 159, 188, 193, 159, 188, 174, 174 177, 196, 177, 199, 159, 154, 185, 154 182, 182, 174, 193, 182, 210, 174, 199 207, 177, 185, 196, 196, 188, 190, 199 164, 188, 174, 216, 202, 159, 207, 188 204, 207, 228, 234, 219, 219, 216, 185 228, 216, 199, 210, 225, 204, 225, 228 237, 219, 240, 237, 202, 210, 213, 231 234, 213, 237, 240, 199, 222, 219, 219 213, 231, 231, 246, 237, 228, 222, 222 240, 228, 210,/