SampleIdent,925D 22H1 85-87 CLAY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,11-mar-1994 6:21,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 276, 269, 266, 246, 228, 253, 253, 234 243, 216, 231, 250, 250, 234, 259, 240 272, 243, 237, 259, 225, 231, 272, 225 216, 231, 231, 250, 213, 240, 225, 213 207, 240, 237, 216, 213, 216, 228, 207 246, 222, 228, 216, 246, 240, 243, 216 225, 222, 262, 204, 237, 237, 246, 228 210, 216, 234, 213, 225, 225, 228, 219 219, 231, 228, 222, 216, 228, 231, 237 228, 231, 207, 225, 228, 234, 237, 207 253, 222, 213, 234, 219, 219, 210, 193 199, 219, 216, 228, 207, 216, 207, 202 193, 216, 222, 222, 199, 210, 246, 225 196, 219, 216, 180, 216, 225, 228, 213 193, 246, 204, 202, 222, 182, 225, 207 180, 213, 213, 240, 193, 237, 213, 231 196, 188, 213, 202, 193, 216, 204, 225 196, 202, 231, 213, 219, 210, 196, 196 207, 219, 210, 228, 204, 219, 199, 190 182, 216, 216, 225, 219, 216, 207, 188 210, 204, 213, 210, 253, 202, 225, 228 256, 216, 193, 213, 231, 228, 196, 222 231, 225, 219, 222, 202, 199, 225, 210 188, 202, 210, 202, 234, 243, 193, 225 207, 210, 202, 228, 210, 204, 222, 228 253, 219, 216, 202, 250, 225, 182, 210 216, 207, 219, 225, 222, 193, 225, 213 204, 222, 240, 216, 237, 188, 216, 219 207, 213, 188, 190, 225, 196, 190, 237 222, 222, 225, 219, 210, 240, 225, 196 222, 225, 237, 237, 237, 202, 199, 228 210, 216, 216, 228, 240, 225, 210, 207 225, 199, 216, 246, 213, 213, 231, 210 222, 199, 231, 210, 210, 207, 228, 216 237, 199, 210, 213, 222, 231, 250, 222 225, 237, 225, 234, 225, 219, 190, 219 225, 234, 210, 231, 231, 240, 213, 243 225, 237, 225, 250, 190, 202, 228, 246 216, 222, 204, 240, 228, 213, 240, 202 243, 237, 269, 222, 222, 222, 219, 231 219, 228, 222, 250, 225, 213, 253, 259 269, 225, 237, 243, 246, 259, 228, 240 234, 228, 246, 216, 256, 219, 240, 272 234, 256, 240, 256, 243, 262, 240, 234 243, 237, 237, 269, 246, 269, 246, 256 250, 259, 246, 259, 237, 237, 243, 262 234, 243, 269, 240, 237, 262, 246, 262 276, 266, 266, 234, 225, 237, 225, 266 279, 234, 256, 240, 246, 243, 237, 250 279, 250, 243, 250, 246, 231, 253, 250 276, 266, 225, 246, 246, 259, 243, 207 240, 289, 256, 250, 253, 256, 246, 262 246, 231, 231, 246, 246, 250, 256, 234 279, 234, 246, 216, 237, 216, 204, 222 219, 202, 204, 234, 228, 199, 207, 219 216, 204, 213, 193, 213, 228, 219, 256 199, 207, 207, 190, 185, 204, 202, 228 199, 216, 193, 196, 210, 219, 222, 219 199, 199, 196, 222, 219, 216, 204, 199 182, 207, 207, 193, 228, 213, 193, 196 231, 204, 180, 207, 188, 222, 196, 193 180, 169, 210, 213, 190, 202, 185, 210 196, 182, 216, 202, 204, 193, 210, 182 169, 182, 174, 196, 196, 185, 202, 185 185, 190, 210, 172, 174, 196, 174, 185 166, 210, 193, 172, 196, 199, 196, 182 169, 188, 182, 185, 159, 182, 193, 188 182, 174, 199, 188, 169, 180, 180, 174 193, 182, 182, 169, 161, 180, 156, 185 188, 172, 156, 169, 188, 174, 190, 193 177, 196, 169, 182, 154, 180, 172, 169 182, 166, 174, 166, 182, 166, 185, 182 149, 161, 188, 169, 172, 164, 196, 172 180, 177, 154, 164, 190, 169, 182, 180 161, 172, 154, 180, 161, 177, 177, 207 172, 204, 210, 196, 164, 177, 164, 149 180, 193, 154, 210, 190, 185, 196, 146 177, 185, 174, 182, 199, 169, 177, 180 196, 182, 182, 159, 154, 177, 174, 210 172, 169, 169, 164, 185, 174, 169, 164 185, 161, 188, 174, 188, 188, 210, 188 166, 193, 213, 182, 202, 207, 202, 210 166, 193, 202, 216, 202, 210, 210, 188 237, 243, 237, 199, 240, 234, 225, 225 246, 262, 228, 272, 259, 276, 243, 231 222, 225, 225, 188, 216, 182, 193, 193 177, 185, 177, 177, 172, 159, 159, 169 161, 172, 174, 156, 154, 177, 151, 166 149, 144, 164, 144, 146, 137, 135, 142 137, 154, 146, 142, 144, 130, 144, 151 135, 125, 139, 121, 128, 135, 132, 135 137, 132, 132, 144, 146, 139, 142, 149 159, 128, 98, 137, 130, 130, 123, 106 132, 121, 106, 137, 125, 130, 106, 110 125, 130, 128, 121, 119, 117, 125, 121 125, 106, 137, 123, 104, 123, 130, 121 110, 104, 108, 112, 123, 110, 137, 119 123, 128, 102, 108, 112, 125, 106, 100 108, 137, 114, 96, 121, 98, 130, 119 106, 125, 104, 96, 123, 104, 114, 94 119, 106, 86, 114, 108, 121, 90, 110 94, 121, 119, 114, 132, 104, 119, 104 104, 104, 119, 128, 123, 96, 106, 94 117, 128, 114, 119, 108, 100, 110, 104 104, 110, 102, 132, 92, 108, 121, 121 106, 110, 86, 130, 110, 128, 121, 112 102, 106, 125, 112, 102, 139, 117, 102 130, 121, 117, 108, 110, 110, 117, 125 106, 106, 100, 119, 104, 123, 96, 130 125, 110, 102, 94, 119, 110, 112, 108 114, 106, 128, 123, 130, 110, 98, 102 123, 117, 123, 123, 123, 114, 102, 128 121, 98, 121, 108, 110, 130, 108, 108 98, 123, 108, 114, 121, 104, 119, 108 100, 100, 108, 114, 125, 117, 100, 130 110, 102, 125, 123, 106, 121, 128, 104 104, 88, 117, 130, 123, 119, 117, 117 128, 123, 121, 137, 110, 114, 104, 108 121, 98, 123, 114, 106, 132, 94, 121 130, 110, 128, 142, 104, 125, 102, 119 108, 130, 135, 125, 102, 110, 98, 121 130, 135, 125, 156, 125, 121, 130, 135 121, 144, 146, 125, 139, 149, 149, 128 135, 156, 135, 149, 130, 177, 156, 128 166, 139, 166, 172, 164, 161, 166, 180 166, 185, 159, 180, 169, 188, 177, 193 216, 210, 210, 204, 216, 207, 243, 234 259, 243, 276, 279, 279, 269, 262, 292 253, 292, 292, 328, 306, 282, 289, 282 299, 262, 237, 272, 237, 237, 237, 207 225, 199, 231, 231, 213, 219, 196, 174 193, 164, 156, 164, 169, 142, 135, 117 142, 146, 137, 125, 132, 123, 125, 125 128, 98, 125, 125, 114, 144, 114, 146 106, 117, 106, 94, 96, 132, 100, 98 112, 119, 117, 90, 110, 112, 100, 100 117, 100, 96, 119, 117, 106, 110, 92 94, 114, 110, 100, 106, 102, 106, 106 108, 114, 85, 100, 83, 104, 108, 92 110, 104, 98, 114, 110, 102, 104, 106 108, 98, 110, 108, 119, 108, 121, 108 117, 94, 88, 94, 96, 106, 108, 83 110, 106, 98, 94, 106, 90, 94, 102 94, 94, 94, 100, 110, 88, 90, 88 100, 98, 114, 98, 77, 88, 104, 117 100, 102, 98, 98, 96, 98, 106, 102 92, 94, 98, 85, 96, 112, 114, 100 110, 85, 90, 121, 92, 102, 96, 94 98, 94, 110, 92, 88, 79, 98, 106 83, 77, 100, 104, 83, 86, 88, 92 100, 85, 100, 90, 112, 85, 100, 112 94, 94, 106, 92, 83, 92, 108, 98 85, 90, 90, 86, 96, 92, 83, 92 100, 110, 108, 88, 96, 104, 104, 104 90, 64, 108, 98, 86, 106, 92, 117 104, 92, 98, 94, 102, 92, 81, 100 98, 88, 98, 98, 98, 96, 104, 96 110, 119, 94, 112, 102, 81, 83, 90 96, 88, 100, 92, 96, 96, 110, 85 85, 114, 98, 104, 100, 104, 76, 96 100, 100, 110, 96, 86, 88, 92, 110 100, 96, 98, 85, 98, 92, 102, 106 102, 102, 110, 106, 112, 90, 106, 92 85, 104, 88, 94, 90, 100, 117, 98 85, 117, 110, 102, 112, 102, 85, 117 90, 98, 112, 110, 98, 121, 98, 114 108, 100, 130, 83, 86, 102, 108, 96 110, 117, 86, 100, 100, 98, 90, 110 110, 85, 92, 83, 85, 98, 96, 110 96, 98, 81, 88, 88, 96, 104, 104 100, 90, 85, 121, 79, 112, 100, 94 117, 85, 90, 106, 94, 98, 98, 108 77, 96, 94, 86, 106, 106, 92, 88 92, 96, 98, 86, 92, 98, 98, 114 108, 100, 88, 88, 117, 98, 94, 102 102, 98, 102, 100, 106, 79, 112, 90 110, 104, 90, 106, 98, 112, 88, 121 94, 92, 94, 102, 112, 85, 102, 117 100, 85, 106, 94, 96, 114, 88, 119 110, 96, 108, 94, 106, 106, 100, 119 104, 110, 132, 104, 114, 98, 112, 94 102, 94, 96, 88, 100, 94, 94, 121 104, 92, 96, 110, 102, 92, 96, 117 86, 104, 106, 121, 119, 121, 98, 102 100, 94, 98, 117, 114, 110, 110, 128 110, 142, 106, 96, 104, 119, 119, 108 100, 108, 100, 106, 108, 112, 90, 110 121, 102, 128, 96, 100, 100, 119, 117 108, 119, 114, 106, 125, 123, 123, 96 117, 123, 102, 96, 130, 108, 128, 130 117, 135, 112, 117, 132, 117, 125, 130 100, 135, 128, 139, 151, 112, 106, 114 142, 137, 121, 137, 142, 137, 128, 137 114, 128, 159, 132, 135, 149, 132, 164 144, 161, 154, 172, 156, 169, 174, 185 190, 174, 213, 202, 213, 185, 219, 180 159, 190, 204, 193, 180, 185, 180, 177 182, 151, 130, 151, 154, 132, 164, 130 142, 135, 125, 164, 144, 130, 142, 137 159, 132, 121, 149, 139, 121, 128, 110 119, 144, 110, 117, 144, 142, 112, 135 130, 135, 117, 130, 142, 121, 135, 123 137, 130, 132, 128, 130, 104, 135, 139 121, 112, 130, 121, 112, 130, 132, 146 130, 112, 130, 137, 144, 121, 151, 125 121, 125, 121, 121, 114, 112, 130, 132 117, 119, 130, 132, 144, 130, 132, 125 130, 117, 112, 132, 132, 123, 128, 128 139, 130, 132, 119, 142, 135, 144, 132 135, 156, 137, 130, 135, 123, 142, 149 139, 154, 146, 137, 128, 106, 135, 128 137, 117, 149, 106, 123, 110, 114, 130 135, 104, 128, 114, 128, 114, 125, 119 123, 121, 108, 110, 110, 128, 114, 132 110, 123, 117, 119, 114, 130, 117, 130 135, 110, 125, 130, 144, 130, 119, 121 137, 123, 130, 139, 151, 130, 151, 149 125, 130, 125, 142, 132, 154, 137, 125 130, 149, 144, 123, 137, 144, 151, 144 146, 132, 146, 137, 139, 166, 139, 164 169, 146, 139, 185, 149, 172, 149, 146 146, 161, 166, 161, 161, 156, 172, 180 146, 174, 174, 174, 166, 149, 146, 154 180, 135, 174, 146, 164, 154, 139, 169 151, 166, 159, 151, 169, 139, 137, 146 172, 144, 149, 149, 164, 142, 154, 149 156, 156, 137, 154, 185, 139, 154, 161 174, 164, 149, 156, 159, 169, 146, 139 149, 161, 172, 159, 151, 139, 151, 121 144, 159, 117, 149, 156, 149, 151, 159 172, 151, 139, 146, 144, 174, 151, 164 156, 161, 137, 151, 149, 146, 149, 180 164, 125, 174, 169, 169, 172, 169, 161 182, 174, 156, 182, 182, 166, 213, 204 196, 213, 219, 276, 328, 292, 292, 324 272, 269, 256, 266, 250, 202, 182, 180 207, 154, 159, 177, 144, 177, 177, 185 164, 177, 151, 164, 149, 166, 166, 154 166, 190, 149, 159, 149, 159, 156, 188 166, 164, 180, 154, 180, 174, 159, 161 166, 156, 164, 185, 177, 159, 169, 164 161, 154, 174, 182, 144, 172, 169, 164 154, 182, 177, 190, 161, 154, 146, 154 169, 161, 174, 139, 182, 164, 154, 159 169, 139, 159, 180, 161, 169, 151, 180 169, 159, 137, 144, 146, 144, 172, 149 185, 154, 164, 154, 154, 172, 169, 159 169, 174, 164, 174, 149, 164, 182, 169 164, 172, 172, 156, 161, 156, 154, 177 154, 180, 159, 177, 185, 149, 159, 164 182, 177, 169, 182, 164, 156, 166, 146 135, 161, 166, 161, 185, 149, 164, 161 164, 159, 159, 174, 159, 177, 174, 177 177, 169, 156, 174, 169, 177, 169, 161 185, 185, 169, 161, 149, 182, 154, 180 180, 156, 166, 185, 174, 188, 166, 172 193, 166, 164, 164, 177, 193, 151, 161 188, 169, 169, 142, 174, 172, 169, 177 159, 177, 156, 166, 149, 182, 149, 177 174, 182, 161, 169, 166, 174, 193, 156 196, 177, 172, 177, 193, 169, 182, 185 166, 213, 228, 222, 190, 225, 276, 256 237, 243, 253, 262, 276, 256, 246, 240 231, 231, 234, 185, 180, 177, 219, 169 207, 182, 190, 193, 182, 182, 193, 174 196, 177, 161, 169, 180, 166, 159, 185 202, 190, 161, 193, 166, 182, 188, 177 188, 182, 185, 190, 177, 193, 177, 207 202, 199, 193, 213, 204, 182, 188, 193 164, 207, 216, 185, 199, 216, 188, 164 193, 169, 182, 182, 199, 180, 174, 182 188, 202, 188, 174, 177, 196, 188, 182 199, 210, 207, 172, 188, 196, 199, 185 193, 193, 174, 188, 180, 196, 164, 188 180, 177, 207, 199, 199, 199, 185, 196 180, 185, 216, 196, 188, 202, 199, 196 210, 174, 204, 216, 216, 193, 204, 193 225, 237, 193, 213, 222, 219, 216, 213 202, 207, 193, 222, 219, 210, 243, 182 210, 231, 210, 222, 216, 196, 210, 207 234, 182, 216, 210, 231, 213, 202, 193 213, 243, 213, 228, 234, 253, 250, 246 276, 266, 246, 276, 216, 269, 276, 282 262, 286, 292, 313, 317, 320, 289, 292 339, 276, 372, 392, 372, 384, 369, 396 346, 388, 369, 396, 320, 342, 346, 353 320, 339, 324, 342, 299, 289, 299, 342 317, 292, 310, 286, 279, 276, 296, 296 286, 292, 289, 296, 306, 286, 306, 286 279, 306, 262, 269, 296, 246, 286, 259 250, 256, 253, 266, 246, 222, 222, 246 231, 266, 246, 231, 228, 234, 225, 262 259, 237, 216, 210, 253, 204, 231, 259 225, 234, 190, 231, 228, 222, 219, 225 262, 222, 237, 259, 204, 210, 243, 225 222, 228, 199, 219, 219, 213, 207, 240 240, 207, 207, 243, 243, 225, 207, 219 210, 231, 196, 188, 228, 196, 219, 193 225, 240, 219, 219, 222, 234, 213, 231 210, 202, 222, 222, 243, 222, 190, 225 237, 210, 246, 202, 216, 231, 199, 228 228, 234, 243, 207, 222, 216, 213, 207 253, 231, 228, 243, 210, 213, 256, 234 210, 246, 266, 276, 231, 262, 256, 276 256, 289, 279, 292, 306, 292, 299, 296 286, 289, 303, 310, 357, 416, 380, 404 471, 538, 610, 666, 790, 906, 894, 961 992, 949, 894, 876, 807, 740, 724, 708 635, 562, 576, 493, 534, 420, 433, 396 408, 400, 388, 388, 380, 365, 320, 303 331, 306, 324, 328, 282, 310, 269, 299 303, 282, 240, 246, 286, 269, 266, 259 282, 246, 269, 276, 279, 276, 243, 219 246, 246, 256, 250, 246, 225, 237, 266 246, 253, 253, 231, 269, 243, 240, 250 222, 259, 259, 259, 246, 213, 276, 272 259, 256, 262, 262, 259, 256, 299, 310 266, 289, 282, 292, 279, 292, 292, 262 259, 259, 266, 272, 243, 253, 246, 272 228, 246, 253, 231, 234, 234, 228, 228 253, 231, 262, 250, 259, 276, 253, 250 250, 272, 256, 246, 243, 240, 246, 296 262, 272, 231, 272, 279, 266, 272, 292 256, 306, 289, 296, 289, 282, 276, 243 246, 225, 240, 250, 237, 210, 282, 210 243, 250, 228, 219, 204, 228, 253, 219 216, 219, 225, 246, 213, 210, 210, 231 177, 219, 199, 204, 237, 210, 213, 250 193, 222, 234, 225, 243, 237, 207, 243 216, 216, 210, 210, 196, 193, 219, 188 225, 222, 219, 234, 182, 225, 219, 182 188, 225, 207, 207, 213, 213, 204, 202 216, 222, 199, 202, 202, 213, 213, 207 207, 177, 182, 204, 222, 193, 240, 190 216, 196, 196, 185, 207, 202, 219, 216 207, 202, 228, 210, 193, 204, 216, 231 213, 196, 204, 199, 219, 210, 222, 246 219, 256, 237, 202, 204, 225, 234, 210 243, 228, 253, 243, 240, 246, 240, 266 250, 279, 256, 276, 292, 353, 346, 369 380, 404, 441, 524, 640, 697, 812, 882 1089, 1183, 1362, 1444, 1521, 1406, 1260, 1239 1211, 1102, 1063, 955, 930, 824, 734, 581 511, 441, 350, 361, 276, 303, 272, 276 231, 243, 225, 253, 216, 253, 256, 234 202, 196, 207, 216, 193, 202, 177, 213 196, 222, 243, 225, 193, 222, 188, 202 196, 202, 216, 216, 207, 219, 210, 204 231, 193, 190, 199, 204, 228, 190, 196 222, 210, 196, 188, 185, 174, 219,/