SampleIdent,925D 28H5 37-39clay,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-mar-1994 15:23,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 174, 161, 159, 174, 159, 149, 164, 161 149, 185, 149, 154, 144, 174, 137, 149 137, 144, 151, 144, 151, 139, 144, 135 144, 146, 159, 164, 161, 154, 164, 139 128, 130, 137, 123, 139, 146, 149, 123 144, 151, 154, 161, 137, 123, 121, 154 146, 123, 130, 108, 112, 151, 128, 161 121, 130, 137, 137, 132, 139, 88, 154 112, 121, 119, 117, 135, 137, 119, 144 135, 130, 121, 130, 137, 119, 128, 139 117, 135, 123, 123, 130, 139, 121, 117 108, 104, 130, 130, 139, 125, 112, 130 94, 137, 128, 130, 121, 102, 117, 110 114, 121, 117, 117, 114, 135, 100, 114 108, 121, 104, 98, 119, 121, 128, 119 123, 114, 135, 130, 117, 125, 112, 123 128, 112, 130, 112, 130, 121, 94, 108 110, 119, 137, 100, 130, 102, 110, 106 94, 106, 119, 108, 117, 121, 114, 112 114, 104, 102, 108, 114, 102, 121, 114 128, 104, 100, 128, 112, 112, 121, 104 110, 112, 96, 102, 130, 92, 100, 130 112, 117, 135, 102, 121, 108, 117, 137 121, 142, 112, 104, 110, 119, 123, 106 128, 104, 119, 114, 123, 121, 119, 104 106, 108, 96, 114, 130, 154, 128, 104 119, 119, 144, 119, 119, 119, 121, 125 125, 130, 114, 104, 92, 104, 117, 132 132, 132, 117, 144, 119, 94, 108, 128 123, 119, 102, 132, 110, 119, 128, 119 102, 104, 123, 119, 110, 125, 106, 123 125, 112, 128, 135, 121, 100, 104, 130 121, 110, 121, 117, 110, 121, 123, 106 121, 132, 119, 117, 114, 125, 112, 108 135, 110, 128, 123, 128, 135, 128, 106 128, 137, 121, 119, 121, 137, 123, 112 106, 137, 125, 137, 119, 132, 98, 125 125, 123, 137, 123, 132, 135, 132, 112 125, 125, 106, 137, 125, 137, 139, 135 137, 132, 121, 159, 125, 132, 110, 137 139, 130, 132, 114, 128, 137, 144, 137 135, 121, 144, 102, 144, 130, 121, 123 149, 121, 135, 112, 128, 135, 137, 144 142, 108, 151, 106, 137, 144, 159, 135 137, 137, 159, 132, 128, 123, 128, 125 121, 137, 130, 121, 123, 156, 144, 146 144, 149, 146, 119, 137, 139, 151, 125 139, 121, 161, 130, 128, 117, 146, 137 144, 135, 142, 154, 149, 146, 149, 139 130, 117, 149, 123, 137, 125, 123, 154 149, 161, 149, 142, 137, 149, 142, 137 151, 139, 159, 144, 149, 139, 132, 130 139, 123, 146, 139, 135, 142, 164, 156 142, 135, 149, 128, 121, 149, 130, 139 135, 159, 142, 144, 156, 139, 154, 146 139, 132, 137, 123, 144, 144, 123, 144 142, 110, 149, 135, 130, 156, 146, 137 128, 135, 139, 144, 123, 139, 144, 114 128, 149, 135, 154, 146, 142, 125, 130 130, 137, 130, 121, 139, 139, 146, 130 149, 130, 139, 110, 159, 114, 154, 125 135, 137, 130, 128, 142, 132, 125, 137 135, 125, 142, 125, 137, 121, 119, 110 142, 128, 130, 117, 139, 139, 132, 119 128, 135, 112, 121, 121, 128, 142, 146 125, 144, 130, 123, 128, 144, 135, 130 119, 137, 125, 121, 130, 132, 130, 139 117, 135, 119, 125, 121, 119, 128, 104 135, 142, 102, 108, 142, 135, 117, 108 130, 135, 123, 130, 125, 123, 130, 146 114, 123, 128, 132, 117, 112, 121, 132 137, 137, 139, 135, 110, 137, 128, 144 139, 154, 130, 128, 123, 132, 132, 128 123, 130, 139, 135, 137, 142, 112, 108 156, 128, 135, 114, 128, 132, 149, 123 102, 128, 123, 125, 130, 130, 121, 132 130, 123, 142, 130, 130, 121, 139, 128 144, 119, 117, 130, 132, 146, 135, 137 125, 149, 142, 139, 144, 137, 139, 149 125, 135, 137, 125, 130, 132, 104, 156 123, 139, 137, 123, 146, 139, 151, 125 142, 149, 125, 159, 151, 161, 161, 159 128, 144, 149, 146, 169, 154, 144, 177 123, 146, 161, 146, 137, 139, 154, 130 164, 144, 151, 166, 159, 154, 156, 149 159, 151, 132, 156, 149, 144, 142, 142 149, 149, 149, 159, 159, 142, 139, 132 144, 139, 151, 106, 139, 144, 135, 132 144, 135, 128, 130, 123, 117, 125, 117 130, 142, 144, 137, 119, 161, 142, 142 137, 117, 130, 121, 117, 112, 135, 132 137, 132, 108, 132, 117, 125, 108, 123 125, 132, 135, 90, 119, 130, 135, 139 117, 123, 119, 104, 108, 112, 123, 119 106, 132, 125, 132, 132, 108, 121, 121 121, 108, 114, 110, 117, 110, 98, 96 106, 108, 121, 100, 123, 117, 114, 117 114, 117, 123, 106, 119, 121, 117, 117 114, 121, 100, 100, 104, 125, 123, 117 96, 121, 100, 108, 108, 128, 98, 117 112, 88, 125, 117, 121, 123, 112, 119 114, 98, 102, 92, 96, 108, 98, 104 121, 135, 104, 108, 106, 130, 110, 104 117, 114, 114, 110, 108, 112, 108, 102 94, 110, 114, 110, 94, 110, 123, 108 117, 102, 137, 104, 110, 94, 100, 96 98, 102, 121, 102, 90, 112, 81, 108 104, 104, 130, 121, 106, 94, 114, 108 98, 98, 117, 114, 108, 121, 114, 119 102, 106, 112, 110, 112, 88, 102, 121 130, 100, 104, 104, 119, 117, 108, 114 114, 117, 119, 102, 102, 100, 108, 104 112, 106, 106, 110, 121, 123, 114, 108 114, 128, 106, 100, 106, 112, 100, 112 110, 117, 104, 108, 104, 112, 119, 125 130, 106, 108, 119, 117, 125, 106, 104 114, 110, 108, 121, 137, 106, 106, 117 110, 119, 121, 112, 125, 123, 128, 119 98, 130, 128, 128, 151, 123, 132, 125 112, 117, 132, 121, 137, 144, 142, 149 137, 125, 121, 144, 128, 119, 144, 149 139, 119, 128, 135, 130, 149, 154, 149 164, 156, 166, 169, 156, 149, 144, 169 159, 166, 182, 180, 177, 172, 174, 164 202, 196, 222, 196, 190, 225, 246, 216 225, 216, 219, 237, 256, 256, 272, 272 320, 253, 246, 317, 320, 306, 324, 365 380, 350, 392, 412, 392, 404, 428, 484 449, 458, 449, 441, 467, 396, 467, 471 437, 428, 433, 471, 437, 437, 424, 408 408, 369, 372, 392, 353, 331, 342, 339 310, 296, 282, 279, 253, 234, 250, 204 190, 213, 228, 174, 196, 177, 180, 177 159, 177, 174, 139, 164, 164, 149, 137 156, 128, 139, 135, 151, 125, 121, 123 139, 144, 139, 114, 132, 121, 112, 110 119, 114, 106, 117, 92, 104, 119, 108 108, 121, 98, 100, 108, 102, 106, 102 112, 94, 98, 83, 102, 90, 86, 117 104, 76, 117, 98, 100, 86, 100, 108 86, 114, 86, 96, 96, 104, 110, 102 92, 85, 96, 85, 86, 104, 81, 108 83, 102, 88, 117, 104, 98, 71, 85 104, 94, 96, 100, 85, 104, 102, 86 90, 96, 108, 90, 96, 102, 102, 90 106, 104, 108, 86, 94, 83, 110, 86 98, 86, 92, 88, 110, 94, 81, 106 102, 119, 88, 94, 90, 110, 102, 72 96, 92, 100, 96, 96, 106, 112, 90 98, 83, 100, 104, 90, 79, 85, 86 74, 86, 76, 81, 79, 85, 85, 86 81, 92, 69, 90, 72, 72, 85, 86 102, 86, 74, 86, 76, 85, 90, 88 83, 96, 81, 98, 86, 67, 88, 96 88, 77, 85, 98, 83, 76, 96, 94 94, 83, 83, 83, 74, 90, 85, 83 86, 86, 83, 85, 90, 83, 77, 83 85, 85, 85, 94, 92, 83, 81, 81 90, 77, 86, 86, 86, 71, 88, 83 90, 81, 79, 79, 85, 86, 81, 76 71, 102, 86, 76, 79, 100, 86, 92 77, 86, 72, 83, 83, 106, 88, 92 85, 79, 85, 77, 94, 88, 86, 74 77, 81, 83, 86, 76, 85, 88, 88 83, 83, 92, 83, 83, 90, 94, 92 76, 67, 77, 100, 86, 85, 86, 94 76, 72, 77, 92, 100, 69, 85, 94 96, 92, 85, 88, 98, 79, 88, 83 106, 77, 81, 76, 90, 88, 88, 83 76, 86, 96, 81, 90, 94, 88, 92 85, 85, 94, 88, 94, 88, 77, 79 85, 98, 81, 110, 85, 100, 102, 83 94, 72, 100, 104, 96, 79, 81, 100 76, 90, 67, 71, 96, 112, 90, 83 102, 92, 67, 77, 83, 85, 85, 92 76, 81, 94, 98, 77, 90, 96, 79 83, 92, 74, 86, 106, 104, 92, 83 76, 77, 96, 94, 92, 79, 96, 102 104, 76, 108, 85, 88, 100, 92, 88 92, 96, 79, 83, 100, 83, 104, 96 100, 86, 85, 94, 98, 83, 88, 92 81, 83, 94, 81, 81, 96, 90, 94 96, 94, 96, 88, 81, 92, 86, 88 94, 90, 83, 92, 79, 102, 85, 72 92, 98, 96, 92, 92, 92, 88, 96 77, 76, 100, 102, 98, 104, 83, 117 86, 88, 85, 85, 96, 88, 100, 85 110, 98, 94, 90, 96, 90, 92, 85 90, 81, 102, 90, 98, 94, 74, 79 83, 94, 98, 96, 85, 106, 92, 110 96, 96, 98, 86, 104, 98, 102, 102 83, 72, 102, 117, 85, 96, 85, 112 98, 77, 98, 114, 98, 86, 90, 114 98, 92, 108, 100, 96, 110, 106, 100 100, 112, 100, 108, 104, 98, 88, 102 125, 110, 135, 108, 125, 106, 114, 121 130, 102, 102, 110, 130, 117, 121, 117 112, 114, 117, 117, 121, 108, 96, 112 110, 123, 98, 117, 123, 106, 110, 108 121, 108, 94, 125, 88, 121, 96, 85 100, 102, 98, 85, 90, 100, 92, 102 100, 98, 106, 88, 86, 98, 119, 100 86, 90, 86, 110, 96, 119, 104, 108 112, 85, 94, 110, 79, 108, 100, 112 108, 110, 100, 100, 112, 96, 100, 92 114, 92, 88, 85, 104, 121, 102, 98 90, 74, 90, 102, 104, 94, 90, 96 121, 94, 83, 108, 110, 90, 79, 71 85, 96, 88, 92, 71, 92, 98, 83 88, 92, 104, 100, 96, 98, 106, 83 94, 96, 85, 98, 112, 96, 114, 96 77, 96, 106, 94, 102, 86, 98, 94 102, 104, 77, 79, 76, 106, 100, 90 94, 86, 83, 94, 88, 94, 98, 100 100, 88, 96, 98, 85, 96, 83, 96 90, 96, 90, 90, 94, 92, 104, 92 96, 100, 119, 112, 104, 90, 98, 100 102, 110, 92, 112, 94, 94, 94, 100 96, 112, 96, 110, 85, 114, 104, 96 119, 106, 98, 132, 108, 119, 112, 123 108, 117, 123, 114, 144, 128, 128, 144 96, 135, 156, 132, 159, 142, 161, 151 161, 159, 139, 151, 123, 149, 161, 132 144, 151, 172, 151, 159, 142, 149, 159 149, 156, 169, 154, 169, 159, 146, 146 169, 164, 137, 149, 137, 174, 144, 146 137, 154, 128, 161, 139, 125, 132, 139 144, 154, 130, 146, 135, 151, 139, 146 137, 144, 119, 139, 128, 154, 119, 125 132, 130, 137, 151, 135, 161, 139, 135 132, 144, 137, 146, 149, 149, 144, 130 144, 130, 142, 144, 130, 137, 114, 128 149, 164, 144, 146, 130, 130, 144, 151 137, 151, 156, 151, 159, 172, 182, 182 185, 182, 213, 207, 228, 240, 234, 243 246, 246, 253, 246, 253, 240, 237, 253 243, 292, 234, 240, 259, 272, 262, 240 243, 213, 207, 219, 202, 166, 177, 182 159, 177, 185, 151, 169, 182, 159, 164 159, 161, 172, 161, 164, 164, 174, 188 172, 149, 172, 196, 169, 193, 159, 161 164, 159, 172, 188, 185, 166, 182, 182 174, 185, 169, 174, 172, 156, 144, 172 159, 182, 164, 164, 154, 137, 161, 149 139, 161, 137, 154, 137, 146, 169, 149 137, 132, 154, 144, 137, 154, 125, 154 125, 151, 144, 144, 154, 142, 151, 151 159, 119, 164, 144, 169, 121, 164, 144 144, 125, 119, 144, 114, 151, 132, 130 135, 137, 128, 146, 154, 144, 159, 161 137, 144, 149, 125, 154, 139, 130, 135 154, 146, 144, 144, 123, 154, 154, 130 146, 130, 130, 137, 137, 146, 123, 130 142, 108, 137, 119, 123, 142, 142, 137 132, 135, 154, 146, 137, 137, 159, 169 135, 130, 149, 132, 135, 128, 142, 144 130, 130, 154, 169, 149, 149, 149, 139 121, 144, 121, 112, 144, 142, 149, 139 119, 139, 128, 139, 151, 123, 142, 128 119, 151, 142, 142, 137, 144, 149, 128 135, 144, 149, 161, 169, 154, 139, 156 144, 132, 142, 137, 137, 130, 151, 135 154, 149, 114, 149, 146, 144, 137, 159 161, 132, 119, 137, 156, 130, 164, 125 146, 139, 137, 149, 144, 149, 146, 125 135, 144, 137, 144, 132, 142, 139, 130 137, 139, 137, 137, 139, 142, 130, 128 151, 135, 130, 156, 137, 154, 121, 144 151, 149, 164, 146, 144, 149, 154, 154 128, 151, 149, 177, 139, 164, 128, 144 156, 169, 164, 161, 156, 164, 174, 132 144, 156, 174, 159, 149, 154, 169, 154 151, 169, 151, 159, 154, 151, 146, 149 146, 151, 159, 149, 172, 174, 164, 149 151, 161, 166, 161, 172, 164, 159, 169 177, 174, 166, 172, 174, 193, 185, 174 164, 174, 182, 169, 166, 199, 174, 219 199, 196, 177, 169, 190, 204, 185, 199 210, 216, 193, 177, 210, 234, 219, 213 199, 213, 237, 225, 225, 202, 210, 228 231, 262, 243, 246, 228, 256, 246, 276 253, 303, 292, 286, 292, 306, 306, 286 320, 357, 350, 400, 400, 412, 428, 449 441, 462, 475, 454, 529, 566, 562, 605 620, 630, 718, 655, 697, 729, 784, 767 790, 795, 912, 858, 870, 876, 930, 918 924, 900, 949, 924, 912, 858, 864, 841 876, 762, 778, 745, 713, 697, 697, 671 635, 610, 586, 586, 576, 538, 497, 484 493, 471, 506, 458, 412, 445, 445, 400 416, 416, 384, 404, 392, 376, 365, 388 365, 353, 404, 372, 357, 339, 335, 346 335, 266, 342, 306, 272, 324, 306, 310 306, 299, 279, 292, 289, 303, 253, 272 286, 266, 272, 269, 269, 253, 253, 250 266, 253, 276, 253, 286, 276, 237, 250 253, 253, 253, 250, 262, 253, 246, 240 234, 246, 276, 240, 243, 256, 256, 210 250, 228, 243, 237, 246, 246, 246, 262 234, 246, 262, 240, 256, 246, 240, 250 250, 276, 225, 243, 253, 262, 228, 237 243, 259, 240, 279, 266, 250, 279, 266 243, 246, 269, 272, 299, 276, 266, 262 276, 296, 320, 279, 324, 276, 303, 292 299, 310, 299, 324, 310, 279, 331, 320 350, 353, 392, 408, 380, 449, 428, 467 488, 534, 543, 571, 666, 640, 708, 790 801, 778, 824, 847, 853, 967, 986, 924 930, 949, 961, 1011, 1082, 1030, 986, 1056 924, 949, 882, 829, 740, 734, 615, 635 576, 471, 538, 462, 424, 437, 420, 342 365, 342, 346, 328, 320, 320, 324, 303 303, 306, 320, 286, 289, 296, 256, 269 310, 216, 289, 262, 256, 276, 253, 250 276, 231, 256, 256, 266, 219, 231, 253 253, 234, 222, 228, 219, 228, 228, 246 225, 219, 246, 213, 222, 237, 253, 222 225, 228, 256, 225, 256, 237, 243, 237 243, 216, 250, 259, 269, 240, 253, 243 262, 262, 228, 234, 240, 207, 202, 228 213, 219, 237, 253, 180, 199, 219, 204 207, 216, 225, 193, 219, 196, 190, 204 216, 204, 199, 190, 216, 210, 228, 196 207, 234, 188, 210, 193, 219, 228, 210 213, 213, 190, 213, 210, 193, 193, 213 199, 213, 219, 219, 193, 199, 199, 185 202, 142, 177, 185, 161, 169, 154, 174 146, 149, 169, 180, 159, 174, 149, 166 144, 166, 172, 207, 159, 142, 154, 151 161, 151, 161, 132, 164, 144, 142, 161 137, 142, 190, 144, 169, 125, 135, 161 142, 156, 180, 142, 130, 156, 151, 164 161, 159, 146, 139, 144, 139, 149, 149 146, 142, 151, 142, 159, 159, 149, 123 156, 128, 149, 130, 144, 149, 144, 137 132, 121, 137, 154, 146, 139, 172, 130 130, 119, 125, 149, 137, 144, 121, 123 144, 108, 154, 130, 139, 151, 149, 119 110, 137, 135, 132, 128, 149, 135, 146 123, 146, 144, 144, 151, 121, 156, 154 142, 128, 154, 146, 139, 139, 142, 144 142, 149, 146, 128, 137, 132, 142, 144 139, 132, 174, 149, 135, 132, 151, 166 125, 130, 130, 159, 125, 161, 139, 159 164, 154, 149, 135, 164, 137, 125, 154 151, 135, 146, 149, 146, 137, 137, 144 142, 144, 132, 149, 149, 159, 164, 154 154, 159, 159, 144, 154, 159, 182, 149 164, 151, 166, 166, 146, 166, 139, 159 174, 144, 169, 164, 159, 169, 154,/