SampleIdent,925D 28H5 37-39gly,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,10-mar-1994 13:27,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 182, 180, 159, 146, 154, 169, 151, 174 161, 149, 128, 142, 172, 161, 154, 154 159, 177, 156, 172, 139, 156, 164, 130 169, 151, 164, 149, 132, 159, 149, 177 142, 156, 125, 142, 144, 154, 123, 137 132, 121, 139, 146, 172, 137, 132, 130 135, 117, 130, 144, 132, 156, 146, 128 137, 121, 135, 130, 125, 130, 135, 135 142, 132, 114, 132, 132, 121, 114, 117 132, 108, 119, 137, 154, 121, 142, 139 123, 128, 114, 137, 130, 110, 132, 106 123, 112, 123, 117, 132, 125, 112, 108 144, 121, 94, 121, 119, 119, 135, 123 121, 132, 114, 130, 112, 112, 123, 119 100, 100, 117, 104, 108, 104, 128, 121 123, 117, 108, 102, 96, 104, 123, 108 119, 121, 96, 112, 119, 146, 104, 114 119, 100, 104, 119, 137, 119, 130, 98 114, 110, 106, 137, 110, 104, 114, 125 110, 102, 123, 108, 121, 110, 104, 117 121, 117, 125, 112, 121, 130, 114, 117 108, 112, 102, 114, 108, 125, 119, 117 137, 110, 121, 137, 123, 106, 123, 128 114, 108, 119, 112, 112, 128, 137, 100 114, 108, 123, 112, 117, 106, 130, 108 125, 119, 102, 117, 96, 98, 132, 96 119, 117, 128, 117, 106, 123, 104, 117 119, 135, 110, 108, 130, 146, 132, 100 128, 106, 144, 119, 96, 128, 128, 94 156, 132, 112, 135, 98, 104, 110, 119 114, 121, 114, 112, 132, 119, 128, 125 121, 110, 125, 130, 100, 119, 130, 102 139, 121, 137, 117, 132, 125, 119, 135 125, 121, 108, 104, 137, 130, 130, 117 117, 119, 114, 137, 121, 149, 130, 112 156, 102, 119, 121, 125, 132, 137, 144 132, 132, 123, 121, 123, 125, 142, 137 132, 128, 132, 123, 121, 132, 144, 142 106, 125, 146, 125, 149, 137, 146, 121 142, 130, 137, 112, 169, 146, 123, 144 159, 144, 139, 112, 146, 146, 112, 121 117, 128, 149, 139, 114, 128, 156, 137 142, 146, 142, 146, 137, 146, 142, 128 144, 137, 159, 154, 117, 151, 114, 137 156, 125, 132, 135, 121, 144, 151, 146 119, 128, 125, 142, 142, 142, 125, 130 146, 149, 123, 128, 169, 135, 128, 121 132, 154, 137, 146, 137, 125, 144, 146 117, 139, 144, 144, 130, 130, 139, 137 149, 137, 137, 142, 149, 154, 121, 144 137, 149, 144, 137, 144, 128, 149, 139 144, 125, 142, 130, 156, 123, 139, 121 112, 130, 137, 177, 121, 130, 128, 128 149, 142, 144, 149, 121, 149, 114, 149 135, 154, 135, 139, 161, 121, 146, 137 154, 132, 139, 159, 121, 137, 149, 142 112, 166, 137, 137, 146, 169, 149, 144 117, 142, 144, 132, 144, 146, 128, 119 117, 137, 123, 132, 144, 121, 128, 146 149, 108, 137, 144, 139, 142, 159, 144 130, 142, 154, 164, 112, 151, 132, 114 139, 121, 159, 125, 130, 149, 114, 130 132, 128, 132, 144, 142, 137, 119, 123 117, 144, 132, 130, 112, 128, 112, 121 132, 119, 151, 130, 149, 125, 137, 119 125, 110, 117, 142, 142, 132, 119, 132 117, 132, 112, 128, 110, 130, 117, 137 130, 125, 125, 114, 128, 123, 117, 125 132, 139, 108, 146, 142, 132, 137, 119 135, 128, 130, 144, 137, 98, 128, 125 137, 125, 135, 130, 121, 123, 123, 128 119, 121, 130, 121, 119, 114, 144, 135 142, 130, 119, 117, 132, 125, 144, 121 112, 117, 135, 114, 130, 114, 137, 142 108, 132, 119, 135, 142, 137, 125, 121 149, 117, 123, 128, 123, 121, 132, 137 108, 112, 132, 144, 139, 135, 125, 121 117, 121, 137, 128, 149, 139, 135, 132 132, 135, 137, 130, 110, 161, 132, 149 137, 151, 128, 137, 149, 114, 135, 149 132, 137, 146, 130, 130, 159, 154, 154 137, 132, 154, 139, 149, 137, 112, 154 132, 151, 154, 149, 137, 166, 156, 128 139, 139, 156, 169, 156, 172, 174, 144 144, 137, 159, 169, 164, 132, 177, 146 144, 144, 144, 164, 144, 144, 154, 132 128, 149, 166, 159, 149, 151, 139, 114 154, 144, 169, 132, 135, 149, 151, 142 139, 144, 139, 135, 130, 119, 149, 125 108, 137, 146, 135, 121, 128, 125, 135 119, 123, 121, 149, 139, 123, 108, 117 123, 119, 130, 125, 130, 123, 106, 104 139, 110, 121, 114, 139, 128, 106, 123 110, 128, 98, 106, 132, 102, 137, 128 108, 128, 106, 110, 96, 114, 125, 128 102, 114, 135, 102, 110, 130, 121, 112 110, 108, 100, 119, 100, 110, 137, 123 123, 130, 132, 110, 135, 100, 125, 117 106, 121, 130, 106, 128, 121, 125, 117 110, 117, 100, 96, 132, 112, 88, 112 128, 98, 106, 96, 117, 108, 119, 96 102, 110, 106, 117, 121, 130, 117, 92 108, 114, 130, 121, 102, 125, 110, 125 112, 102, 132, 100, 112, 96, 117, 108 102, 104, 110, 121, 114, 102, 96, 121 96, 117, 102, 92, 119, 96, 106, 114 106, 135, 119, 130, 102, 121, 110, 117 117, 98, 90, 96, 98, 106, 106, 102 123, 119, 104, 114, 104, 86, 96, 110 94, 114, 102, 98, 121, 112, 123, 104 108, 137, 106, 110, 100, 96, 102, 108 108, 110, 92, 125, 106, 121, 98, 106 117, 110, 119, 114, 100, 110, 96, 132 104, 104, 108, 106, 114, 117, 108, 121 90, 102, 112, 112, 130, 125, 154, 123 121, 102, 117, 130, 106, 137, 123, 123 121, 108, 123, 119, 135, 123, 121, 121 121, 117, 119, 121, 139, 139, 123, 128 110, 123, 125, 119, 117, 135, 110, 102 121, 144, 125, 149, 159, 123, 146, 130 121, 139, 132, 154, 137, 137, 144, 149 123, 149, 137, 154, 159, 144, 156, 142 161, 135, 151, 154, 146, 139, 151, 149 154, 161, 169, 185, 190, 193, 202, 182 216, 207, 204, 202, 225, 204, 222, 222 222, 225, 246, 253, 253, 228, 296, 279 279, 289, 262, 296, 313, 320, 313, 365 346, 372, 384, 376, 384, 396, 433, 420 412, 458, 488, 449, 458, 475, 520, 493 458, 471, 433, 458, 467, 400, 449, 404 412, 396, 342, 412, 372, 376, 331, 282 320, 276, 282, 299, 286, 240, 243, 231 240, 213, 196, 182, 188, 172, 172, 166 180, 144, 188, 154, 156, 156, 164, 146 135, 121, 156, 137, 132, 142, 121, 144 137, 121, 98, 123, 125, 110, 102, 114 117, 130, 108, 130, 102, 102, 121, 123 98, 100, 96, 110, 96, 106, 106, 112 94, 106, 100, 110, 102, 104, 94, 108 92, 106, 86, 90, 85, 104, 100, 94 94, 104, 100, 90, 108, 81, 112, 110 86, 92, 90, 104, 102, 92, 96, 98 96, 104, 106, 77, 98, 79, 85, 98 100, 83, 81, 90, 86, 100, 83, 92 100, 94, 114, 74, 98, 96, 88, 96 96, 100, 94, 92, 92, 85, 94, 92 96, 88, 86, 83, 83, 90, 100, 98 88, 83, 90, 72, 96, 69, 96, 85 92, 110, 90, 90, 96, 92, 92, 88 67, 92, 92, 88, 83, 85, 94, 79 94, 90, 96, 76, 81, 83, 94, 81 76, 94, 104, 85, 106, 88, 66, 77 79, 83, 85, 79, 92, 81, 81, 94 83, 98, 81, 94, 79, 86, 88, 90 79, 62, 81, 88, 85, 71, 85, 69 94, 85, 69, 76, 90, 90, 81, 74 83, 77, 64, 100, 94, 92, 92, 88 67, 74, 83, 88, 98, 92, 81, 90 90, 76, 72, 88, 94, 79, 86, 92 81, 94, 94, 81, 104, 83, 77, 71 77, 96, 108, 98, 83, 86, 94, 96 79, 79, 86, 85, 77, 88, 90, 92 67, 96, 83, 90, 77, 90, 79, 86 81, 77, 72, 76, 104, 83, 85, 88 81, 85, 94, 90, 86, 100, 69, 94 74, 90, 79, 81, 83, 85, 98, 79 76, 98, 85, 76, 86, 81, 83, 92 86, 83, 88, 86, 94, 86, 86, 92 90, 94, 104, 94, 79, 85, 76, 83 83, 77, 85, 100, 81, 83, 76, 86 86, 85, 86, 67, 79, 81, 83, 86 86, 94, 90, 94, 94, 88, 98, 85 92, 100, 90, 83, 98, 88, 98, 104 94, 98, 85, 92, 102, 94, 92, 100 88, 86, 77, 96, 88, 72, 88, 74 81, 79, 96, 74, 83, 106, 85, 100 77, 86, 81, 92, 83, 83, 90, 85 92, 85, 106, 92, 85, 79, 88, 85 92, 98, 85, 88, 94, 86, 108, 90 71, 96, 98, 85, 86, 76, 79, 96 94, 86, 88, 98, 77, 85, 94, 98 104, 86, 77, 86, 100, 88, 85, 100 102, 88, 88, 90, 85, 100, 88, 88 86, 100, 85, 94, 100, 86, 88, 100 92, 94, 83, 90, 79, 72, 96, 83 100, 104, 106, 79, 74, 94, 83, 90 94, 94, 90, 90, 96, 104, 100, 102 114, 100, 94, 102, 92, 92, 83, 86 90, 96, 88, 98, 92, 72, 85, 85 98, 112, 83, 86, 85, 106, 100, 79 94, 100, 96, 86, 85, 83, 102, 92 94, 76, 98, 104, 96, 86, 104, 100 102, 69, 86, 96, 102, 98, 114, 114 88, 106, 94, 104, 98, 108, 104, 114 96, 98, 114, 100, 106, 130, 100, 100 100, 102, 106, 117, 110, 121, 114, 110 112, 114, 123, 110, 110, 130, 121, 112 114, 130, 128, 125, 128, 112, 125, 106 96, 121, 100, 106, 128, 108, 112, 139 100, 102, 117, 106, 108, 92, 98, 96 90, 104, 110, 94, 94, 104, 88, 112 106, 90, 98, 92, 96, 100, 94, 110 121, 112, 81, 86, 88, 108, 79, 108 88, 92, 110, 106, 94, 108, 108, 108 90, 98, 90, 94, 92, 86, 92, 104 104, 86, 92, 100, 98, 88, 86, 90 96, 90, 90, 92, 108, 117, 90, 100 102, 83, 85, 110, 102, 110, 98, 92 102, 90, 98, 86, 76, 90, 79, 90 92, 83, 96, 86, 104, 98, 86, 106 92, 88, 72, 96, 88, 94, 106, 85 83, 108, 96, 117, 96, 88, 98, 79 110, 86, 112, 98, 102, 104, 92, 98 85, 94, 102, 85, 98, 69, 85, 86 86, 102, 86, 92, 92, 94, 92, 92 94, 86, 94, 100, 86, 96, 110, 85 94, 88, 88, 98, 83, 98, 106, 90 96, 88, 98, 106, 94, 90, 100, 108 94, 114, 106, 98, 114, 117, 92, 112 108, 98, 139, 110, 137, 114, 121, 98 110, 130, 121, 121, 125, 119, 130, 137 139, 114, 142, 149, 149, 132, 137, 139 139, 161, 172, 166, 172, 169, 169, 144 151, 180, 164, 159, 159, 180, 142, 166 154, 139, 161, 149, 154, 128, 166, 174 142, 149, 159, 149, 139, 154, 139, 144 139, 130, 135, 166, 144, 149, 135, 142 125, 159, 123, 139, 139, 144, 130, 137 144, 125, 125, 119, 149, 135, 151, 130 151, 137, 137, 146, 144, 146, 142, 144 123, 128, 144, 130, 139, 119, 149, 144 137, 130, 169, 144, 123, 128, 146, 137 156, 142, 149, 146, 144, 144, 132, 164 159, 169, 154, 137, 161, 159, 188, 202 207, 207, 228, 204, 237, 256, 213, 237 246, 237, 216, 262, 246, 231, 246, 253 219, 250, 250, 250, 225, 246, 250, 231 219, 204, 228, 213, 199, 188, 190, 159 169, 177, 159, 166, 188, 180, 172, 144 154, 169, 188, 161, 169, 169, 182, 159 151, 156, 164, 177, 180, 154, 161, 154 196, 174, 182, 161, 154, 132, 180, 177 146, 174, 182, 185, 169, 151, 154, 161 149, 159, 151, 159, 177, 146, 180, 146 156, 159, 149, 161, 139, 156, 166, 159 149, 159, 146, 144, 125, 161, 149, 137 156, 149, 161, 159, 135, 144, 149, 159 159, 139, 159, 149, 142, 144, 123, 135 139, 121, 142, 137, 154, 137, 156, 142 151, 139, 164, 142, 144, 144, 144, 159 119, 135, 146, 139, 149, 128, 135, 154 137, 151, 139, 156, 144, 137, 114, 125 156, 144, 144, 125, 125, 132, 151, 123 149, 132, 144, 135, 149, 125, 151, 142 146, 130, 125, 125, 142, 149, 130, 151 154, 154, 149, 154, 121, 159, 139, 123 135, 135, 144, 144, 156, 159, 135, 137 130, 149, 144, 137, 144, 128, 130, 156 130, 144, 144, 121, 137, 128, 117, 154 142, 139, 161, 137, 125, 137, 128, 132 137, 156, 144, 132, 144, 130, 146, 144 151, 146, 132, 146, 121, 149, 123, 144 142, 144, 142, 164, 151, 151, 146, 130 151, 128, 151, 151, 135, 123, 123, 161 139, 164, 142, 144, 117, 144, 164, 108 154, 137, 139, 139, 154, 137, 156, 146 161, 146, 154, 128, 156, 154, 142, 154 132, 142, 154, 149, 149, 172, 132, 149 154, 166, 149, 159, 159, 159, 139, 164 151, 159, 159, 154, 156, 164, 177, 156 151, 196, 154, 130, 142, 151, 172, 139 159, 144, 177, 180, 185, 159, 164, 130 151, 139, 159, 164, 144, 174, 146, 169 172, 149, 180, 188, 185, 174, 164, 177 135, 149, 164, 180, 182, 169, 169, 161 180, 182, 166, 161, 180, 182, 174, 174 190, 193, 182, 196, 177, 174, 210, 193 196, 193, 210, 204, 185, 193, 190, 231 190, 199, 216, 199, 219, 190, 213, 222 207, 240, 207, 210, 207, 234, 210, 219 234, 231, 246, 243, 231, 246, 289, 313 282, 303, 289, 289, 313, 299, 306, 357 346, 392, 365, 380, 388, 372, 388, 416 424, 484, 471, 497, 548, 557, 576, 625 566, 666, 650, 697, 724, 751, 745, 767 835, 841, 853, 778, 894, 853, 942, 930 986, 999, 961, 864, 882, 906, 924, 841 829, 784, 829, 756, 745, 713, 640, 702 671, 645, 605, 645, 562, 552, 488, 506 506, 471, 475, 437, 433, 400, 420, 458 384, 392, 365, 384, 372, 384, 357, 388 361, 346, 388, 357, 350, 365, 384, 346 339, 313, 320, 328, 324, 317, 317, 289 286, 310, 317, 282, 282, 266, 306, 289 282, 259, 262, 243, 276, 262, 262, 286 292, 243, 266, 259, 240, 276, 286, 243 276, 256, 259, 240, 266, 276, 207, 240 243, 246, 259, 228, 240, 243, 259, 243 276, 250, 222, 269, 269, 262, 240, 231 243, 246, 231, 210, 259, 240, 256, 279 225, 240, 237, 243, 250, 282, 246, 262 243, 259, 246, 286, 246, 262, 262, 282 256, 286, 262, 276, 253, 306, 282, 262 237, 276, 279, 282, 262, 292, 313, 272 286, 313, 282, 313, 296, 306, 306, 346 317, 365, 376, 376, 408, 408, 424, 449 484, 566, 543, 595, 600, 630, 729, 724 784, 824, 870, 858, 853, 882, 912, 955 986, 949, 1050, 1024, 1037, 1050, 1037, 1024 1018, 973, 894, 870, 812, 713, 650, 590 571, 524, 497, 502, 424, 428, 396, 408 372, 388, 353, 350, 317, 310, 313, 331 286, 286, 296, 259, 286, 262, 272, 279 266, 256, 246, 253, 231, 228, 253, 225 269, 237, 240, 246, 253, 228, 246, 259 222, 253, 225, 225, 202, 250, 225, 253 216, 231, 228, 253, 250, 231, 246, 253 237, 231, 207, 199, 240, 222, 225, 228 231, 259, 234, 246, 243, 213, 234, 202 222, 219, 228, 231, 237, 228, 246, 231 210, 216, 228, 243, 231, 225, 182, 216 216, 222, 213, 202, 185, 216, 199, 204 213, 196, 196, 210, 213, 216, 202, 231 199, 216, 202, 188, 196, 202, 202, 199 180, 204, 196, 182, 193, 188, 210, 199 185, 180, 169, 190, 182, 156, 161, 164 182, 188, 177, 185, 169, 164, 172, 174 161, 156, 193, 172, 159, 151, 156, 154 166, 154, 154, 144, 156, 154, 177, 154 159, 149, 161, 151, 149, 159, 144, 149 174, 151, 139, 154, 146, 159, 159, 149 144, 156, 159, 154, 159, 137, 161, 156 149, 125, 117, 137, 121, 132, 146, 139 161, 159, 154, 144, 159, 164, 146, 149 166, 130, 137, 154, 137, 154, 135, 142 142, 161, 132, 137, 144, 142, 135, 154 144, 149, 149, 128, 151, 146, 132, 130 135, 137, 142, 144, 132, 137, 146, 132 128, 164, 128, 144, 151, 142, 144, 144 137, 112, 144, 161, 161, 159, 146, 164 164, 159, 128, 123, 144, 154, 146, 159 123, 132, 144, 130, 130, 121, 142, 135 130, 121, 128, 108, 137, 142, 130, 154 146, 130, 151, 139, 146, 139, 144, 135 154, 139, 139, 146, 154, 154, 151, 137 132, 137, 142, 128, 151, 144, 159, 156 164, 151, 130, 123, 144, 172, 159, 159 174, 154, 130, 164, 149, 169, 135, 159 154, 149, 144, 149, 174, 166, 182, 151 154, 151, 154, 169, 146, 149, 156, 149 154, 149, 159, 137, 130, 130, 149, 159 146, 149, 142, 151, 161, 149, 137, 135 164, 130, 156, 142, 142, 128, 142, 112 142, 137, 156, 128, 151, 151, 146, 132 128, 149, 144, 121, 154, 130, 154, 130 137, 121, 130, 132, 114, 161, 135, 132 123, 128, 159, 144, 146, 146, 137, 142 130, 146, 146, 137, 117, 135, 125, 144 119, 151, 149, 130, 149, 123, 135, 130 119, 137, 135, 135, 132, 132, 142, 159 128, 135, 146, 151, 151, 137, 154, 146 139, 106, 139, 132, 154, 137, 149, 121 137, 154, 137, 142, 114, 146, 149, 132 135, 139, 139, 125, 121, 130, 128, 137 132, 119, 121, 137, 149, 132, 164, 137 182, 132, 135, 159, 142, 121, 139, 135 144, 161, 125, 154, 154, 123, 156, 154 128, 128, 132, 132, 137, 166, 137, 142 130, 139, 119, 137, 132, 139, 139, 146 130, 132, 144, 123, 144, 125, 125, 139 123, 159, 137, 112, 123, 125, 125, 139 117, 132, 142, 139, 151, 142, 135, 130 119, 137, 117, 128, 117, 125, 130, 130 119, 130, 161, 139, 108, 117, 130, 119 119, 139, 117, 130, 132, 144, 137, 137 130, 123, 123, 112, 125, 132, 132, 119 135, 142, 121, 117, 135, 130, 137, 123 130, 121, 135, 144, 117, 128, 114, 132 130, 130, 130, 112, 123, 132, 144, 144 125, 125, 123, 128, 135, 130, 132, 135 119, 119, 110, 137, 121, 128, 121, 117 123, 121, 121, 146, 112, 121, 119, 123 125, 130, 132, 98, 106, 110, 144, 114 108, 112, 112, 121, 130, 149, 137, 132 128, 125, 123, 130, 130, 130, 123, 117 112, 132, 121, 119, 110, 132, 144, 125 139, 119, 123, 135, 156, 132, 139, 125 104, 121, 121, 146, 121, 110, 144, 159 139, 137, 132, 177, 151, 142, 149, 149 139, 159, 144, 121, 132, 149, 174, 137 144, 108, 142, 130, 149, 166, 149, 139 146, 149, 156, 135, 142, 132, 137, 156 144, 142, 139, 146, 169, 137, 161, 130 142, 137, 149, 114, 146, 121, 142, 137 114, 121, 125, 130, 123, 125, 135, 149 130, 125, 142, 104, 110, 130, 137, 123 130, 121, 114, 128, 117, 106, 114, 94 130, 128, 112, 117, 123, 130, 102, 135 112, 117, 108, 117, 112, 104, 98, 121 121, 117, 106, 125, 106, 98, 108, 106 125, 100, 130, 121, 114, 121, 135, 110 112, 121, 114, 137, 102, 94, 110, 112 119, 110, 94, 121, 114, 121, 100, 110 154, 114, 130, 123, 130, 144, 135, 125 130, 117, 104, 123, 137, 135, 139, 128 117, 142, 130, 128, 146, 137, 144, 119 121, 128, 130, 128, 146, 137, 146, 119 135, 121, 135, 130, 159, 146, 154, 159 149, 144, 172, 151, 166, 159, 156, 161 174, 154, 156, 151, 142, 174, 156, 154 139, 142, 182, 188, 161, 169, 188, 159 182, 193, 164, 188, 185, 182, 164, 190 177, 177, 172,/