SampleIdent,926A 4H5 34-36 CLAY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,11-mar-1994 7:19,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 151, 154, 196, 169, 166, 172, 164, 166 164, 161, 172, 159, 174, 174, 135, 169 159, 149, 161, 142, 174, 156, 146, 139 164, 146, 139, 161, 161, 174, 154, 144 132, 156, 130, 161, 164, 142, 161, 146 154, 146, 125, 159, 174, 135, 154, 149 144, 137, 146, 151, 146, 121, 137, 144 137, 149, 149, 144, 139, 132, 154, 130 135, 154, 144, 130, 154, 151, 130, 135 156, 149, 130, 137, 137, 144, 159, 139 146, 154, 137, 161, 125, 135, 161, 135 146, 132, 130, 146, 156, 149, 108, 169 128, 144, 135, 154, 144, 146, 142, 166 135, 149, 156, 142, 121, 130, 132, 137 130, 146, 137, 144, 139, 149, 166, 144 125, 137, 139, 146, 156, 159, 154, 130 149, 149, 149, 144, 128, 166, 139, 156 151, 135, 130, 149, 144, 161, 137, 146 144, 159, 169, 125, 159, 137, 139, 146 149, 117, 135, 130, 169, 159, 146, 151 139, 164, 130, 137, 137, 159, 144, 149 164, 164, 139, 137, 149, 154, 137, 142 169, 156, 142, 161, 164, 142, 174, 159 144, 144, 151, 144, 135, 159, 151, 156 139, 146, 156, 119, 154, 159, 132, 135 159, 144, 144, 146, 142, 172, 180, 146 182, 125, 159, 130, 135, 151, 146, 159 182, 135, 164, 174, 149, 151, 146, 137 164, 164, 132, 159, 156, 149, 174, 164 151, 159, 154, 144, 174, 169, 139, 164 130, 159, 132, 146, 151, 137, 139, 154 154, 146, 123, 151, 151, 174, 172, 146 139, 128, 164, 144, 159, 156, 146, 144 159, 130, 142, 156, 164, 132, 156, 151 154, 159, 177, 182, 130, 156, 144, 154 154, 169, 149, 169, 164, 151, 154, 139 144, 156, 149, 159, 146, 169, 174, 144 144, 146, 144, 169, 149, 156, 151, 185 166, 159, 159, 180, 159, 164, 164, 174 144, 164, 177, 159, 172, 169, 182, 174 164, 182, 177, 164, 166, 185, 146, 169 164, 164, 161, 144, 156, 149, 161, 151 182, 149, 185, 164, 172, 146, 177, 177 193, 166, 172, 161, 182, 193, 182, 177 169, 174, 182, 159, 174, 177, 177, 154 188, 166, 169, 159, 188, 180, 159, 185 180, 174, 182, 202, 174, 188, 196, 149 166, 196, 180, 188, 156, 172, 182, 161 196, 196, 188, 161, 169, 172, 177, 199 204, 196, 199, 174, 188, 172, 185, 185 188, 207, 204, 180, 185, 199, 164, 188 188, 190, 210, 169, 207, 182, 199, 177 185, 196, 180, 193, 159, 219, 216, 185 213, 174, 174, 182, 180, 182, 174, 174 199, 190, 185, 174, 188, 199, 172, 185 193, 169, 185, 180, 182, 193, 190, 177 169, 166, 164, 164, 177, 159, 185, 172 169, 166, 164, 172, 166, 169, 180, 146 213, 185, 172, 154, 182, 164, 180, 154 182, 142, 172, 139, 182, 164, 161, 151 182, 156, 166, 159, 193, 172, 151, 190 149, 180, 177, 135, 159, 132, 159, 177 144, 137, 144, 172, 172, 156, 161, 164 169, 169, 142, 154, 166, 169, 166, 164 139, 177, 159, 132, 164, 177, 185, 137 149, 151, 144, 159, 154, 154, 164, 164 156, 154, 156, 154, 139, 144, 151, 139 149, 137, 151, 169, 177, 151, 172, 166 146, 146, 154, 149, 149, 149, 144, 154 146, 159, 154, 164, 154, 144, 149, 154 139, 154, 151, 154, 149, 123, 159, 149 149, 177, 154, 164, 146, 159, 169, 139 156, 159, 137, 146, 146, 137, 137, 135 137, 151, 135, 161, 164, 164, 137, 159 137, 139, 159, 149, 172, 144, 149, 137 149, 137, 161, 159, 177, 144, 125, 156 161, 144, 159, 154, 130, 144, 161, 174 132, 174, 149, 159, 142, 151, 156, 164 154, 166, 135, 144, 161, 144, 139, 156 151, 144, 159, 154, 146, 128, 159, 139 159, 144, 164, 151, 146, 159, 132, 177 146, 146, 137, 154, 146, 177, 161, 146 169, 154, 185, 159, 144, 161, 151, 164 144, 172, 161, 180, 182, 169, 149, 188 182, 172, 166, 182, 188, 193, 213, 196 196, 225, 228, 207, 207, 207, 237, 222 222, 213, 193, 193, 188, 172, 182, 188 159, 146, 156, 151, 137, 144, 159, 149 139, 128, 121, 123, 123, 119, 142, 144 130, 137, 119, 108, 144, 139, 137, 132 123, 142, 130, 119, 125, 117, 112, 114 114, 110, 132, 106, 130, 119, 117, 90 121, 132, 123, 121, 104, 98, 121, 119 146, 114, 130, 106, 123, 108, 123, 110 106, 121, 117, 102, 110, 132, 130, 108 125, 117, 128, 110, 94, 112, 123, 104 119, 108, 123, 110, 119, 112, 119, 96 106, 114, 108, 102, 132, 123, 121, 90 121, 119, 104, 85, 119, 106, 98, 104 104, 123, 121, 104, 100, 108, 112, 117 100, 106, 110, 102, 123, 94, 119, 110 117, 117, 104, 104, 114, 114, 76, 96 98, 98, 110, 117, 104, 90, 98, 117 110, 81, 114, 106, 119, 104, 117, 114 108, 110, 106, 128, 108, 104, 125, 104 94, 121, 117, 128, 106, 132, 110, 106 110, 135, 100, 117, 94, 104, 94, 117 110, 112, 110, 117, 121, 98, 114, 100 108, 106, 96, 102, 108, 108, 104, 128 117, 104, 94, 112, 106, 119, 114, 130 121, 104, 114, 128, 121, 119, 110, 85 106, 100, 117, 102, 100, 108, 106, 104 110, 102, 90, 121, 86, 112, 106, 106 96, 88, 125, 102, 123, 106, 96, 112 108, 100, 92, 90, 104, 110, 121, 112 92, 119, 102, 102, 96, 90, 112, 96 106, 98, 139, 125, 125, 102, 110, 114 128, 110, 104, 121, 98, 96, 110, 100 112, 130, 130, 117, 135, 108, 130, 110 121, 119, 96, 114, 110, 117, 132, 94 119, 130, 123, 92, 128, 117, 98, 112 121, 114, 121, 112, 108, 121, 128, 130 135, 114, 146, 117, 121, 144, 119, 130 121, 137, 114, 117, 114, 123, 110, 112 135, 149, 144, 151, 125, 146, 142, 149 135, 151, 119, 137, 159, 144, 142, 161 144, 161, 166, 169, 185, 169, 174, 188 180, 182, 180, 193, 180, 199, 185, 219 231, 202, 219, 219, 202, 219, 237, 243 262, 253, 237, 234, 237, 246, 250, 243 231, 228, 216, 222, 222, 219, 237, 228 199, 177, 188, 202, 196, 172, 174, 166 172, 164, 172, 164, 161, 130, 166, 135 130, 123, 121, 114, 137, 139, 139, 128 119, 102, 117, 130, 135, 110, 114, 121 104, 106, 106, 104, 112, 104, 114, 106 108, 102, 121, 100, 130, 106, 100, 125 112, 104, 100, 108, 104, 117, 92, 108 114, 110, 114, 106, 85, 92, 104, 98 102, 132, 112, 104, 92, 98, 106, 108 88, 121, 98, 86, 106, 100, 104, 92 100, 106, 114, 90, 117, 96, 104, 108 94, 94, 102, 92, 121, 92, 114, 117 100, 106, 92, 117, 110, 110, 114, 90 102, 117, 100, 108, 90, 98, 96, 104 121, 104, 114, 112, 98, 98, 96, 114 108, 86, 98, 90, 98, 100, 102, 108 104, 108, 112, 92, 125, 102, 85, 96 117, 90, 96, 108, 88, 85, 94, 100 100, 100, 86, 79, 110, 102, 112, 86 106, 117, 94, 102, 117, 96, 108, 86 100, 114, 92, 119, 112, 102, 114, 92 100, 96, 104, 102, 98, 123, 77, 119 110, 100, 100, 100, 83, 94, 110, 83 104, 85, 96, 92, 106, 108, 94, 104 92, 108, 112, 114, 98, 104, 96, 98 100, 123, 110, 125, 100, 102, 100, 88 100, 100, 94, 92, 102, 83, 96, 96 92, 106, 100, 88, 121, 88, 100, 77 98, 100, 108, 108, 86, 88, 106, 94 121, 108, 85, 114, 96, 114, 110, 81 98, 94, 88, 96, 114, 108, 90, 100 110, 96, 119, 100, 88, 128, 98, 108 108, 106, 100, 110, 112, 100, 110, 104 112, 102, 96, 110, 106, 104, 94, 98 94, 94, 92, 104, 108, 102, 102, 112 114, 98, 100, 96, 96, 104, 112, 108 106, 110, 92, 100, 96, 90, 102, 98 86, 119, 106, 114, 112, 100, 114, 108 102, 106, 110, 88, 112, 79, 125, 110 98, 88, 92, 104, 96, 108, 119, 102 117, 108, 100, 94, 106, 110, 106, 112 106, 102, 85, 106, 123, 125, 100, 117 100, 106, 108, 86, 100, 100, 110, 108 110, 110, 121, 119, 100, 106, 110, 119 117, 119, 88, 102, 94, 117, 121, 123 123, 108, 94, 123, 121, 90, 106, 114 104, 102, 119, 102, 123, 130, 100, 96 110, 110, 119, 117, 102, 108, 108, 121 106, 108, 121, 104, 128, 106, 108, 119 100, 100, 114, 125, 108, 108, 110, 104 121, 112, 106, 117, 130, 108, 110, 125 98, 128, 119, 112, 106, 119, 106, 104 112, 110, 123, 123, 121, 110, 128, 108 128, 96, 112, 121, 112, 117, 149, 112 130, 132, 108, 110, 108, 142, 106, 142 121, 121, 132, 121, 112, 106, 112, 123 121, 117, 100, 130, 104, 146, 114, 121 100, 114, 119, 102, 130, 108, 144, 125 125, 117, 112, 108, 137, 121, 110, 98 110, 117, 119, 128, 121, 142, 100, 102 114, 119, 146, 132, 135, 130, 128, 137 146, 137, 121, 132, 132, 110, 144, 119 128, 132, 137, 132, 121, 128, 154, 146 132, 119, 149, 142, 142, 149, 149, 156 135, 164, 139, 169, 164, 154, 166, 154 180, 172, 177, 172, 180, 193, 174, 177 169, 199, 193, 193, 182, 161, 207, 169 172, 199, 180, 169, 164, 144, 172, 144 177, 154, 154, 166, 154, 146, 135, 135 130, 149, 149, 139, 151, 139, 128, 142 144, 149, 144, 121, 135, 137, 146, 151 139, 154, 154, 137, 142, 128, 139, 144 151, 144, 130, 159, 144, 149, 130, 166 154, 135, 139, 154, 151, 161, 112, 146 137, 128, 144, 121, 142, 132, 132, 144 146, 130, 154, 132, 164, 151, 137, 139 130, 128, 132, 146, 144, 161, 151, 135 151, 151, 169, 159, 132, 137, 144, 130 132, 149, 164, 135, 128, 146, 146, 142 177, 156, 144, 151, 135, 164, 137, 174 144, 161, 151, 151, 149, 144, 142, 149 174, 154, 137, 149, 139, 149, 146, 161 139, 130, 137, 156, 151, 149, 130, 166 166, 144, 144, 137, 121, 159, 123, 132 146, 156, 146, 159, 137, 166, 169, 146 159, 161, 169, 151, 154, 149, 132, 146 156, 149, 164, 156, 149, 149, 151, 164 144, 164, 185, 169, 159, 159, 142, 174 151, 174, 154, 159, 161, 169, 169, 159 182, 164, 177, 174, 174, 185, 164, 182 185, 174, 190, 182, 190, 182, 190, 193 196, 210, 174, 204, 207, 193, 204, 202 196, 219, 196, 177, 202, 207, 188, 202 188, 196, 199, 216, 169, 196, 185, 193 182, 177, 188, 210, 219, 213, 172, 202 166, 180, 196, 193, 199, 188, 199, 199 174, 180, 202, 164, 185, 180, 180, 216 177, 202, 188, 188, 202, 202, 188, 177 202, 174, 188, 188, 216, 190, 196, 188 180, 216, 169, 204, 193, 193, 210, 182 190, 177, 204, 169, 185, 196, 193, 193 193, 177, 182, 196, 193, 190, 196, 196 161, 188, 213, 177, 196, 166, 190, 204 237, 216, 228, 216, 231, 240, 262, 250 289, 253, 286, 276, 286, 292, 279, 335 303, 303, 289, 320, 279, 234, 262, 246 253, 219, 228, 216, 182, 222, 193, 185 202, 204, 199, 207, 202, 166, 204, 202 207, 177, 185, 234, 228, 182, 190, 207 202, 182, 234, 219, 196, 202, 196, 204 204, 202, 193, 196, 202, 204, 237, 202 202, 180, 190, 207, 202, 219, 196, 188 204, 193, 225, 213, 204, 193, 222, 202 190, 185, 222, 182, 210, 196, 199, 202 210, 177, 210, 202, 193, 234, 185, 213 188, 180, 207, 207, 196, 174, 185, 207 196, 216, 185, 204, 207, 216, 182, 213 199, 177, 213, 207, 199, 213, 210, 185 216, 199, 185, 193, 204, 213, 234, 202 225, 204, 228, 222, 207, 207, 196, 207 228, 196, 213, 219, 193, 213, 225, 196 204, 210, 185, 222, 188, 225, 199, 210 228, 213, 207, 216, 193, 202, 204, 216 216, 219, 199, 225, 234, 234, 210, 213 234, 210, 190, 219, 225, 207, 202, 219 177, 202, 219, 210, 210, 202, 225, 196 202, 199, 204, 204, 202, 210, 204, 225 207, 219, 216, 210, 202, 196, 210, 225 207, 216, 199, 216, 228, 225, 196, 199 222, 196, 207, 204, 225, 237, 222, 213 231, 213, 202, 237, 225, 225, 225, 202 207, 219, 213, 202, 237, 216, 202, 222 234, 237, 204, 199, 216, 222, 237, 219 222, 213, 219, 213, 219, 213, 216, 213 213, 185, 213, 213, 225, 216, 243, 240 204, 231, 259, 243, 259, 240, 207, 213 234, 225, 259, 225, 193, 222, 216, 237 234, 231, 237, 228, 222, 240, 193, 219 246, 207, 234, 243, 228, 243, 240, 237 231, 246, 225, 240, 246, 234, 190, 228 225, 262, 237, 259, 234, 246, 253, 250 237, 219, 202, 240, 225, 237, 237, 237 216, 246, 231, 246, 259, 228, 219, 202 222, 253, 213, 272, 253, 243, 250, 222 240, 240, 228, 222, 240, 246, 237, 231 253, 243, 225, 240, 253, 250, 253, 240 272, 228, 243, 276, 240, 222, 256, 219 234, 259, 246, 240, 256, 237, 231, 237 262, 250, 250, 259, 246, 266, 246, 231 259, 228, 210, 231, 259, 246, 262, 246 246, 266, 259, 256, 253, 228, 250, 272 269, 276, 276, 269, 269, 296, 269, 286 292, 299, 292, 292, 286, 292, 286, 299 262, 272, 289, 331, 320, 310, 328, 365 342, 306, 342, 361, 365, 372, 353, 376 396, 365, 380, 384, 384, 357, 350, 392 357, 369, 342, 380, 365, 328, 342, 339 324, 306, 320, 317, 313, 320, 328, 335 313, 339, 310, 292, 313, 310, 313, 335 320, 335, 299, 328, 303, 303, 292, 306 296, 282, 292, 331, 303, 324, 253, 272 289, 282, 272, 286, 262, 306, 266, 276 279, 303, 253, 282, 269, 259, 299, 276 289, 262, 250, 266, 228, 266, 269, 259 269, 240, 246, 269, 269, 246, 256, 262 240, 256, 286, 253, 240, 306, 259, 231 237, 269, 279, 250, 266, 253, 253, 253 276, 272, 243, 262, 234, 266, 237, 259 262, 286, 250, 243, 259, 250, 276, 286 286, 225, 243, 246, 276, 240, 243, 272 276, 266, 234, 243, 253, 228, 276, 262 259, 246, 269, 289, 266, 266, 269, 253 262, 243, 253, 246, 259, 262, 262, 259 269, 292, 262, 292, 296, 286, 272, 282 292, 286, 292, 276, 317, 303, 350, 328 361, 392, 353, 392, 396, 471, 480, 515 520, 600, 590, 620, 630, 686, 713, 778 729, 795, 767, 824, 734, 762, 812, 829 812, 718, 762, 676, 645, 571, 548, 557 506, 502, 449, 408, 416, 420, 369, 392 353, 357, 380, 339, 365, 328, 357, 331 299, 310, 313, 310, 320, 299, 289, 331 310, 276, 313, 279, 286, 262, 269, 289 272, 262, 282, 272, 276, 282, 306, 292 286, 289, 272, 289, 286, 289, 250, 289 276, 262, 289, 292, 266, 266, 272, 289 276, 246, 303, 276, 269, 272, 262, 306 286, 279, 282, 282, 276, 286, 286, 286 320, 262, 313, 296, 292, 279, 289, 299 310, 279, 250, 279, 279, 256, 289, 303 259, 276, 292, 289, 328, 299, 279, 276 299, 286, 282, 292, 289, 306, 279, 292 320, 282, 296, 328, 306, 320, 306, 331 292, 313, 279, 313, 317, 320, 331, 299 346, 306, 299, 320, 246, 292, 299, 289 292, 279, 272, 237, 237, 272, 266, 272 243, 250, 246, 256, 269, 246, 262, 246 231, 237, 250, 246, 243, 237, 262, 250 259, 269, 256, 246, 240, 269, 234, 246 240, 240, 250, 234, 234, 253, 250, 231 246, 266, 243, 243, 262, 225, 250, 234 246, 237, 243, 243, 213, 259, 240, 228 228, 246, 228, 243, 246, 237, 250, 234 234, 240, 237, 246, 216, 231, 253, 234 228, 228, 207, 231, 240, 219, 237, 231 272, 228, 243, 259, 231, 231, 225, 243 222, 250, 246, 234, 246, 228, 228, 219 225, 219, 250, 253, 216, 234, 243, 234 253, 234, 234, 262, 259, 246, 234, 231 250, 199, 240, 243, 246, 210, 243, 246 213, 219, 234, 213, 240, 219, 243, 219 243, 234, 228, 259, 228, 213, 222, 228 246, 228, 243, 204, 210, 202, 253, 243 237, 228, 231, 237, 225, 216, 237, 259 216, 243, 243, 237, 237, 237, 237, 250 240, 240, 250, 246, 240, 246, 246, 259 193, 253, 219, 256, 276, 231, 225, 262 234, 237, 259, 219, 243, 234, 231, 219 250, 262, 262, 259, 240, 213, 250,/