SampleIdent,926A 26H5 105-107clay,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,12-mar-1994 4:23,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 154, 169, 161, 177, 169, 156, 144, 174 139, 156, 135, 135, 151, 151, 164, 135 154, 139, 144, 135, 149, 159, 151, 144 144, 159, 123, 156, 149, 149, 149, 142 144, 132, 137, 144, 169, 169, 146, 169 139, 149, 159, 159, 130, 149, 123, 139 135, 125, 144, 130, 149, 132, 117, 132 142, 132, 121, 144, 132, 125, 137, 123 121, 139, 132, 130, 142, 132, 130, 112 139, 125, 144, 128, 142, 123, 135, 121 110, 135, 144, 128, 123, 144, 149, 117 137, 128, 121, 139, 121, 137, 125, 132 128, 96, 128, 112, 146, 142, 132, 119 130, 135, 125, 119, 130, 125, 125, 132 128, 137, 121, 132, 119, 125, 119, 144 144, 125, 110, 146, 137, 121, 121, 132 137, 137, 137, 114, 117, 128, 146, 144 114, 151, 132, 146, 151, 139, 151, 130 144, 132, 144, 137, 149, 132, 121, 137 121, 123, 130, 142, 110, 154, 159, 161 142, 135, 125, 137, 159, 135, 135, 137 137, 135, 135, 146, 130, 135, 121, 130 137, 142, 137, 121, 146, 137, 149, 146 128, 139, 123, 137, 139, 164, 132, 125 151, 142, 154, 139, 151, 139, 142, 149 146, 144, 139, 154, 144, 149, 144, 130 130, 139, 146, 144, 159, 144, 125, 149 146, 149, 144, 159, 146, 142, 149, 169 139, 132, 132, 149, 130, 142, 146, 164 137, 151, 137, 132, 151, 137, 137, 128 137, 135, 164, 146, 132, 149, 146, 149 146, 154, 156, 149, 137, 144, 151, 149 159, 146, 159, 117, 142, 146, 139, 128 169, 137, 144, 149, 156, 149, 146, 139 159, 149, 123, 146, 142, 135, 142, 161 130, 169, 142, 154, 154, 144, 135, 142 142, 149, 149, 142, 151, 154, 144, 146 132, 137, 164, 144, 137, 139, 149, 151 149, 149, 117, 156, 156, 139, 146, 164 154, 149, 151, 135, 161, 154, 130, 132 128, 146, 144, 151, 146, 156, 151, 156 130, 137, 154, 164, 164, 172, 151, 154 169, 154, 156, 193, 135, 146, 149, 159 161, 151, 151, 151, 146, 149, 137, 149 164, 135, 135, 149, 159, 151, 144, 156 172, 164, 142, 149, 172, 144, 146, 146 144, 135, 164, 137, 164, 159, 144, 164 174, 149, 185, 174, 146, 132, 151, 159 130, 172, 146, 144, 172, 139, 172, 166 154, 149, 146, 164, 164, 154, 154, 164 151, 169, 132, 151, 166, 154, 164, 159 144, 182, 174, 161, 159, 161, 154, 172 190, 154, 166, 154, 159, 164, 151, 144 156, 161, 174, 169, 174, 154, 174, 169 172, 146, 164, 166, 154, 142, 169, 156 154, 172, 132, 156, 151, 137, 146, 161 188, 172, 161, 151, 164, 166, 164, 154 149, 154, 156, 156, 177, 149, 154, 172 149, 159, 169, 154, 128, 154, 182, 149 169, 146, 159, 154, 144, 164, 166, 169 142, 149, 159, 156, 144, 161, 149, 154 174, 159, 169, 154, 137, 159, 130, 149 144, 139, 142, 182, 142, 151, 132, 130 154, 159, 139, 174, 166, 151, 166, 154 161, 172, 135, 149, 135, 137, 149, 137 164, 137, 135, 144, 159, 159, 154, 149 135, 161, 169, 151, 132, 137, 151, 146 144, 149, 151, 180, 151, 149, 132, 130 137, 144, 125, 132, 156, 144, 154, 130 149, 139, 139, 139, 172, 149, 128, 144 149, 137, 154, 139, 144, 154, 121, 135 121, 125, 146, 135, 112, 125, 137, 135 132, 142, 132, 128, 154, 144, 137, 130 139, 164, 132, 144, 156, 137, 144, 146 144, 159, 142, 154, 154, 128, 144, 123 128, 139, 164, 149, 135, 161, 144, 130 139, 144, 159, 142, 135, 132, 121, 137 139, 128, 144, 156, 121, 156, 125, 125 154, 130, 154, 146, 149, 154, 137, 137 144, 149, 117, 137, 154, 149, 130, 132 139, 159, 142, 130, 135, 151, 137, 144 149, 139, 156, 156, 149, 128, 137, 137 139, 142, 144, 154, 121, 128, 161, 144 146, 135, 121, 130, 142, 151, 156, 137 123, 130, 142, 144, 121, 159, 142, 142 149, 144, 154, 159, 132, 137, 117, 130 159, 121, 121, 151, 135, 117, 135, 117 117, 108, 137, 130, 130, 135, 117, 132 121, 130, 108, 137, 112, 128, 114, 125 117, 100, 96, 114, 100, 119, 117, 114 117, 123, 135, 121, 108, 114, 104, 106 125, 123, 108, 98, 96, 108, 100, 102 98, 112, 123, 137, 112, 114, 114, 114 112, 100, 98, 119, 106, 96, 96, 119 90, 94, 121, 114, 110, 98, 108, 94 86, 121, 98, 142, 90, 112, 94, 106 110, 90, 90, 96, 112, 110, 108, 98 88, 104, 106, 114, 112, 98, 117, 92 104, 100, 104, 86, 90, 104, 88, 92 110, 128, 114, 100, 100, 110, 112, 110 59, 96, 106, 125, 86, 102, 94, 92 106, 96, 100, 92, 96, 92, 117, 104 100, 112, 79, 104, 92, 100, 104, 121 112, 112, 92, 104, 92, 94, 121, 102 114, 88, 102, 102, 102, 114, 112, 117 119, 94, 102, 86, 98, 96, 88, 100 88, 79, 94, 92, 96, 98, 121, 85 98, 100, 98, 85, 110, 94, 94, 71 104, 90, 98, 104, 98, 88, 106, 92 86, 119, 112, 94, 108, 112, 100, 108 86, 119, 94, 86, 112, 79, 85, 117 106, 88, 106, 92, 114, 83, 94, 92 96, 102, 96, 102, 104, 85, 110, 112 96, 100, 90, 128, 102, 112, 79, 102 110, 125, 119, 98, 100, 104, 106, 85 96, 100, 100, 117, 88, 108, 90, 79 104, 100, 110, 110, 90, 102, 106, 83 92, 100, 106, 106, 79, 102, 90, 106 114, 104, 106, 98, 102, 102, 117, 88 119, 110, 119, 112, 108, 86, 100, 94 96, 112, 108, 106, 106, 130, 100, 102 92, 117, 112, 121, 114, 121, 98, 114 104, 125, 121, 108, 110, 121, 132, 112 128, 100, 112, 139, 119, 125, 142, 144 128, 132, 154, 144, 130, 151, 135, 156 144, 166, 154, 146, 142, 185, 149, 188 172, 164, 151, 177, 219, 207, 193, 202 213, 216, 228, 216, 237, 219, 234, 253 262, 250, 276, 256, 279, 266, 286, 296 286, 303, 269, 286, 286, 253, 279, 279 246, 259, 259, 228, 231, 219, 213, 202 202, 185, 207, 185, 190, 164, 144, 172 142, 151, 149, 154, 139, 144, 135, 125 135, 128, 125, 135, 125, 119, 117, 121 119, 92, 112, 121, 117, 121, 114, 119 130, 108, 119, 114, 92, 119, 100, 86 108, 96, 110, 114, 106, 96, 104, 102 110, 90, 110, 94, 98, 90, 98, 106 94, 100, 123, 104, 100, 90, 98, 92 96, 100, 112, 108, 106, 92, 92, 83 88, 104, 94, 104, 81, 114, 92, 77 100, 102, 112, 100, 86, 108, 92, 106 85, 102, 88, 96, 92, 86, 102, 92 85, 102, 108, 86, 98, 92, 94, 112 106, 92, 108, 94, 96, 90, 98, 102 85, 76, 88, 102, 98, 96, 106, 98 98, 94, 94, 88, 102, 98, 102, 92 86, 121, 85, 102, 108, 90, 102, 86 98, 83, 117, 83, 108, 86, 88, 100 94, 98, 108, 106, 81, 106, 98, 98 106, 92, 117, 96, 117, 92, 85, 106 76, 102, 123, 86, 92, 94, 92, 88 94, 86, 88, 88, 85, 110, 86, 83 98, 100, 100, 96, 96, 94, 98, 106 86, 85, 96, 92, 119, 90, 100, 102 119, 88, 106, 100, 98, 100, 86, 104 104, 100, 88, 114, 96, 94, 106, 106 106, 94, 92, 104, 85, 102, 110, 112 90, 112, 90, 92, 85, 106, 121, 98 98, 108, 96, 114, 92, 98, 123, 85 114, 98, 88, 102, 96, 92, 94, 112 110, 104, 112, 110, 108, 92, 108, 108 110, 102, 100, 106, 114, 100, 102, 92 102, 96, 90, 85, 104, 86, 110, 106 112, 106, 108, 94, 98, 86, 88, 108 90, 114, 102, 98, 102, 106, 104, 112 100, 108, 96, 104, 98, 104, 102, 88 92, 106, 106, 104, 88, 137, 86, 90 85, 106, 106, 112, 104, 98, 112, 92 102, 108, 106, 90, 112, 98, 85, 98 86, 85, 98, 104, 121, 108, 102, 88 112, 98, 106, 85, 104, 104, 88, 92 108, 108, 106, 104, 100, 108, 86, 100 90, 98, 102, 102, 94, 104, 92, 104 108, 100, 121, 110, 119, 112, 98, 117 112, 119, 110, 112, 102, 117, 121, 94 108, 98, 100, 94, 108, 119, 117, 108 110, 119, 121, 102, 100, 110, 96, 100 92, 121, 106, 119, 125, 108, 106, 130 102, 114, 104, 100, 104, 117, 104, 130 90, 110, 114, 112, 104, 92, 117, 106 119, 110, 92, 121, 110, 110, 119, 112 100, 110, 108, 121, 106, 135, 119, 121 106, 130, 100, 106, 98, 112, 90, 114 117, 119, 123, 121, 114, 94, 112, 123 114, 130, 106, 102, 128, 110, 90, 121 137, 121, 125, 98, 96, 132, 149, 117 121, 125, 112, 130, 100, 130, 112, 106 117, 86, 108, 123, 100, 125, 114, 121 128, 112, 104, 102, 125, 128, 110, 104 100, 112, 117, 135, 130, 98, 98, 132 112, 123, 108, 128, 117, 119, 114, 112 125, 117, 108, 125, 135, 123, 128, 121 121, 130, 121, 137, 128, 108, 139, 135 137, 102, 137, 137, 144, 130, 130, 123 137, 154, 121, 151, 121, 108, 125, 114 130, 128, 121, 117, 137, 125, 117, 144 123, 161, 144, 130, 142, 146, 125, 125 114, 121, 130, 121, 135, 121, 135, 123 119, 125, 142, 112, 112, 144, 149, 130 142, 112, 146, 114, 128, 130, 137, 146 139, 114, 117, 137, 130, 142, 137, 132 146, 132, 137, 151, 123, 114, 146, 121 123, 142, 137, 130, 114, 135, 130, 146 128, 117, 119, 114, 130, 142, 121, 135 125, 121, 135, 104, 130, 144, 117, 137 132, 137, 121, 119, 149, 125, 123, 132 135, 132, 128, 130, 132, 137, 119, 135 128, 135, 119, 119, 125, 128, 139, 128 128, 159, 135, 139, 130, 142, 135, 156 137, 151, 132, 130, 135, 154, 137, 144 128, 154, 128, 132, 169, 135, 128, 146 128, 137, 119, 139, 132, 135, 139, 144 123, 161, 128, 151, 125, 154, 144, 123 119, 123, 146, 149, 137, 151, 161, 149 137, 144, 144, 161, 139, 161, 144, 159 159, 159, 151, 159, 151, 151, 159, 172 146, 182, 130, 139, 144, 142, 154, 142 139, 169, 146, 154, 166, 132, 154, 151 146, 159, 161, 156, 174, 180, 185, 190 174, 161, 166, 185, 169, 169, 193, 196 164, 182, 202, 188, 219, 180, 177, 210 199, 222, 210, 196, 225, 210, 213, 234 222, 202, 222, 222, 210, 196, 225, 228 234, 234, 213, 228, 243, 204, 190, 207 231, 199, 204, 213, 202, 196, 172, 199 204, 234, 222, 216, 222, 219, 204, 196 196, 202, 228, 219, 196, 188, 219, 182 213, 213, 180, 216, 196, 169, 222, 190 216, 196, 188, 234, 199, 222, 190, 196 185, 185, 228, 210, 216, 225, 185, 177 210, 185, 188, 199, 190, 207, 188, 222 204, 207, 219, 202, 210, 231, 199, 207 204, 196, 196, 219, 219, 222, 216, 193 234, 240, 228, 199, 246, 225, 199, 269 262, 231, 259, 253, 269, 266, 296, 282 269, 246, 246, 266, 228, 286, 240, 253 228, 240, 204, 222, 196, 228, 213, 193 210, 216, 199, 185, 199, 225, 193, 193 207, 219, 207, 207, 228, 228, 225, 202 196, 207, 237, 202, 237, 188, 185, 185 199, 182, 190, 216, 199, 234, 234, 213 219, 199, 207, 216, 210, 188, 228, 210 237, 193, 231, 256, 213, 228, 228, 231 216, 225, 237, 225, 213, 234, 199, 204 196, 202, 196, 210, 222, 225, 210, 222 216, 196, 210, 207, 202, 188, 216, 204 213, 231, 225, 199, 166, 219, 222, 199 199, 225, 216, 204, 222, 231, 231, 204 204, 202, 199, 202, 199, 202, 199, 213 216, 207, 196, 210, 188, 199, 188, 210 222, 234, 196, 219, 216, 202, 213, 210 222, 213, 225, 228, 207, 234, 199, 202 216, 234, 210, 228, 228, 222, 219, 231 210, 204, 231, 228, 210, 216, 231, 210 234, 207, 204, 202, 222, 213, 210, 222 237, 204, 222, 213, 225, 243, 213, 213 231, 210, 207, 199, 231, 216, 225, 234 240, 216, 237, 228, 216, 196, 210, 216 202, 207, 219, 207, 213, 228, 213, 193 210, 207, 219, 231, 188, 243, 240, 222 243, 231, 222, 237, 228, 219, 234, 259 219, 234, 222, 228, 219, 222, 250, 190 216, 240, 207, 210, 216, 202, 228, 246 234, 253, 222, 253, 231, 228, 219, 219 237, 240, 190, 228, 207, 216, 219, 213 237, 231, 231, 213, 222, 213, 222, 253 222, 219, 237, 240, 228, 231, 231, 237 228, 228, 234, 225, 246, 213, 246, 210 210, 222, 228, 228, 237, 216, 219, 219 246, 210, 216, 219, 246, 219, 246, 225 250, 246, 207, 243, 237, 219, 237, 262 240, 256, 237, 237, 246, 222, 269, 202 234, 234, 266, 256, 234, 210, 231, 243 231, 210, 253, 225, 219, 256, 256, 225 246, 225, 250, 246, 225, 253, 250, 240 243, 216, 246, 207, 276, 231, 231, 216 253, 250, 225, 259, 243, 246, 246, 216 246, 231, 253, 237, 250, 259, 246, 243 246, 243, 237, 240, 243, 231, 269, 262 234, 231, 259, 276, 276, 272, 250, 292 243, 262, 269, 272, 286, 296, 276, 266 253, 276, 259, 266, 276, 306, 279, 289 331, 303, 313, 331, 299, 317, 310, 317 328, 335, 346, 384, 376, 388, 376, 372 388, 424, 361, 420, 412, 416, 441, 428 380, 412, 408, 467, 424, 441, 428, 424 412, 388, 388, 384, 361, 384, 328, 353 346, 365, 320, 331, 320, 324, 331, 320 299, 310, 296, 303, 324, 324, 317, 269 328, 276, 259, 292, 282, 299, 269, 296 279, 269, 292, 286, 292, 262, 262, 266 286, 240, 282, 253, 269, 289, 262, 240 266, 253, 276, 289, 286, 246, 250, 269 272, 262, 262, 276, 272, 266, 240, 272 243, 289, 237, 222, 225, 240, 269, 266 272, 246, 266, 234, 259, 286, 266, 228 228, 222, 272, 259, 262, 234, 262, 256 259, 262, 272, 266, 216, 272, 256, 250 250, 240, 250, 243, 225, 250, 202, 256 262, 240, 246, 262, 256, 272, 246, 253 240, 259, 259, 272, 272, 222, 282, 279 243, 266, 276, 266, 246, 256, 256, 246 240, 282, 246, 276, 246, 243, 262, 272 282, 266, 237, 219, 253, 259, 279, 266 266, 259, 250, 286, 286, 335, 303, 299 292, 328, 313, 335, 372, 342, 380, 392 441, 449, 454, 462, 471, 471, 475, 538 562, 543, 548, 548, 571, 515, 548, 506 497, 475, 433, 388, 369, 376, 365, 331 282, 310, 331, 296, 292, 279, 306, 272 289, 296, 306, 266, 303, 299, 256, 286 292, 276, 303, 276, 269, 246, 253, 256 266, 243, 269, 259, 231, 246, 272, 279 246, 246, 282, 259, 269, 253, 243, 234 250, 246, 272, 228, 256, 222, 282, 262 259, 266, 262, 266, 306, 266, 259, 299 256, 266, 246, 240, 253, 269, 276, 262 237, 272, 269, 266, 269, 246, 279, 256 259, 266, 279, 231, 256, 234, 272, 259 269, 282, 262, 231, 246, 246, 272, 256 228, 259, 269, 246, 250, 231, 256, 250 256, 276, 269, 262, 262, 250, 253, 243 253, 256, 259, 234, 259, 256, 279, 253 246, 240, 237, 250, 256, 296, 256, 276 256, 266, 240, 246, 216, 256, 243, 240 234, 237, 272, 219, 269, 225, 231, 250 253, 219, 246, 240, 243, 243, 222, 259 237, 256, 231, 225, 231, 256, 243, 225 237, 243, 276, 250, 237, 228, 228, 250 256, 228, 246, 182, 259, 240, 237, 246 231, 234, 231, 259, 225, 216, 222, 259 240, 243, 246, 246, 213, 222, 228, 246 246, 237, 253, 243, 243, 259, 219, 276 222, 231, 216, 225, 256, 243, 228, 234 246, 240, 228, 219, 266, 225, 222, 216 259, 237, 213, 243, 237, 231, 225, 246 222, 228, 231, 243, 234, 219, 219, 240 250, 240, 262, 219, 228, 219, 250, 228 231, 213, 231, 246, 234, 231, 207, 216 240, 253, 240, 240, 231, 234, 213, 243 222, 253, 204, 222, 225, 219, 225, 246 259, 196, 262, 240, 262, 213, 262, 240 243, 216, 243, 225, 237, 237, 225, 199 234, 228, 219, 225, 219, 246, 262, 213 213, 246, 225, 219, 246, 231, 234, 240 210, 213, 231, 243, 213, 237, 207, 222 234, 259, 222, 231, 213, 234, 246, 243 250, 240, 204, 222, 234, 256, 231, 222 234, 243, 250, 222, 222, 250, 219,/