SampleIdent,926B 25H7 29-31,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 6-mar-1994 15:13,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 240, 202, 240, 190, 185, 174, 188, 202 222, 202, 213, 196, 213, 154, 196, 202 216, 196, 180, 196, 190, 188, 193, 188 199, 190, 161, 185, 182, 202, 210, 177 199, 190, 180, 199, 180, 174, 193, 204 172, 193, 193, 161, 180, 196, 172, 180 180, 182, 177, 185, 185, 159, 190, 188 196, 144, 207, 196, 188, 185, 174, 188 164, 177, 180, 144, 174, 166, 164, 177 151, 188, 177, 177, 164, 174, 149, 177 185, 199, 185, 174, 182, 164, 190, 172 188, 190, 164, 185, 213, 154, 185, 169 166, 156, 174, 174, 177, 149, 169, 169 169, 164, 161, 172, 169, 169, 166, 177 182, 177, 164, 174, 161, 159, 154, 172 180, 159, 177, 169, 180, 161, 174, 182 146, 188, 164, 185, 161, 213, 177, 188 185, 185, 180, 182, 144, 169, 190, 196 196, 172, 149, 164, 149, 188, 193, 177 174, 169, 180, 182, 185, 177, 164, 172 174, 177, 182, 182, 159, 185, 190, 180 154, 161, 166, 174, 177, 169, 193, 156 174, 188, 174, 202, 182, 185, 199, 188 182, 193, 185, 164, 182, 185, 182, 164 185, 199, 193, 185, 177, 169, 156, 169 177, 174, 182, 196, 202, 196, 151, 182 193, 182, 193, 199, 174, 174, 164, 177 166, 182, 169, 164, 180, 182, 180, 174 193, 169, 174, 177, 159, 202, 177, 180 177, 177, 185, 185, 182, 193, 196, 188 177, 177, 193, 204, 190, 185, 174, 185 159, 204, 182, 177, 196, 174, 180, 188 196, 193, 210, 210, 196, 219, 188, 185 180, 172, 182, 196, 196, 193, 196, 196 193, 180, 169, 190, 216, 202, 193, 174 213, 188, 225, 193, 222, 196, 213, 188 180, 213, 210, 204, 185, 202, 177, 210 228, 216, 213, 196, 185, 213, 202, 210 216, 202, 188, 210, 196, 161, 204, 190 199, 188, 193, 222, 199, 202, 207, 190 190, 199, 219, 196, 210, 222, 210, 219 210, 202, 225, 202, 213, 202, 234, 199 185, 199, 199, 216, 213, 204, 219, 228 219, 202, 213, 228, 237, 207, 228, 222 204, 199, 222, 219, 199, 228, 199, 213 210, 204, 210, 202, 219, 210, 185, 225 216, 210, 222, 225, 199, 240, 234, 207 228, 222, 190, 213, 228, 231, 222, 210 199, 202, 210, 243, 210, 213, 219, 204 188, 193, 213, 193, 225, 207, 219, 210 207, 204, 222, 207, 231, 204, 210, 225 222, 246, 210, 204, 190, 204, 196, 216 204, 207, 193, 193, 222, 199, 219, 196 210, 204, 204, 210, 193, 250, 196, 199 207, 207, 185, 185, 231, 222, 177, 199 222, 219, 177, 210, 213, 196, 202, 213 185, 202, 182, 166, 225, 210, 182, 190 180, 199, 196, 182, 196, 199, 210, 180 199, 199, 169, 190, 207, 207, 174, 182 219, 188, 193, 207, 172, 210, 204, 193 177, 177, 185, 213, 190, 172, 180, 182 182, 190, 144, 199, 185, 204, 202, 199 177, 177, 180, 164, 174, 154, 151, 188 159, 169, 182, 182, 154, 196, 185, 204 154, 156, 174, 177, 185, 151, 193, 166 177, 188, 172, 185, 185, 164, 151, 161 182, 193, 174, 185, 169, 151, 182, 164 161, 169, 161, 169, 149, 159, 159, 190 169, 169, 174, 188, 172, 164, 174, 154 185, 174, 161, 177, 161, 159, 169, 159 139, 177, 196, 161, 164, 144, 177, 159 185, 193, 161, 125, 151, 172, 174, 169 172, 182, 164, 169, 149, 172, 159, 166 164, 174, 177, 149, 182, 166, 159, 154 182, 182, 185, 164, 177, 159, 156, 149 169, 151, 146, 139, 161, 149, 164, 188 172, 159, 164, 164, 177, 180, 164, 166 149, 144, 161, 180, 151, 172, 166, 164 154, 177, 169, 159, 151, 199, 144, 166 182, 188, 177, 154, 149, 177, 169, 164 166, 164, 174, 188, 180, 156, 185, 154 166, 182, 151, 159, 164, 177, 156, 159 159, 174, 139, 188, 180, 190, 182, 188 190, 172, 188, 182, 164, 185, 185, 159 161, 199, 169, 169, 169, 172, 149, 154 132, 137, 151, 166, 177, 142, 154, 130 161, 161, 159, 149, 149, 128, 144, 149 130, 123, 149, 130, 166, 142, 146, 149 132, 137, 132, 146, 142, 142, 108, 102 130, 128, 121, 128, 130, 125, 149, 130 130, 130, 117, 121, 110, 135, 137, 119 128, 144, 121, 142, 137, 144, 135, 130 139, 121, 128, 108, 112, 110, 135, 139 135, 114, 121, 146, 130, 123, 125, 106 142, 117, 132, 104, 121, 108, 125, 135 110, 130, 96, 110, 119, 123, 123, 139 104, 108, 130, 121, 114, 108, 112, 128 106, 121, 112, 119, 100, 114, 102, 125 110, 123, 114, 125, 121, 110, 98, 96 123, 119, 123, 110, 102, 128, 137, 104 121, 114, 123, 106, 94, 104, 137, 125 117, 106, 139, 123, 100, 102, 123, 117 117, 135, 108, 117, 108, 106, 110, 121 119, 96, 132, 100, 108, 121, 123, 110 121, 94, 114, 119, 123, 110, 121, 132 106, 117, 96, 117, 108, 125, 121, 125 117, 106, 94, 121, 112, 121, 108, 112 119, 112, 130, 108, 121, 128, 112, 121 90, 130, 135, 119, 114, 117, 119, 114 108, 121, 106, 90, 100, 110, 117, 114 112, 137, 102, 110, 130, 100, 125, 119 119, 117, 121, 114, 125, 117, 119, 123 132, 117, 121, 144, 135, 92, 119, 121 142, 114, 130, 121, 144, 121, 114, 110 121, 117, 114, 128, 119, 128, 117, 121 121, 130, 130, 114, 142, 149, 139, 117 139, 128, 130, 119, 137, 130, 149, 132 125, 130, 130, 142, 144, 159, 146, 125 164, 154, 149, 156, 156, 132, 132, 123 137, 128, 149, 149, 172, 177, 154, 166 174, 151, 164, 161, 154, 161, 182, 166 202, 182, 199, 196, 182, 207, 210, 193 159, 216, 222, 228, 243, 222, 240, 243 269, 246, 269, 266, 266, 259, 289, 292 313, 328, 331, 372, 365, 365, 376, 376 424, 420, 437, 433, 454, 467, 475, 520 488, 520, 557, 571, 538, 548, 586, 566 586, 655, 630, 557, 538, 557, 562, 524 502, 538, 511, 467, 484, 416, 404, 335 369, 392, 313, 299, 306, 282, 276, 303 292, 256, 266, 243, 228, 237, 225, 210 172, 199, 180, 190, 182, 180, 169, 180 161, 159, 159, 146, 166, 166, 139, 166 149, 174, 159, 121, 142, 125, 149, 139 128, 102, 102, 137, 128, 135, 130, 104 117, 135, 130, 119, 125, 125, 119, 106 132, 119, 114, 135, 112, 117, 114, 121 110, 114, 112, 135, 108, 110, 114, 104 110, 112, 94, 119, 117, 92, 100, 92 108, 104, 108, 104, 106, 108, 106, 119 123, 121, 114, 102, 94, 102, 90, 79 88, 86, 90, 117, 88, 117, 92, 92 102, 79, 92, 77, 79, 94, 100, 96 121, 104, 106, 121, 85, 94, 94, 106 81, 88, 100, 94, 106, 96, 108, 102 98, 98, 104, 90, 94, 85, 96, 112 106, 85, 92, 79, 106, 94, 123, 94 98, 98, 104, 94, 106, 100, 85, 96 104, 94, 130, 102, 79, 108, 81, 92 106, 88, 85, 106, 79, 98, 94, 100 117, 96, 83, 94, 94, 92, 90, 106 88, 96, 106, 90, 94, 90, 121, 100 104, 96, 86, 119, 81, 92, 112, 79 114, 83, 96, 94, 94, 112, 98, 96 85, 100, 86, 104, 79, 90, 108, 96 90, 79, 85, 100, 104, 100, 94, 108 106, 98, 92, 112, 92, 108, 88, 98 106, 83, 92, 106, 98, 112, 94, 90 94, 88, 88, 94, 88, 83, 106, 92 94, 100, 119, 98, 77, 92, 100, 98 112, 94, 104, 94, 98, 77, 100, 85 90, 94, 96, 114, 94, 100, 72, 76 106, 100, 96, 94, 90, 92, 81, 100 85, 104, 102, 86, 104, 102, 90, 81 110, 96, 98, 59, 108, 98, 94, 100 100, 121, 98, 106, 102, 92, 83, 98 92, 98, 96, 74, 88, 90, 100, 98 100, 92, 98, 90, 100, 88, 94, 81 100, 106, 110, 96, 106, 96, 94, 86 85, 94, 110, 114, 106, 98, 79, 92 104, 102, 86, 98, 81, 96, 86, 88 102, 94, 77, 86, 77, 92, 108, 88 92, 106, 100, 102, 106, 104, 94, 100 110, 104, 102, 96, 76, 106, 94, 102 114, 90, 110, 96, 104, 96, 102, 98 88, 98, 104, 96, 88, 108, 90, 92 104, 100, 100, 102, 102, 100, 96, 94 96, 74, 100, 85, 106, 86, 96, 106 100, 92, 110, 114, 98, 94, 104, 96 96, 83, 92, 106, 83, 92, 110, 98 114, 90, 86, 92, 96, 106, 114, 90 100, 79, 90, 110, 102, 98, 98, 110 88, 102, 100, 98, 85, 104, 106, 106 121, 102, 90, 104, 85, 117, 94, 106 123, 104, 90, 83, 96, 90, 83, 94 96, 88, 92, 90, 104, 114, 92, 100 79, 100, 100, 94, 96, 100, 121, 114 110, 102, 104, 110, 100, 104, 90, 96 117, 96, 94, 117, 112, 108, 114, 90 108, 96, 119, 108, 114, 108, 108, 94 98, 117, 130, 117, 130, 106, 108, 114 106, 106, 123, 119, 119, 110, 119, 102 121, 135, 119, 102, 123, 110, 114, 108 146, 130, 125, 117, 144, 110, 123, 142 104, 110, 132, 154, 132, 130, 149, 149 144, 137, 121, 142, 142, 117, 130, 132 135, 130, 135, 128, 149, 128, 117, 128 119, 110, 88, 132, 114, 106, 110, 114 132, 110, 94, 102, 108, 102, 112, 104 121, 114, 94, 108, 117, 121, 102, 108 92, 94, 130, 88, 102, 112, 100, 117 88, 96, 110, 106, 100, 104, 104, 106 100, 100, 112, 79, 110, 121, 106, 119 85, 92, 102, 108, 112, 88, 86, 92 98, 92, 94, 102, 92, 123, 92, 108 98, 85, 112, 104, 98, 106, 102, 102 100, 88, 108, 98, 98, 98, 96, 96 102, 102, 110, 86, 108, 102, 104, 85 94, 88, 119, 94, 106, 96, 108, 92 98, 85, 121, 100, 96, 100, 125, 90 90, 104, 86, 102, 86, 108, 102, 106 102, 94, 90, 83, 94, 110, 88, 108 94, 102, 100, 102, 98, 76, 98, 104 104, 104, 114, 110, 108, 96, 121, 121 104, 90, 96, 112, 102, 98, 102, 117 106, 108, 94, 123, 110, 112, 102, 117 125, 104, 112, 114, 137, 112, 117, 119 96, 135, 132, 132, 137, 119, 137, 144 139, 123, 156, 135, 149, 149, 169, 151 146, 149, 149, 159, 169, 166, 182, 182 199, 196, 182, 177, 213, 204, 213, 180 199, 172, 193, 199, 188, 196, 196, 210 202, 188, 172, 210, 193, 199, 185, 177 180, 204, 177, 177, 177, 182, 182, 199 185, 193, 190, 174, 182, 159, 156, 177 172, 164, 164, 164, 166, 146, 164, 164 193, 169, 164, 169, 180, 146, 164, 154 169, 172, 149, 185, 159, 174, 154, 169 164, 169, 169, 142, 151, 161, 164, 139 169, 169, 180, 166, 156, 149, 144, 161 172, 149, 169, 154, 169, 172, 154, 144 164, 185, 161, 177, 177, 174, 169, 199 166, 177, 182, 193, 210, 199, 199, 193 231, 219, 253, 253, 237, 231, 240, 243 262, 266, 234, 272, 253, 207, 216, 216 222, 185, 196, 180, 196, 174, 172, 169 169, 146, 154, 207, 174, 185, 154, 159 174, 146, 154, 159, 185, 159, 146, 172 149, 159, 169, 161, 137, 164, 159, 164 154, 177, 164, 142, 132, 182, 146, 180 146, 159, 154, 156, 169, 156, 161, 182 154, 146, 164, 154, 144, 154, 144, 144 142, 149, 159, 130, 190, 130, 174, 130 164, 146, 159, 159, 161, 139, 161, 144 144, 123, 151, 161, 154, 154, 149, 149 161, 149, 132, 151, 166, 128, 144, 149 137, 146, 151, 159, 149, 137, 164, 164 172, 154, 172, 149, 149, 154, 146, 146 139, 161, 166, 137, 196, 156, 154, 169 151, 154, 142, 149, 159, 142, 149, 159 172, 164, 154, 151, 130, 154, 132, 146 172, 164, 151, 146, 154, 142, 169, 169 151, 154, 185, 142, 174, 149, 169, 169 151, 156, 149, 164, 149, 164, 156, 146 164, 185, 154, 156, 121, 159, 154, 144 154, 149, 159, 159, 161, 166, 166, 164 161, 164, 166, 151, 159, 172, 156, 161 149, 161, 169, 151, 169, 154, 182, 142 169, 164, 166, 154, 156, 169, 172, 169 149, 177, 177, 132, 182, 164, 177, 164 164, 177, 182, 144, 188, 159, 144, 154 159, 137, 182, 159, 151, 144, 161, 164 146, 177, 154, 142, 169, 154, 154, 169 154, 164, 159, 146, 139, 144, 185, 188 180, 177, 154, 164, 151, 180, 137, 156 151, 132, 172, 169, 169, 185, 159, 156 156, 177, 164, 159, 166, 154, 172, 193 156, 161, 159, 164, 172, 185, 164, 169 154, 159, 164, 185, 174, 174, 177, 146 177, 190, 151, 154, 180, 154, 146, 156 182, 146, 164, 172, 164, 144, 137, 174 164, 193, 169, 169, 193, 159, 154, 180 185, 166, 177, 177, 172, 154, 159, 172 166, 166, 199, 177, 177, 154, 207, 193 188, 159, 174, 174, 202, 188, 188, 207 213, 207, 182, 228, 204, 216, 213, 204 196, 210, 219, 210, 213, 234, 234, 246 207, 225, 225, 228, 234, 237, 228, 231 276, 246, 262, 250, 256, 272, 269, 256 279, 296, 279, 313, 282, 313, 324, 339 331, 350, 357, 372, 342, 400, 420, 428 458, 475, 449, 467, 534, 515, 576, 581 600, 586, 630, 681, 666, 708, 708, 784 807, 801, 858, 853, 906, 870, 888, 961 906, 918, 894, 955, 853, 847, 807, 853 807, 751, 681, 745, 692, 676, 625, 625 600, 595, 538, 502, 515, 520, 462, 454 458, 467, 437, 412, 408, 445, 392, 400 396, 392, 384, 392, 357, 353, 361, 384 335, 339, 320, 346, 346, 306, 328, 346 335, 303, 286, 306, 303, 299, 292, 303 292, 256, 253, 256, 240, 262, 279, 259 279, 231, 276, 262, 222, 259, 246, 259 240, 243, 231, 231, 228, 240, 231, 243 190, 225, 231, 253, 256, 234, 250, 231 250, 210, 246, 219, 204, 204, 222, 202 228, 228, 204, 193, 199, 216, 204, 240 190, 202, 234, 213, 219, 188, 185, 210 196, 207, 219, 219, 207, 219, 219, 202 234, 228, 219, 222, 216, 196, 222, 240 213, 202, 250, 213, 219, 213, 207, 246 240, 204, 240, 240, 237, 240, 250, 246 246, 243, 240, 243, 240, 246, 246, 237 246, 240, 276, 234, 253, 282, 272, 292 303, 310, 324, 335, 404, 369, 365, 433 471, 529, 538, 586, 676, 724, 751, 767 824, 858, 835, 876, 835, 835, 784, 778 676, 686, 686, 600, 566, 488, 454, 380 404, 420, 384, 384, 353, 310, 328, 328 299, 262, 299, 303, 296, 310, 266, 276 279, 266, 262, 286, 279, 256, 262, 276 292, 243, 259, 256, 259, 250, 246, 240 222, 253, 266, 219, 256, 256, 222, 246 228, 243, 219, 225, 213, 237, 228, 225 222, 216, 231, 231, 259, 246, 243, 210 243, 237, 250, 246, 269, 234, 250, 256 234, 219, 259, 269, 266, 234, 259, 243 266, 246, 276, 231, 266, 246, 256, 240 240, 237, 253, 234, 240, 210, 243, 228 199, 231, 199, 213, 237, 240, 246, 210 213, 237, 228, 243, 204, 246, 225, 234 225, 228, 228, 240, 231, 231, 219, 240 228, 246, 256, 237, 256, 243, 216, 234 237, 262, 234, 231, 228, 213, 219, 240 234, 225, 190, 196, 207, 210, 193, 202 207, 188, 210, 190, 199, 188, 174, 180 185, 210, 199, 174, 185, 190, 213, 199 180, 190, 207, 202, 219, 213, 180, 177 188, 213, 174, 193, 199, 193, 172, 207 193, 182, 166, 185, 182, 169, 193, 193 177, 188, 193, 204, 182, 174, 188, 164 185, 196, 169, 182, 180, 193, 190, 177 172, 185, 169, 185, 199, 174, 156, 166 174, 188, 174, 166, 172, 188, 185, 188 185, 185, 169, 182, 177, 188, 169, 159 166, 169, 156, 161, 169, 180, 210, 174 177, 190, 202, 193, 199, 156, 174, 180 199, 164, 180, 182, 161, 169, 182, 188 199, 174, 169, 185, 210, 216, 166, 164 169, 188, 182, 169, 199, 156, 193, 169 182, 169, 169, 172, 166, 177, 169, 190 169, 151, 164, 196, 169, 154, 193, 185 185, 180, 172, 174, 161, 177, 180, 156 166, 166, 166, 164, 172, 185, 159, 188 149, 164, 161, 174, 169, 164, 154, 177 196, 193, 159, 180, 172, 174, 159, 172 164, 182, 166, 174, 154, 188, 154, 193 174, 190, 169, 151, 180, 164, 199, 166 169, 159, 151, 174, 159, 154, 166, 193 146, 154, 169, 144, 137, 149, 156,/