SampleIdent,927A 23H4 136-138,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime, 8-mar-1994 8:03,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 234, 240, 253, 256, 240, 266, 262, 231 266, 272, 237, 246, 222, 253, 231, 253 219, 219, 246, 256, 237, 262, 222, 243 246, 222, 216, 234, 246, 250, 253, 210 256, 292, 240, 259, 237, 286, 228, 207 243, 210, 222, 240, 216, 210, 234, 262 231, 237, 219, 216, 225, 259, 222, 240 210, 219, 216, 234, 222, 225, 237, 231 219, 262, 222, 216, 204, 222, 207, 250 228, 207, 250, 210, 240, 207, 237, 231 240, 234, 216, 253, 202, 231, 234, 237 216, 222, 246, 225, 240, 234, 225, 237 231, 237, 243, 240, 210, 228, 222, 237 234, 199, 190, 246, 240, 210, 216, 246 216, 228, 228, 228, 219, 231, 234, 225 222, 234, 222, 216, 207, 246, 240, 204 225, 237, 228, 237, 228, 199, 237, 253 231, 243, 225, 250, 240, 250, 213, 222 240, 234, 237, 240, 193, 213, 216, 243 237, 210, 256, 237, 219, 216, 237, 202 219, 207, 243, 256, 234, 243, 246, 219 225, 219, 210, 222, 219, 225, 207, 231 207, 225, 222, 243, 216, 216, 250, 234 240, 210, 199, 250, 253, 216, 246, 234 231, 234, 237, 253, 234, 231, 196, 219 213, 234, 202, 246, 250, 240, 213, 237 222, 256, 219, 213, 246, 234, 216, 231 250, 228, 253, 266, 225, 234, 210, 204 222, 234, 250, 225, 228, 213, 240, 222 234, 222, 222, 228, 240, 246, 228, 237 231, 228, 216, 237, 237, 210, 225, 231 237, 250, 210, 262, 228, 222, 225, 240 243, 250, 269, 216, 246, 243, 243, 219 228, 225, 237, 207, 231, 222, 237, 222 246, 199, 240, 259, 216, 210, 228, 225 237, 240, 202, 234, 234, 246, 243, 210 228, 246, 256, 225, 202, 237, 243, 269 279, 240, 240, 231, 240, 231, 262, 272 276, 231, 253, 237, 276, 256, 266, 246 231, 250, 250, 246, 253, 234, 222, 222 246, 234, 243, 250, 262, 219, 253, 269 253, 225, 216, 250, 259, 272, 272, 240 243, 234, 234, 240, 237, 272, 279, 259 253, 237, 237, 256, 259, 250, 266, 259 262, 234, 256, 256, 279, 259, 266, 262 240, 292, 272, 253, 286, 282, 250, 231 272, 262, 272, 253, 262, 262, 234, 266 259, 276, 259, 240, 289, 276, 272, 279 282, 272, 262, 253, 286, 256, 306, 234 250, 279, 266, 266, 253, 286, 272, 276 240, 282, 279, 272, 276, 269, 250, 266 243, 256, 286, 269, 256, 266, 299, 289 282, 262, 292, 282, 262, 269, 296, 259 253, 282, 259, 262, 259, 240, 231, 253 243, 262, 222, 231, 262, 272, 276, 250 262, 234, 259, 262, 234, 234, 272, 266 234, 237, 269, 243, 237, 246, 228, 222 240, 246, 228, 243, 253, 259, 269, 228 234, 237, 237, 256, 234, 207, 231, 237 213, 231, 250, 231, 234, 225, 234, 259 240, 213, 256, 225, 243, 234, 228, 266 213, 237, 231, 259, 228, 216, 243, 231 272, 231, 231, 243, 237, 253, 237, 237 234, 240, 188, 256, 228, 234, 253, 246 231, 199, 246, 243, 234, 219, 207, 228 240, 228, 225, 210, 234, 246, 225, 246 219, 240, 234, 216, 228, 228, 213, 213 213, 213, 231, 231, 234, 231, 207, 213 210, 199, 210, 234, 237, 237, 213, 196 219, 219, 210, 225, 234, 204, 216, 202 207, 222, 225, 216, 216, 225, 202, 202 225, 199, 210, 202, 234, 202, 216, 225 219, 240, 210, 213, 222, 219, 228, 210 231, 225, 204, 225, 246, 234, 204, 207 185, 246, 240, 231, 207, 204, 228, 222 234, 202, 210, 199, 207, 199, 222, 213 219, 216, 219, 199, 219, 210, 225, 207 234, 228, 225, 219, 231, 246, 210, 222 237, 222, 222, 207, 219, 188, 237, 243 240, 228, 243, 210, 222, 216, 231, 225 246, 199, 196, 225, 240, 231, 219, 210 240, 250, 246, 234, 250, 250, 256, 231 210, 243, 225, 246, 246, 225, 207, 266 243, 259, 286, 231, 250, 228, 272, 269 276, 276, 292, 272, 286, 253, 250, 246 246, 243, 253, 204, 222, 182, 225, 231 196, 180, 193, 174, 188, 190, 180, 174 177, 172, 193, 149, 177, 180, 164, 172 161, 169, 159, 161, 174, 169, 159, 156 159, 154, 146, 156, 159, 156, 142, 144 154, 151, 132, 121, 139, 135, 151, 130 146, 149, 121, 151, 142, 156, 156, 123 128, 156, 161, 130, 146, 135, 146, 132 125, 149, 137, 146, 142, 149, 144, 149 128, 137, 123, 137, 139, 144, 139, 121 135, 112, 114, 130, 102, 135, 146, 117 139, 132, 146, 123, 125, 114, 142, 130 123, 142, 137, 121, 130, 119, 112, 156 121, 114, 112, 121, 121, 119, 128, 121 130, 144, 123, 108, 119, 137, 135, 119 119, 123, 110, 130, 130, 121, 128, 128 119, 149, 130, 108, 119, 119, 135, 128 125, 135, 130, 114, 121, 117, 125, 128 125, 112, 125, 130, 121, 114, 123, 106 123, 114, 135, 98, 123, 114, 130, 128 130, 117, 121, 110, 144, 112, 100, 112 104, 114, 114, 108, 102, 114, 110, 102 123, 121, 104, 102, 125, 123, 112, 125 114, 125, 114, 125, 146, 130, 114, 125 117, 112, 146, 132, 137, 128, 125, 135 119, 112, 114, 139, 125, 132, 119, 112 112, 130, 117, 144, 102, 112, 132, 117 117, 123, 110, 121, 142, 110, 130, 121 125, 125, 139, 114, 114, 128, 123, 128 125, 110, 144, 112, 142, 139, 123, 117 135, 154, 139, 142, 139, 139, 139, 135 139, 123, 119, 135, 132, 154, 144, 130 135, 125, 144, 139, 132, 128, 130, 137 146, 130, 146, 135, 139, 149, 159, 169 142, 164, 166, 154, 137, 151, 177, 149 159, 185, 182, 177, 172, 182, 193, 188 188, 188, 190, 188, 199, 210, 196, 207 207, 193, 207, 219, 188, 202, 231, 231 222, 225, 231, 256, 259, 266, 292, 272 262, 276, 350, 320, 357, 324, 342, 339 361, 380, 376, 428, 392, 420, 441, 441 458, 484, 497, 493, 552, 581, 581, 566 562, 630, 605, 660, 708, 676, 729, 697 702, 697, 671, 676, 605, 630, 666, 557 557, 543, 515, 488, 449, 392, 428, 388 420, 357, 313, 328, 286, 317, 262, 279 243, 246, 234, 234, 225, 190, 204, 234 204, 196, 180, 177, 185, 177, 182, 164 202, 159, 154, 164, 172, 137, 123, 142 169, 137, 135, 123, 144, 132, 149, 119 146, 137, 137, 130, 117, 130, 128, 104 128, 121, 135, 125, 130, 119, 121, 102 137, 117, 108, 121, 100, 123, 112, 114 96, 123, 104, 117, 102, 121, 104, 104 114, 104, 114, 98, 114, 125, 104, 110 102, 119, 112, 119, 102, 114, 112, 110 106, 100, 119, 100, 106, 119, 92, 104 104, 92, 102, 121, 121, 86, 106, 119 112, 104, 121, 92, 110, 102, 114, 94 110, 106, 104, 114, 106, 98, 112, 108 106, 104, 117, 94, 121, 96, 112, 106 94, 117, 108, 119, 139, 119, 108, 114 94, 128, 98, 117, 108, 130, 104, 100 108, 106, 104, 110, 96, 114, 112, 96 106, 110, 112, 98, 108, 83, 121, 102 96, 100, 98, 104, 94, 117, 90, 106 108, 121, 119, 100, 100, 96, 102, 92 102, 100, 100, 100, 98, 104, 104, 88 114, 96, 117, 112, 110, 90, 100, 81 112, 94, 112, 102, 108, 94, 104, 98 112, 102, 114, 98, 100, 106, 112, 86 117, 121, 94, 96, 100, 71, 121, 117 100, 98, 106, 110, 110, 108, 110, 112 92, 117, 86, 85, 96, 92, 79, 112 108, 100, 100, 94, 88, 104, 121, 102 100, 108, 106, 108, 110, 104, 104, 106 100, 110, 108, 112, 98, 104, 110, 114 94, 119, 100, 102, 110, 92, 83, 96 108, 104, 100, 114, 104, 100, 108, 98 96, 94, 106, 102, 123, 96, 88, 106 114, 100, 94, 100, 96, 86, 102, 100 104, 114, 100, 96, 94, 92, 114, 112 102, 88, 96, 88, 104, 104, 90, 72 110, 130, 117, 119, 108, 100, 110, 102 123, 90, 96, 98, 110, 104, 121, 114 104, 112, 96, 110, 90, 106, 123, 110 110, 92, 104, 106, 108, 110, 104, 114 102, 119, 102, 106, 102, 100, 112, 121 108, 117, 100, 114, 106, 123, 96, 100 104, 104, 94, 108, 98, 92, 125, 102 108, 108, 98, 102, 94, 108, 96, 108 110, 114, 112, 92, 102, 92, 108, 106 130, 117, 114, 125, 98, 98, 108, 98 125, 106, 117, 119, 102, 119, 98, 102 102, 110, 104, 102, 112, 114, 130, 90 108, 112, 123, 104, 110, 108, 106, 110 110, 119, 94, 86, 117, 119, 117, 121 121, 119, 119, 119, 119, 121, 100, 110 114, 108, 108, 114, 121, 110, 106, 114 125, 102, 112, 121, 123, 112, 121, 110 137, 108, 112, 117, 114, 110, 137, 104 123, 123, 121, 123, 106, 121, 135, 98 123, 151, 112, 112, 117, 121, 114, 108 119, 114, 128, 108, 102, 139, 123, 125 112, 130, 128, 125, 110, 132, 117, 130 112, 128, 144, 146, 112, 128, 112, 137 125, 117, 125, 114, 137, 142, 132, 144 128, 135, 125, 142, 130, 125, 135, 139 139, 130, 144, 130, 125, 137, 142, 169 149, 146, 149, 151, 151, 151, 169, 151 154, 164, 156, 174, 156, 188, 210, 156 185, 172, 185, 185, 190, 177, 142, 164 149, 169, 161, 149, 132, 144, 156, 137 135, 125, 159, 142, 121, 144, 137, 119 135, 137, 144, 142, 144, 139, 125, 132 117, 149, 119, 135, 151, 123, 119, 119 110, 135, 144, 130, 154, 144, 137, 144 135, 149, 139, 137, 139, 139, 144, 125 144, 130, 121, 121, 130, 135, 154, 128 121, 139, 166, 159, 130, 130, 132, 132 123, 128, 139, 137, 154, 130, 130, 144 125, 123, 135, 149, 123, 130, 139, 137 137, 128, 128, 128, 154, 119, 135, 125 149, 144, 135, 139, 144, 159, 146, 137 142, 146, 123, 125, 137, 100, 117, 149 159, 137, 112, 121, 125, 130, 130, 128 128, 132, 146, 114, 142, 151, 144, 125 151, 123, 123, 142, 154, 137, 125, 151 142, 149, 123, 139, 132, 132, 142, 137 114, 112, 144, 110, 130, 128, 144, 166 135, 132, 139, 159, 121, 139, 159, 144 164, 149, 121, 135, 146, 144, 161, 149 144, 149, 137, 144, 142, 169, 135, 156 144, 144, 144, 137, 130, 156, 172, 156 154, 164, 144, 172, 182, 161, 151, 169 185, 169, 172, 159, 164, 174, 161, 190 169, 154, 174, 159, 161, 177, 169, 190 174, 169, 161, 182, 169, 180, 166, 188 166, 172, 174, 156, 172, 161, 199, 139 182, 185, 164, 164, 164, 180, 156, 156 146, 142, 154, 156, 164, 190, 188, 144 166, 151, 166, 177, 154, 156, 185, 142 199, 161, 164, 154, 180, 166, 169, 169 166, 164, 151, 177, 149, 164, 182, 193 180, 164, 159, 159, 151, 185, 161, 166 164, 185, 188, 188, 182, 159, 199, 159 174, 146, 164, 161, 190, 174, 177, 185 182, 180, 164, 164, 202, 174, 180, 159 219, 182, 185, 222, 219, 228, 210, 219 210, 269, 246, 266, 237, 259, 246, 272 262, 237, 240, 246, 199, 202, 185, 202 196, 164, 204, 199, 199, 182, 169, 196 196, 180, 169, 188, 177, 188, 204, 213 156, 193, 180, 185, 174, 188, 193, 225 169, 188, 216, 188, 196, 199, 204, 196 185, 207, 196, 193, 202, 190, 213, 196 202, 193, 177, 185, 188, 193, 164, 196 199, 190, 188, 177, 185, 177, 166, 180 202, 166, 177, 180, 193, 161, 182, 190 164, 190, 190, 185, 177, 177, 188, 193 177, 188, 188, 159, 210, 193, 166, 166 182, 177, 199, 196, 188, 199, 174, 199 164, 188, 182, 177, 169, 188, 174, 193 190, 182, 164, 185, 193, 182, 202, 177 182, 188, 213, 159, 149, 182, 182, 164 199, 180, 193, 177, 177, 207, 185, 190 193, 154, 202, 202, 166, 193, 177, 177 213, 185, 185, 169, 207, 182, 182, 174 188, 190, 174, 185, 182, 202, 185, 213 213, 222, 190, 185, 174, 190, 207, 185 185, 182, 199, 193, 182, 196, 188, 180 185, 182, 177, 169, 193, 204, 202, 196 182, 172, 193, 196, 185, 219, 199, 199 204, 166, 199, 199, 185, 174, 182, 193 185, 202, 202, 199, 202, 202, 182, 196 188, 202, 182, 193, 207, 202, 207, 231 177, 216, 188, 177, 202, 172, 222, 222 219, 188, 207, 202, 169, 196, 159, 207 204, 210, 213, 228, 196, 202, 210, 207 210, 188, 234, 237, 207, 222, 202, 193 207, 204, 196, 213, 207, 193, 188, 199 207, 199, 222, 231, 207, 188, 185, 174 225, 216, 193, 204, 240, 219, 190, 207 210, 202, 225, 231, 262, 204, 225, 199 231, 193, 196, 216, 234, 213, 193, 222 185, 213, 207, 222, 202, 216, 213, 204 225, 216, 213, 207, 204, 225, 213, 193 202, 225, 228, 259, 234, 234, 231, 228 199, 219, 222, 250, 219, 204, 228, 231 228, 213, 196, 225, 237, 216, 243, 225 222, 246, 243, 234, 237, 243, 240, 259 253, 237, 216, 222, 243, 250, 228, 259 272, 269, 250, 253, 269, 279, 282, 246 256, 269, 279, 262, 272, 272, 259, 259 266, 313, 259, 272, 282, 282, 296, 289 303, 286, 306, 328, 320, 313, 320, 303 335, 350, 350, 380, 372, 380, 404, 458 449, 449, 441, 462, 462, 493, 534, 506 497, 506, 562, 615, 630, 676, 681, 713 671, 713, 795, 790, 807, 824, 784, 824 778, 790, 795, 773, 756, 762, 702, 713 660, 625, 625, 620, 566, 562, 502, 548 454, 471, 441, 441, 420, 428, 454, 404 404, 441, 412, 396, 372, 342, 361, 350 376, 357, 350, 335, 376, 346, 346, 350 292, 320, 342, 335, 303, 342, 306, 306 313, 317, 328, 303, 320, 299, 292, 289 276, 276, 256, 317, 299, 272, 289, 289 269, 320, 272, 292, 299, 286, 286, 286 306, 279, 272, 282, 246, 262, 225, 276 256, 276, 272, 259, 240, 286, 266, 246 286, 231, 246, 282, 228, 276, 276, 231 272, 222, 237, 256, 259, 231, 279, 266 246, 234, 253, 262, 256, 246, 256, 262 259, 237, 228, 256, 262, 259, 243, 262 266, 246, 246, 219, 269, 234, 256, 266 256, 234, 262, 246, 246, 262, 262, 276 299, 282, 243, 256, 266, 279, 296, 272 279, 289, 262, 276, 269, 269, 289, 286 303, 286, 313, 324, 320, 331, 342, 324 328, 369, 365, 380, 433, 428, 441, 445 493, 557, 576, 600, 655, 660, 671, 718 751, 756, 751, 713, 829, 697, 660, 620 600, 571, 515, 524, 520, 462, 454, 420 396, 412, 369, 424, 408, 433, 420, 400 372, 357, 361, 365, 339, 350, 317, 331 317, 303, 317, 303, 313, 296, 289, 289 310, 289, 272, 317, 276, 286, 282, 272 259, 292, 246, 303, 310, 276, 279, 317 272, 276, 303, 282, 279, 250, 282, 279 259, 286, 286, 303, 276, 279, 299, 272 303, 320, 299, 320, 346, 313, 313, 320 320, 339, 350, 369, 331, 331, 324, 346 317, 306, 313, 317, 269, 303, 296, 292 282, 306, 272, 286, 292, 269, 259, 269 253, 262, 279, 262, 237, 266, 292, 310 272, 276, 299, 262, 262, 299, 259, 269 279, 266, 272, 286, 259, 299, 299, 296 292, 272, 303, 299, 313, 292, 266, 286 231, 276, 282, 262, 272, 262, 259, 289 250, 234, 246, 269, 228, 234, 240, 253 266, 272, 259, 250, 246, 259, 250, 228 216, 228, 207, 234, 225, 240, 213, 250 231, 240, 222, 253, 240, 259, 234, 219 222, 240, 219, 225, 237, 204, 246, 228 228, 256, 250, 228, 246, 222, 246, 243 199, 237, 188, 219, 246, 243, 228, 228 256, 243, 222, 219, 213, 222, 222, 222 253, 210, 216, 196, 231, 225, 231, 225 216, 213, 213, 219, 225, 213, 237, 234 213, 219, 222, 182, 219, 213, 222, 210 222, 222, 225, 231, 243, 234, 210, 210 216, 196, 225, 253, 234, 202, 225, 234 216, 219, 202, 190, 253, 234, 231, 237 237, 225, 213, 216, 216, 228, 202, 234 246, 202, 243, 219, 202, 219, 207, 243 199, 210, 222, 225, 222, 234, 222, 231 202, 207, 213, 213, 243, 213, 210, 196 225, 216, 225, 222, 207, 213, 185, 240 228, 213, 196, 216, 216, 234, 213, 210 246, 213, 207, 253, 222, 199, 204, 250 188, 196, 243, 210, 216, 213, 202, 222 222, 286, 237, 228, 207, 231, 207, 231 199, 240, 228, 207, 213, 204, 190, 219 216, 202, 237, 228, 219, 193, 225,/