SampleIdent,928A 16H5 74-76,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-mar-1994 19:54,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 180, 180, 202, 228, 222, 228, 207, 190 188, 204, 196, 188, 193, 210, 222, 222 213, 193, 185, 180, 210, 193, 172, 190 185, 196, 188, 180, 185, 207, 188, 219 199, 202, 188, 188, 188, 185, 207, 172 202, 161, 190, 190, 177, 216, 180, 196 188, 204, 199, 210, 213, 193, 193, 190 207, 196, 182, 188, 207, 202, 210, 180 164, 177, 207, 182, 199, 182, 182, 193 193, 188, 185, 185, 185, 213, 190, 169 196, 190, 182, 185, 199, 207, 188, 188 199, 193, 193, 180, 180, 188, 207, 196 161, 190, 169, 161, 177, 182, 188, 222 213, 182, 182, 188, 182, 216, 193, 185 185, 177, 182, 174, 193, 204, 180, 207 193, 216, 182, 180, 202, 172, 207, 182 182, 196, 188, 185, 196, 177, 199, 193 207, 193, 199, 185, 174, 177, 216, 177 210, 193, 202, 219, 193, 188, 199, 204 213, 177, 174, 185, 182, 174, 182, 202 196, 202, 219, 188, 202, 190, 177, 185 149, 180, 196, 180, 177, 180, 188, 188 207, 188, 193, 231, 219, 169, 193, 207 182, 210, 166, 204, 210, 193, 196, 193 193, 202, 190, 196, 222, 204, 182, 216 185, 202, 216, 207, 207, 177, 210, 190 196, 199, 202, 204, 177, 204, 182, 185 207, 234, 204, 169, 216, 207, 196, 196 204, 204, 213, 180, 185, 207, 188, 190 213, 196, 193, 199, 202, 202, 222, 190 182, 207, 196, 182, 207, 213, 219, 204 188, 199, 196, 190, 180, 202, 202, 174 193, 188, 177, 228, 177, 196, 213, 188 237, 177, 204, 213, 196, 182, 207, 234 225, 210, 196, 177, 216, 216, 207, 219 219, 202, 222, 213, 185, 196, 204, 196 193, 210, 222, 222, 196, 210, 216, 213 222, 202, 225, 213, 196, 219, 210, 219 237, 213, 237, 222, 196, 190, 219, 190 228, 210, 202, 225, 213, 196, 182, 231 202, 204, 237, 246, 193, 207, 219, 210 228, 228, 207, 193, 228, 225, 228, 207 213, 225, 231, 228, 213, 237, 237, 225 222, 262, 250, 240, 219, 225, 253, 243 228, 262, 250, 243, 243, 237, 234, 216 272, 225, 256, 272, 210, 253, 259, 246 243, 250, 246, 256, 282, 237, 240, 256 266, 256, 262, 234, 243, 234, 243, 262 240, 253, 269, 240, 272, 262, 250, 250 243, 243, 269, 231, 240, 259, 250, 292 246, 237, 269, 234, 246, 259, 250, 246 246, 256, 276, 256, 262, 259, 269, 250 253, 243, 276, 246, 250, 237, 246, 256 243, 269, 262, 210, 234, 231, 231, 225 222, 225, 213, 225, 222, 237, 204, 240 231, 240, 225, 216, 213, 213, 199, 243 234, 207, 213, 216, 196, 193, 213, 196 219, 228, 202, 177, 193, 228, 225, 243 190, 210, 240, 237, 225, 202, 193, 222 202, 190, 228, 190, 213, 185, 225, 188 213, 216, 207, 190, 228, 207, 202, 216 196, 185, 199, 216, 213, 185, 193, 207 207, 188, 204, 207, 177, 202, 204, 213 216, 177, 188, 225, 166, 207, 216, 190 190, 180, 190, 180, 199, 193, 196, 193 185, 190, 231, 166, 188, 169, 159, 210 172, 188, 188, 199, 174, 199, 188, 182 188, 182, 199, 190, 207, 161, 196, 196 190, 193, 177, 196, 188, 207, 210, 193 180, 180, 144, 180, 177, 182, 185, 185 174, 193, 182, 180, 199, 169, 185, 196 169, 185, 174, 188, 174, 177, 193, 172 154, 188, 190, 204, 207, 207, 185, 177 177, 177, 169, 185, 174, 177, 180, 185 202, 182, 172, 204, 204, 202, 164, 196 190, 193, 182, 199, 188, 196, 199, 169 182, 185, 185, 199, 174, 193, 182, 159 196, 182, 185, 159, 196, 182, 174, 193 219, 204, 185, 164, 169, 188, 172, 202 199, 190, 182, 225, 216, 188, 204, 190 202, 185, 182, 204, 188, 225, 225, 219 219, 210, 210, 225, 216, 231, 202, 228 204, 237, 216, 202, 219, 216, 231, 250 237, 243, 246, 286, 299, 266, 299, 299 279, 342, 357, 353, 365, 346, 357, 376 408, 339, 361, 331, 303, 313, 317, 282 262, 237, 228, 222, 216, 182, 199, 193 172, 182, 204, 190, 169, 185, 166, 161 169, 149, 169, 166, 174, 169, 159, 154 151, 149, 164, 156, 154, 137, 164, 154 169, 156, 130, 135, 132, 144, 149, 144 142, 135, 156, 154, 142, 121, 154, 130 164, 151, 130, 144, 135, 142, 146, 139 119, 135, 132, 128, 144, 132, 125, 132 142, 132, 114, 137, 154, 130, 121, 104 128, 132, 125, 137, 117, 128, 117, 125 112, 119, 98, 88, 135, 106, 110, 114 125, 106, 108, 135, 108, 117, 112, 119 123, 123, 117, 137, 110, 123, 125, 114 123, 135, 117, 123, 112, 106, 121, 90 106, 104, 100, 108, 92, 125, 108, 130 102, 112, 106, 102, 108, 108, 112, 114 112, 110, 117, 104, 130, 106, 104, 128 98, 137, 121, 114, 114, 114, 104, 119 98, 112, 117, 117, 132, 106, 121, 121 117, 121, 112, 128, 94, 121, 119, 110 106, 117, 117, 119, 102, 112, 108, 106 119, 94, 121, 119, 132, 110, 117, 123 106, 106, 110, 112, 108, 108, 102, 96 123, 104, 121, 112, 96, 98, 132, 106 117, 121, 128, 117, 96, 139, 110, 123 112, 121, 100, 112, 135, 106, 112, 104 106, 108, 108, 121, 119, 114, 104, 112 117, 114, 104, 130, 119, 121, 102, 123 112, 100, 128, 110, 110, 132, 102, 139 114, 108, 125, 114, 117, 100, 130, 135 110, 125, 108, 123, 123, 144, 112, 112 125, 114, 121, 104, 114, 117, 130, 144 110, 130, 130, 130, 96, 137, 154, 112 125, 132, 132, 114, 123, 112, 139, 125 132, 132, 139, 135, 125, 125, 146, 146 123, 130, 130, 123, 139, 144, 139, 137 117, 130, 130, 151, 137, 135, 154, 154 159, 142, 166, 146, 146, 166, 159, 144 164, 156, 151, 146, 164, 174, 156, 188 169, 188, 196, 172, 207, 199, 190, 202 222, 222, 222, 216, 219, 259, 231, 272 250, 276, 289, 299, 306, 324, 331, 303 317, 328, 376, 365, 361, 380, 350, 365 408, 346, 350, 357, 357, 339, 346, 313 346, 331, 310, 320, 320, 306, 324, 320 269, 306, 286, 269, 253, 240, 207, 231 225, 193, 164, 172, 159, 169, 125, 144 128, 142, 151, 121, 132, 121, 128, 135 121, 139, 135, 121, 119, 130, 119, 125 125, 98, 130, 114, 112, 121, 117, 123 98, 121, 119, 114, 106, 137, 100, 110 102, 108, 100, 121, 117, 119, 106, 85 110, 125, 121, 100, 117, 110, 96, 114 102, 100, 121, 98, 104, 96, 100, 117 96, 86, 106, 102, 81, 110, 108, 92 104, 108, 90, 114, 98, 114, 119, 112 94, 96, 96, 106, 86, 92, 98, 94 112, 104, 100, 119, 96, 102, 121, 90 92, 90, 108, 100, 110, 92, 98, 92 106, 104, 112, 104, 108, 119, 102, 92 106, 88, 100, 102, 102, 123, 94, 98 96, 121, 100, 137, 117, 102, 121, 92 100, 92, 102, 110, 98, 104, 94, 81 104, 98, 100, 102, 85, 79, 102, 92 104, 79, 92, 96, 96, 81, 102, 92 92, 96, 96, 110, 92, 88, 94, 94 106, 100, 106, 110, 100, 104, 94, 98 90, 110, 110, 94, 94, 90, 100, 104 112, 92, 102, 90, 104, 117, 94, 96 77, 108, 90, 114, 96, 102, 90, 123 106, 100, 79, 98, 96, 106, 77, 88 85, 92, 90, 90, 102, 96, 102, 94 110, 90, 85, 117, 94, 117, 86, 110 100, 94, 86, 92, 94, 102, 110, 92 98, 110, 123, 96, 94, 71, 98, 90 94, 86, 106, 108, 94, 106, 100, 98 94, 96, 88, 92, 106, 92, 98, 88 94, 104, 96, 104, 92, 90, 117, 110 96, 108, 98, 92, 81, 85, 86, 85 100, 98, 86, 94, 88, 106, 114, 96 104, 100, 100, 110, 112, 98, 94, 94 92, 96, 106, 110, 88, 86, 102, 108 100, 108, 94, 114, 96, 102, 98, 106 119, 110, 104, 96, 121, 104, 104, 110 96, 110, 106, 100, 102, 96, 96, 100 102, 112, 112, 110, 110, 106, 98, 102 106, 110, 102, 114, 98, 77, 106, 104 106, 104, 98, 106, 96, 102, 117, 100 108, 88, 114, 104, 94, 106, 92, 112 102, 100, 92, 102, 92, 92, 88, 88 100, 100, 100, 104, 100, 117, 96, 92 130, 110, 98, 100, 114, 102, 96, 108 108, 119, 117, 114, 100, 114, 110, 96 92, 104, 110, 114, 100, 102, 98, 96 104, 117, 100, 112, 106, 102, 85, 114 96, 114, 108, 110, 106, 114, 102, 119 85, 98, 96, 106, 112, 108, 112, 104 123, 132, 98, 112, 104, 114, 86, 121 102, 110, 117, 114, 110, 96, 137, 125 108, 112, 106, 106, 106, 102, 96, 123 108, 112, 130, 106, 119, 121, 108, 123 121, 121, 119, 102, 128, 110, 100, 106 123, 100, 137, 108, 114, 132, 110, 121 121, 125, 123, 117, 132, 128, 128, 130 125, 112, 151, 128, 130, 144, 146, 139 151, 151, 130, 135, 125, 149, 142, 142 144, 142, 144, 156, 139, 139, 144, 172 144, 146, 142, 144, 144, 154, 174, 172 164, 146, 166, 174, 182, 190, 182, 199 216, 213, 210, 222, 292, 262, 282, 256 269, 282, 306, 282, 269, 299, 299, 289 231, 289, 234, 262, 219, 213, 213, 177 182, 193, 185, 159, 169, 180, 190, 149 156, 149, 164, 172, 177, 151, 156, 177 169, 164, 144, 137, 142, 146, 142, 144 130, 164, 159, 135, 144, 144, 146, 137 159, 139, 139, 144, 144, 151, 154, 137 144, 130, 149, 169, 151, 164, 154, 151 137, 137, 151, 132, 151, 149, 156, 137 144, 169, 142, 144, 139, 132, 161, 151 151, 159, 137, 156, 149, 142, 154, 166 149, 161, 159, 142, 139, 139, 142, 154 159, 146, 161, 166, 172, 174, 169, 166 174, 177, 142, 166, 180, 149, 188, 164 159, 164, 156, 156, 156, 128, 164, 139 137, 154, 139, 142, 149, 139, 130, 123 137, 144, 144, 137, 123, 151, 130, 135 114, 132, 130, 149, 121, 130, 121, 137 144, 144, 132, 123, 121, 130, 132, 128 154, 151, 144, 144, 146, 137, 130, 135 135, 149, 130, 137, 139, 149, 142, 159 139, 135, 137, 132, 144, 142, 161, 130 151, 144, 156, 135, 159, 135, 149, 142 132, 166, 166, 151, 161, 161, 137, 161 169, 174, 161, 169, 146, 154, 185, 166 164, 180, 182, 180, 199, 199, 185, 172 190, 174, 172, 174, 174, 190, 196, 166 190, 196, 199, 172, 207, 202, 166, 172 188, 182, 159, 190, 161, 172, 202, 177 199, 169, 185, 144, 190, 149, 185, 156 159, 169, 172, 164, 172, 174, 169, 182 169, 146, 166, 174, 185, 169, 182, 149 164, 190, 180, 151, 156, 169, 164, 177 125, 182, 149, 164, 164, 137, 144, 174 182, 164, 190, 182, 182, 177, 156, 174 188, 172, 169, 151, 172, 169, 177, 149 174, 196, 169, 188, 177, 166, 182, 185 199, 188, 177, 169, 202, 188, 196, 199 196, 225, 276, 243, 317, 350, 346, 320 350, 412, 350, 376, 369, 369, 328, 313 276, 299, 286, 286, 240, 237, 228, 202 156, 219, 204, 185, 196, 177, 207, 182 182, 188, 196, 177, 193, 161, 199, 166 174, 182, 177, 180, 166, 164, 164, 159 182, 166, 182, 199, 174, 177, 199, 185 182, 174, 166, 174, 159, 172, 149, 185 188, 185, 188, 188, 164, 172, 196, 166 177, 177, 161, 169, 180, 177, 180, 190 182, 172, 180, 169, 188, 188, 180, 196 174, 182, 164, 164, 164, 185, 177, 188 177, 174, 169, 169, 159, 182, 177, 182 161, 177, 190, 161, 193, 182, 174, 182 199, 166, 202, 151, 185, 177, 185, 193 196, 193, 172, 207, 193, 193, 182, 190 177, 169, 174, 177, 190, 180, 190, 185 169, 180, 185, 169, 182, 172, 199, 182 193, 199, 172, 196, 190, 164, 185, 188 177, 193, 196, 190, 188, 188, 225, 180 193, 196, 182, 177, 172, 154, 190, 177 169, 172, 190, 177, 177, 207, 188, 193 188, 182, 196, 219, 174, 193, 202, 188 169, 190, 185, 193, 177, 182, 185, 182 185, 202, 193, 222, 166, 199, 182, 190 177, 166, 204, 180, 185, 196, 177, 161 190, 196, 213, 207, 185, 182, 216, 188 207, 210, 207, 196, 216, 210, 190, 202 193, 199, 193, 210, 207, 174, 210, 199 202, 204, 202, 193, 188, 177, 219, 216 172, 182, 174, 193, 207, 193, 182, 182 193, 193, 180, 199, 210, 188, 188, 196 199, 182, 199, 196, 202, 202, 185, 190 188, 216, 228, 222, 182, 199, 210, 207 222, 228, 207, 237, 219, 219, 213, 237 262, 237, 243, 216, 216, 219, 204, 213 237, 246, 246, 222, 202, 243, 188, 219 225, 182, 177, 207, 213, 213, 190, 234 188, 219, 225, 207, 199, 237, 216, 228 228, 188, 207, 222, 216, 219, 237, 243 231, 213, 193, 199, 213, 225, 216, 228 216, 225, 193, 213, 237, 216, 219, 202 216, 225, 225, 210, 246, 210, 225, 262 228, 207, 219, 250, 207, 262, 219, 213 234, 210, 279, 250, 202, 253, 225, 256 222, 250, 219, 234, 253, 237, 234, 246 246, 222, 240, 231, 256, 228, 262, 243 225, 246, 243, 262, 250, 243, 299, 292 282, 259, 289, 266, 324, 272, 328, 313 296, 320, 353, 350, 324, 346, 324, 357 353, 392, 408, 408, 420, 458, 412, 416 441, 480, 462, 480, 471, 480, 428, 511 511, 445, 441, 437, 412, 404, 428, 441 408, 392, 396, 384, 376, 372, 346, 365 372, 339, 369, 392, 388, 369, 372, 357 392, 380, 365, 376, 392, 346, 339, 361 380, 339, 376, 396, 361, 353, 365, 320 306, 320, 303, 296, 328, 296, 335, 303 306, 276, 279, 282, 292, 299, 272, 282 276, 279, 276, 296, 256, 269, 266, 266 240, 279, 259, 250, 262, 243, 259, 262 279, 289, 234, 289, 253, 269, 272, 234 269, 228, 250, 243, 240, 250, 262, 246 231, 243, 262, 246, 266, 259, 272, 262 250, 231, 243, 250, 259, 246, 266, 266 259, 240, 269, 272, 246, 269, 256, 266 250, 246, 246, 266, 243, 286, 279, 266 240, 296, 246, 272, 256, 272, 262, 276 266, 272, 286, 240, 262, 266, 299, 262 256, 286, 259, 272, 276, 276, 279, 292 272, 324, 331, 320, 299, 320, 350, 317 331, 357, 369, 369, 396, 384, 437, 484 497, 524, 571, 635, 692, 790, 912, 980 992, 1102, 1197, 1232, 1354, 1406, 1482, 1436 1421, 1384, 1318, 1204, 1170, 1050, 1056, 999 900, 818, 807, 751, 676, 681, 630, 586 576, 557, 538, 506, 497, 497, 480, 484 416, 454, 384, 408, 392, 376, 369, 372 357, 369, 328, 353, 353, 331, 303, 313 350, 350, 306, 324, 335, 320, 317, 317 324, 292, 328, 303, 269, 299, 313, 292 299, 306, 296, 306, 324, 320, 289, 357 289, 296, 339, 296, 306, 320, 313, 357 357, 328, 331, 331, 350, 361, 331, 339 324, 339, 339, 331, 350, 328, 342, 289 320, 313, 331, 306, 313, 292, 279, 317 313, 279, 317, 306, 299, 259, 324, 279 313, 289, 286, 331, 282, 282, 303, 296 310, 299, 289, 289, 262, 350, 310, 289 335, 313, 361, 384, 376, 361, 392, 361 372, 369, 384, 346, 361, 313, 313, 317 310, 289, 310, 303, 286, 256, 279, 259 286, 269, 279, 269, 272, 282, 243, 256 234, 243, 276, 269, 259, 237, 279, 228 266, 207, 240, 243, 240, 237, 237, 259 259, 237, 234, 228, 259, 228, 234, 231 237, 272, 210, 243, 225, 237, 250, 228 213, 231, 228, 225, 250, 253, 210, 246 256, 234, 231, 246, 231, 234, 228, 256 231, 234, 253, 213, 243, 272, 222, 256 250, 240, 202, 250, 219, 246, 216, 199 210, 228, 216, 253, 222, 231, 246, 240 256, 225, 246, 225, 231, 246, 213, 240 250, 222, 222, 246, 259, 225, 225, 250 204, 228, 231, 269, 207, 243, 228, 231 237, 243, 228, 246, 207, 234, 246, 213 216, 213, 225, 216, 231, 219, 222, 234 225, 202, 243, 237, 213, 234, 243, 243 219, 210, 237, 240, 213, 210, 225, 216 213, 210, 240, 228, 250, 231, 199, 190 240, 190, 256, 216, 225, 216, 210, 204 222, 222, 246, 228, 216, 216, 213, 234 250, 231, 213, 225, 228, 240, 231, 246 237, 231, 222, 259, 228, 250, 240, 250 246, 222, 207, 210, 225, 234, 225, 222 240, 240, 234, 210, 219, 228, 202,/