SampleIdent,928A 17H1 72-74,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-mar-1994 20:53,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 142, 193, 169, 182, 174, 172, 169, 159 169, 188, 161, 161, 137, 166, 169, 159 161, 154, 164, 164, 156, 159, 177, 142 159, 180, 161, 164, 154, 154, 146, 139 159, 161, 169, 151, 159, 146, 161, 139 174, 154, 159, 149, 164, 174, 164, 151 161, 166, 166, 149, 185, 154, 151, 154 161, 135, 177, 146, 156, 164, 156, 180 159, 151, 169, 177, 154, 151, 190, 154 174, 156, 154, 174, 166, 159, 161, 172 202, 169, 149, 154, 149, 159, 185, 174 174, 154, 174, 177, 159, 161, 169, 164 159, 164, 154, 182, 188, 172, 169, 166 177, 180, 159, 169, 154, 180, 177, 159 159, 174, 164, 159, 164, 196, 185, 180 177, 154, 156, 182, 188, 180, 193, 154 188, 188, 164, 193, 174, 202, 199, 180 169, 193, 177, 185, 169, 199, 172, 177 185, 193, 182, 202, 169, 207, 225, 204 196, 185, 166, 180, 166, 177, 193, 182 202, 164, 207, 177, 180, 182, 188, 204 199, 193, 172, 182, 202, 190, 188, 196 207, 188, 172, 196, 216, 174, 231, 164 182, 213, 180, 185, 204, 210, 216, 207 202, 177, 202, 202, 199, 207, 204, 199 216, 182, 216, 190, 207, 207, 228, 222 190, 196, 207, 202, 199, 202, 222, 193 177, 188, 216, 207, 210, 228, 207, 204 207, 213, 196, 219, 213, 207, 196, 219 225, 202, 207, 219, 204, 210, 202, 213 207, 199, 243, 210, 219, 213, 193, 225 219, 207, 219, 231, 228, 207, 202, 202 216, 202, 202, 228, 256, 216, 240, 199 216, 234, 240, 204, 228, 202, 228, 196 225, 250, 219, 210, 216, 225, 259, 228 231, 202, 216, 210, 222, 199, 210, 240 210, 234, 204, 228, 246, 234, 240, 219 207, 250, 210, 219, 228, 228, 225, 216 246, 240, 219, 207, 253, 228, 237, 225 237, 240, 253, 234, 246, 240, 243, 250 234, 259, 246, 240, 234, 228, 243, 231 250, 269, 243, 269, 234, 243, 253, 231 246, 228, 250, 246, 237, 269, 231, 237 286, 269, 272, 253, 256, 237, 272, 237 246, 282, 266, 266, 253, 282, 262, 266 246, 276, 262, 250, 276, 272, 256, 286 292, 240, 276, 282, 266, 266, 262, 286 286, 276, 272, 292, 289, 276, 282, 272 253, 279, 269, 266, 279, 296, 253, 276 276, 240, 272, 253, 296, 276, 286, 279 269, 253, 279, 262, 262, 237, 286, 292 299, 310, 282, 269, 269, 292, 286, 299 286, 292, 272, 266, 292, 272, 276, 289 299, 253, 286, 266, 250, 272, 246, 269 262, 250, 262, 256, 246, 292, 253, 256 237, 250, 256, 219, 207, 272, 253, 213 276, 240, 228, 237, 259, 240, 219, 240 210, 219, 228, 228, 219, 222, 231, 199 207, 243, 256, 222, 219, 210, 228, 237 216, 219, 207, 222, 225, 204, 207, 202 234, 228, 246, 231, 228, 213, 199, 228 234, 213, 228, 188, 202, 222, 216, 231 196, 216, 202, 216, 210, 207, 246, 207 219, 207, 213, 202, 207, 219, 213, 210 210, 213, 250, 234, 219, 207, 180, 237 188, 207, 234, 204, 193, 185, 210, 222 185, 193, 213, 225, 190, 199, 231, 199 199, 172, 216, 169, 202, 202, 204, 182 210, 196, 204, 202, 185, 180, 174, 193 169, 202, 190, 193, 204, 199, 193, 188 196, 202, 213, 177, 196, 207, 219, 177 216, 188, 219, 202, 234, 216, 177, 219 213, 161, 177, 202, 182, 190, 182, 210 202, 213, 190, 185, 185, 202, 193, 225 174, 177, 185, 188, 180, 190, 182, 204 199, 196, 228, 202, 204, 188, 190, 169 193, 199, 225, 210, 196, 190, 225, 207 193, 207, 164, 193, 204, 213, 207, 216 193, 190, 164, 193, 185, 196, 207, 207 185, 193, 185, 185, 228, 225, 207, 193 210, 216, 216, 210, 196, 216, 202, 219 231, 250, 204, 228, 237, 237, 240, 237 256, 250, 246, 250, 266, 250, 250, 282 262, 279, 262, 256, 289, 292, 306, 320 369, 335, 372, 357, 357, 369, 339, 369 376, 365, 353, 353, 320, 303, 306, 276 269, 259, 237, 228, 207, 231, 216, 196 185, 188, 180, 185, 166, 182, 177, 193 193, 185, 180, 188, 174, 185, 177, 177 159, 149, 151, 144, 164, 169, 144, 154 159, 164, 151, 146, 135, 137, 132, 146 149, 132, 121, 137, 144, 125, 135, 132 130, 144, 149, 154, 166, 144, 146, 159 144, 130, 123, 112, 146, 156, 137, 135 137, 144, 130, 121, 132, 132, 137, 130 119, 135, 139, 125, 149, 112, 117, 144 128, 123, 108, 123, 106, 123, 137, 135 121, 121, 144, 132, 117, 114, 137, 146 130, 112, 112, 137, 130, 130, 121, 108 123, 121, 139, 121, 114, 110, 130, 119 110, 121, 119, 112, 110, 121, 128, 112 119, 110, 114, 98, 114, 137, 125, 112 117, 123, 119, 119, 114, 117, 119, 125 123, 110, 112, 114, 112, 128, 114, 132 128, 121, 117, 137, 123, 114, 92, 121 121, 123, 110, 123, 117, 112, 117, 119 98, 119, 106, 130, 130, 102, 117, 114 123, 119, 94, 117, 112, 106, 123, 123 108, 114, 135, 144, 106, 100, 108, 130 108, 130, 90, 117, 117, 117, 112, 104 117, 121, 112, 119, 119, 106, 128, 108 114, 128, 108, 98, 119, 125, 117, 128 121, 106, 121, 110, 112, 137, 130, 100 117, 121, 110, 123, 104, 123, 142, 112 117, 121, 135, 146, 106, 112, 119, 119 108, 125, 79, 106, 144, 106, 144, 123 112, 121, 125, 132, 114, 121, 112, 100 121, 137, 121, 130, 130, 119, 130, 123 119, 121, 119, 114, 149, 135, 128, 137 125, 108, 137, 132, 123, 137, 146, 130 123, 144, 139, 137, 151, 128, 135, 121 161, 142, 154, 135, 149, 146, 130, 130 125, 169, 142, 164, 144, 151, 154, 151 156, 161, 174, 146, 166, 190, 146, 182 149, 169, 190, 159, 188, 174, 185, 188 177, 199, 213, 222, 207, 207, 256, 231 243, 240, 231, 243, 253, 259, 299, 286 289, 320, 306, 306, 310, 313, 324, 331 346, 384, 357, 392, 353, 392, 400, 339 380, 400, 335, 361, 350, 365, 328, 353 324, 335, 317, 328, 313, 306, 282, 317 292, 269, 286, 276, 279, 240, 213, 213 188, 199, 188, 180, 188, 164, 166, 144 164, 164, 137, 151, 154, 139, 137, 121 130, 117, 142, 137, 119, 117, 123, 94 110, 130, 108, 130, 128, 114, 119, 112 112, 112, 125, 125, 110, 119, 96, 100 119, 110, 123, 121, 98, 106, 121, 90 112, 128, 110, 104, 119, 112, 86, 102 106, 117, 104, 123, 119, 108, 88, 110 98, 90, 108, 125, 117, 112, 98, 106 110, 102, 96, 106, 92, 114, 110, 92 108, 106, 96, 123, 92, 102, 100, 96 132, 108, 94, 114, 100, 121, 112, 96 94, 106, 108, 104, 123, 125, 117, 121 117, 128, 96, 108, 119, 121, 110, 98 117, 85, 112, 112, 110, 92, 102, 104 98, 94, 106, 108, 96, 98, 117, 125 108, 94, 104, 112, 106, 104, 117, 100 96, 106, 96, 123, 114, 92, 112, 102 112, 104, 108, 98, 100, 110, 90, 104 96, 94, 100, 96, 98, 102, 106, 100 119, 100, 114, 106, 100, 83, 100, 104 94, 90, 121, 108, 110, 114, 94, 86 98, 121, 92, 88, 96, 117, 94, 100 104, 106, 121, 121, 102, 92, 98, 102 92, 110, 100, 92, 98, 96, 98, 104 86, 108, 94, 86, 94, 92, 92, 85 90, 104, 96, 110, 88, 102, 94, 121 123, 94, 92, 98, 106, 108, 100, 96 98, 92, 83, 125, 114, 92, 77, 98 110, 102, 102, 96, 104, 106, 114, 96 94, 83, 92, 100, 102, 102, 123, 121 110, 85, 98, 88, 108, 100, 110, 102 100, 100, 85, 112, 102, 66, 112, 98 117, 110, 98, 106, 98, 106, 98, 117 106, 114, 102, 96, 108, 100, 104, 106 119, 98, 112, 114, 112, 112, 110, 104 112, 98, 108, 98, 112, 114, 106, 114 106, 94, 119, 110, 114, 92, 108, 117 117, 98, 98, 106, 114, 102, 128, 110 104, 90, 88, 119, 102, 100, 106, 100 106, 108, 114, 112, 117, 119, 86, 98 108, 117, 121, 108, 114, 130, 123, 130 110, 100, 90, 96, 106, 108, 102, 104 106, 88, 94, 117, 108, 112, 110, 110 108, 117, 100, 98, 104, 117, 121, 121 96, 79, 104, 110, 106, 98, 121, 106 108, 121, 121, 104, 108, 110, 112, 104 117, 106, 106, 100, 125, 125, 130, 121 100, 102, 112, 119, 106, 108, 119, 102 119, 100, 100, 117, 104, 114, 100, 112 108, 119, 110, 119, 96, 112, 125, 104 112, 132, 94, 110, 121, 102, 121, 119 114, 130, 112, 117, 110, 110, 100, 130 119, 125, 98, 102, 130, 121, 137, 121 121, 112, 108, 128, 125, 125, 130, 130 119, 137, 110, 119, 114, 128, 121, 110 146, 112, 135, 121, 149, 137, 125, 130 130, 144, 144, 149, 132, 119, 130, 142 130, 121, 114, 117, 149, 132, 130, 142 135, 154, 154, 137, 156, 142, 156, 154 142, 137, 142, 130, 149, 169, 151, 154 151, 144, 146, 142, 159, 166, 156, 166 193, 159, 193, 193, 202, 207, 185, 219 222, 250, 246, 276, 266, 259, 276, 250 313, 279, 276, 320, 313, 296, 292, 269 243, 253, 253, 246, 210, 222, 210, 204 219, 210, 190, 169, 174, 161, 177, 159 144, 154, 164, 177, 177, 144, 161, 149 177, 159, 159, 149, 156, 142, 156, 149 137, 146, 161, 151, 137, 144, 149, 144 166, 166, 137, 177, 135, 144, 144, 139 149, 166, 154, 142, 146, 166, 144, 137 161, 164, 137, 151, 144, 154, 159, 154 130, 144, 149, 154, 166, 144, 146, 154 159, 142, 132, 154, 139, 159, 149, 144 156, 151, 123, 161, 154, 169, 156, 151 144, 159, 161, 146, 154, 144, 177, 166 149, 164, 164, 174, 159, 161, 169, 169 182, 142, 180, 149, 149, 154, 149, 154 166, 137, 132, 166, 123, 117, 144, 130 166, 156, 149, 151, 149, 137, 130, 139 149, 144, 135, 135, 146, 144, 130, 151 151, 137, 137, 135, 130, 149, 121, 130 135, 137, 142, 154, 135, 144, 164, 154 144, 144, 132, 151, 146, 146, 132, 149 137, 132, 135, 151, 128, 146, 139, 149 146, 142, 154, 164, 161, 142, 149, 154 177, 144, 174, 161, 149, 164, 149, 166 164, 154, 182, 182, 149, 190, 159, 174 182, 174, 172, 180, 185, 180, 204, 154 174, 174, 180, 159, 193, 188, 188, 159 172, 193, 177, 193, 188, 169, 185, 182 202, 196, 177, 196, 174, 180, 164, 180 193, 196, 169, 188, 169, 159, 169, 182 159, 149, 164, 172, 193, 177, 190, 151 188, 146, 159, 151, 159, 177, 164, 166 159, 161, 177, 156, 144, 169, 154, 142 159, 161, 172, 182, 166, 139, 188, 188 174, 169, 139, 174, 174, 182, 166, 185 177, 161, 174, 166, 159, 180, 177, 177 188, 202, 169, 161, 169, 151, 193, 174 190, 193, 190, 196, 222, 202, 234, 246 262, 286, 279, 269, 299, 303, 369, 339 286, 346, 350, 342, 335, 328, 292, 335 313, 276, 279, 286, 259, 286, 240, 240 250, 240, 213, 222, 219, 237, 216, 202 207, 225, 202, 228, 196, 199, 219, 216 199, 199, 202, 207, 234, 234, 204, 240 225, 188, 216, 188, 213, 196, 174, 216 222, 177, 193, 188, 185, 180, 177, 199 193, 193, 199, 180, 199, 196, 159, 196 202, 180, 180, 161, 196, 177, 185, 190 164, 164, 177, 199, 196, 182, 182, 166 188, 182, 177, 172, 174, 202, 182, 166 172, 180, 182, 166, 177, 177, 164, 177 185, 164, 164, 219, 161, 169, 156, 172 188, 180, 174, 204, 193, 180, 196, 188 193, 202, 199, 222, 193, 196, 174, 219 174, 174, 185, 188, 174, 204, 207, 188 193, 204, 182, 180, 182, 172, 174, 193 182, 172, 207, 196, 164, 185, 169, 182 204, 202, 188, 193, 182, 182, 188, 210 193, 185, 204, 190, 169, 193, 169, 196 207, 207, 149, 204, 188, 193, 188, 177 174, 199, 164, 193, 190, 161, 210, 222 193, 185, 188, 210, 202, 177, 193, 193 207, 204, 199, 207, 188, 190, 199, 188 159, 182, 196, 172, 202, 213, 199, 196 188, 180, 196, 159, 225, 193, 188, 207 188, 210, 196, 207, 213, 196, 207, 228 225, 177, 204, 196, 207, 193, 188, 199 199, 185, 204, 222, 222, 196, 216, 222 210, 196, 213, 204, 196, 216, 196, 188 219, 196, 210, 228, 210, 219, 202, 222 240, 213, 216, 225, 228, 210, 222, 222 210, 199, 246, 228, 228, 228, 231, 225 237, 225, 222, 225, 225, 234, 259, 243 240, 219, 243, 204, 237, 240, 225, 231 259, 256, 180, 234, 225, 216, 234, 253 193, 234, 237, 219, 207, 228, 225, 228 207, 216, 204, 213, 207, 228, 234, 196 240, 222, 250, 202, 234, 237, 243, 234 228, 193, 234, 228, 213, 219, 219, 207 219, 231, 213, 202, 228, 222, 240, 237 234, 219, 231, 216, 228, 231, 231, 228 231, 234, 243, 222, 243, 237, 225, 237 266, 240, 228, 213, 256, 240, 256, 231 240, 259, 246, 253, 269, 269, 237, 253 259, 231, 262, 262, 246, 246, 253, 250 282, 246, 246, 253, 299, 259, 313, 276 286, 299, 317, 292, 279, 317, 331, 324 313, 328, 339, 372, 342, 346, 388, 361 396, 380, 445, 449, 424, 424, 467, 458 506, 506, 493, 475, 502, 493, 502, 475 497, 462, 488, 502, 467, 471, 424, 380 404, 372, 404, 404, 361, 369, 384, 376 369, 365, 396, 380, 388, 380, 372, 369 388, 400, 392, 369, 365, 350, 384, 361 372, 380, 420, 369, 342, 353, 342, 335 350, 317, 339, 324, 339, 324, 262, 328 296, 250, 246, 313, 292, 299, 306, 282 276, 292, 276, 272, 266, 296, 292, 282 279, 292, 276, 266, 289, 256, 276, 282 269, 282, 286, 286, 269, 269, 299, 282 286, 234, 259, 276, 231, 282, 225, 253 256, 240, 282, 262, 262, 262, 266, 276 269, 253, 262, 246, 225, 259, 276, 282 240, 269, 256, 240, 243, 246, 259, 276 272, 272, 286, 266, 276, 266, 262, 250 272, 276, 269, 276, 262, 231, 266, 266 282, 269, 259, 279, 266, 299, 279, 256 231, 296, 266, 276, 282, 292, 342, 292 324, 320, 331, 306, 324, 310, 350, 320 357, 353, 388, 396, 392, 462, 475, 484 529, 581, 620, 645, 729, 818, 949, 955 1063, 1102, 1204, 1246, 1354, 1347, 1376, 1391 1391, 1303, 1225, 1136, 1082, 1076, 955, 918 784, 745, 762, 734, 676, 640, 655, 586 543, 581, 552, 529, 502, 493, 471, 458 400, 392, 392, 416, 353, 400, 357, 331 350, 335, 365, 320, 342, 339, 357, 339 350, 357, 328, 328, 328, 313, 303, 335 320, 306, 320, 303, 306, 299, 292, 292 286, 292, 313, 286, 299, 303, 328, 320 313, 324, 299, 313, 299, 310, 310, 328 310, 328, 342, 353, 353, 339, 342, 342 350, 339, 369, 335, 335, 353, 320, 289 324, 306, 303, 303, 299, 299, 296, 272 292, 303, 310, 296, 303, 299, 313, 286 317, 269, 276, 296, 306, 328, 306, 296 317, 299, 313, 317, 306, 324, 339, 357 372, 328, 339, 328, 372, 339, 361, 335 317, 369, 306, 299, 339, 331, 320, 276 313, 282, 299, 306, 272, 299, 282, 256 276, 246, 262, 276, 256, 296, 243, 289 253, 250, 243, 243, 276, 240, 243, 269 259, 250, 276, 256, 259, 266, 262, 266 269, 237, 259, 237, 256, 231, 219, 234 262, 240, 234, 237, 269, 234, 234, 234 237, 237, 259, 213, 266, 234, 240, 246 222, 262, 234, 228, 246, 231, 216, 240 237, 231, 202, 222, 234, 234, 222, 243 240, 246, 225, 237, 256, 225, 234, 253 228, 240, 246, 240, 256, 219, 243, 190 250, 213, 240, 240, 231, 225, 219, 210 240, 234, 234, 237, 234, 250, 250, 231 234, 228, 256, 225, 237, 240, 256, 225 219, 231, 207, 234, 225, 246, 246, 253 225, 216, 228, 240, 216, 228, 231, 243 246, 222, 188, 219, 210, 256, 216, 210 222, 231, 219, 202, 202, 240, 228, 234 210, 225, 240, 219, 243, 216, 231, 234 202, 210, 222, 240, 219, 234, 213, 196 225, 216, 259, 231, 199, 202, 243, 234 240, 216, 250, 234, 234, 231, 216, 231 240, 262, 243, 222, 240, 231, 259, 219 219, 228, 231, 256, 234, 250, 228, 243 222, 240, 216, 213, 237, 222, 216,/