SampleIdent,928A 19H3 82-84,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,15-mar-1994 1:48,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 177, 169, 172, 164, 161, 161, 166, 123 149, 144, 139, 164, 161, 149, 169, 161 164, 130, 142, 149, 156, 132, 146, 149 146, 149, 161, 135, 137, 146, 137, 154 135, 154, 146, 188, 154, 132, 139, 154 154, 146, 144, 135, 123, 123, 128, 151 125, 125, 128, 139, 128, 142, 151, 128 128, 123, 132, 149, 151, 137, 119, 142 135, 139, 156, 174, 164, 128, 161, 154 174, 137, 159, 156, 159, 156, 149, 182 154, 144, 199, 164, 188, 182, 196, 177 182, 182, 174, 185, 185, 207, 199, 182 207, 228, 180, 202, 174, 177, 202, 177 164, 190, 185, 182, 196, 204, 166, 174 185, 185, 159, 169, 199, 196, 188, 180 202, 177, 185, 202, 177, 210, 166, 190 196, 193, 193, 196, 185, 188, 202, 213 188, 185, 199, 193, 196, 204, 193, 207 213, 199, 180, 172, 188, 199, 210, 216 188, 219, 207, 190, 216, 204, 177, 213 216, 193, 219, 196, 213, 185, 196, 161 199, 213, 213, 199, 199, 180, 222, 210 204, 204, 219, 202, 196, 207, 216, 231 213, 193, 164, 213, 231, 228, 222, 204 199, 219, 222, 190, 202, 196, 216, 213 202, 231, 204, 207, 213, 210, 213, 202 210, 228, 222, 188, 207, 219, 193, 207 199, 228, 259, 228, 213, 222, 207, 228 219, 234, 216, 207, 216, 231, 228, 246 225, 228, 225, 213, 199, 240, 219, 199 240, 219, 225, 231, 228, 219, 225, 237 231, 234, 237, 222, 213, 234, 210, 225 219, 222, 222, 225, 219, 216, 231, 216 210, 222, 216, 225, 231, 237, 222, 213 222, 276, 222, 231, 237, 225, 246, 253 237, 234, 219, 213, 234, 222, 240, 243 246, 228, 240, 228, 222, 243, 237, 240 250, 237, 243, 225, 234, 234, 237, 253 240, 234, 246, 256, 222, 262, 262, 256 222, 240, 259, 250, 216, 282, 250, 266 231, 262, 256, 256, 269, 246, 276, 243 234, 266, 250, 234, 234, 259, 262, 250 253, 266, 250, 253, 259, 259, 259, 259 276, 259, 250, 256, 279, 259, 296, 259 266, 282, 266, 286, 262, 276, 276, 266 250, 262, 240, 276, 250, 282, 262, 256 266, 256, 262, 276, 266, 272, 272, 286 286, 279, 286, 262, 272, 282, 269, 240 262, 279, 269, 272, 256, 266, 282, 256 256, 286, 243, 228, 272, 269, 262, 262 296, 256, 246, 269, 243, 256, 259, 262 253, 279, 279, 234, 259, 253, 266, 246 240, 253, 250, 250, 259, 243, 253, 246 219, 231, 243, 250, 253, 222, 225, 237 253, 237, 253, 237, 231, 210, 250, 216 250, 246, 243, 231, 237, 243, 243, 237 213, 222, 262, 219, 219, 250, 219, 202 234, 237, 250, 216, 246, 225, 228, 228 272, 193, 231, 213, 210, 240, 210, 234 243, 216, 237, 234, 182, 240, 193, 213 199, 180, 202, 216, 190, 219, 213, 219 188, 207, 210, 199, 199, 237, 207, 193 202, 225, 228, 199, 222, 213, 228, 182 207, 190, 219, 177, 190, 225, 219, 193 193, 219, 196, 213, 196, 207, 193, 180 210, 182, 196, 177, 188, 161, 188, 185 202, 207, 156, 207, 213, 207, 185, 199 185, 161, 210, 210, 177, 204, 172, 188 199, 172, 199, 180, 174, 185, 199, 164 190, 182, 190, 190, 182, 228, 174, 185 199, 188, 149, 182, 204, 174, 196, 174 202, 159, 166, 193, 202, 193, 199, 166 199, 182, 164, 161, 169, 190, 199, 190 174, 180, 182, 182, 154, 202, 193, 159 193, 196, 185, 204, 159, 190, 193, 182 169, 154, 164, 172, 164, 190, 161, 185 188, 193, 193, 169, 180, 190, 190, 177 174, 174, 199, 166, 161, 196, 164, 169 169, 199, 190, 180, 204, 216, 164, 196 196, 188, 185, 182, 166, 193, 199, 188 188, 177, 219, 182, 202, 193, 193, 190 174, 174, 159, 166, 193, 193, 156, 196 169, 204, 185, 190, 185, 169, 196, 190 196, 219, 180, 222, 202, 213, 190, 202 202, 190, 210, 182, 188, 196, 202, 219 193, 190, 188, 185, 199, 199, 193, 180 159, 177, 169, 177, 185, 169, 149, 172 144, 174, 154, 156, 159, 137, 161, 166 149, 164, 135, 139, 146, 149, 149, 135 151, 146, 154, 144, 177, 144, 174, 164 137, 130, 149, 128, 146, 135, 132, 142 121, 144, 137, 137, 108, 142, 114, 132 137, 132, 137, 135, 119, 121, 149, 132 146, 123, 161, 125, 121, 149, 119, 125 144, 132, 139, 104, 123, 139, 128, 119 121, 132, 128, 125, 130, 119, 121, 130 144, 135, 137, 119, 130, 139, 139, 117 121, 142, 128, 117, 94, 135, 108, 121 102, 121, 119, 130, 110, 106, 96, 130 123, 125, 114, 123, 110, 119, 121, 110 121, 146, 125, 117, 100, 125, 130, 121 128, 125, 106, 112, 104, 112, 106, 106 137, 119, 90, 96, 100, 110, 92, 110 114, 110, 114, 123, 112, 108, 98, 108 117, 132, 104, 137, 117, 119, 119, 130 119, 121, 108, 121, 96, 114, 104, 112 125, 102, 121, 117, 135, 117, 110, 96 112, 104, 106, 117, 112, 125, 119, 121 128, 123, 110, 130, 102, 121, 102, 125 112, 123, 108, 132, 125, 102, 119, 117 114, 108, 119, 132, 128, 110, 108, 128 114, 112, 106, 112, 114, 104, 112, 104 132, 123, 130, 121, 130, 123, 112, 108 119, 125, 144, 108, 119, 125, 135, 121 123, 125, 119, 137, 137, 137, 119, 108 121, 100, 142, 132, 121, 123, 112, 128 144, 139, 110, 100, 132, 121, 108, 135 149, 146, 137, 128, 130, 149, 128, 121 123, 146, 114, 164, 123, 146, 123, 144 132, 137, 137, 149, 174, 142, 139, 161 164, 188, 151, 172, 156, 154, 174, 159 156, 188, 164, 188, 151, 180, 161, 164 166, 204, 177, 159, 199, 204, 164, 177 164, 196, 202, 196, 231, 231, 231, 234 213, 213, 250, 219, 225, 259, 269, 240 279, 299, 292, 292, 306, 299, 313, 320 331, 346, 372, 376, 392, 404, 404, 392 392, 437, 384, 493, 484, 475, 497, 502 548, 562, 524, 529, 502, 543, 520, 488 497, 484, 484, 437, 475, 400, 420, 365 342, 342, 342, 313, 328, 289, 262, 250 266, 246, 213, 240, 199, 222, 210, 216 169, 207, 185, 188, 188, 169, 177, 156 156, 149, 149, 185, 149, 123, 164, 135 144, 149, 149, 123, 128, 137, 144, 128 125, 135, 139, 146, 128, 137, 117, 117 135, 119, 128, 119, 112, 102, 112, 110 106, 132, 119, 128, 112, 117, 123, 100 110, 108, 98, 108, 117, 110, 123, 121 112, 121, 108, 112, 90, 104, 86, 100 108, 121, 102, 94, 92, 100, 110, 100 104, 102, 98, 96, 121, 108, 110, 86 108, 104, 106, 102, 98, 123, 100, 108 117, 92, 94, 88, 90, 102, 110, 76 96, 100, 102, 98, 130, 77, 106, 108 106, 112, 104, 92, 112, 100, 102, 106 104, 106, 110, 96, 114, 112, 88, 121 106, 104, 123, 102, 110, 100, 86, 100 106, 119, 108, 94, 114, 128, 94, 114 114, 98, 98, 92, 92, 88, 112, 100 117, 114, 98, 98, 114, 102, 86, 92 100, 100, 90, 96, 98, 100, 102, 94 92, 96, 106, 102, 110, 108, 100, 88 100, 106, 104, 90, 106, 117, 98, 88 117, 96, 96, 108, 85, 90, 104, 98 85, 108, 94, 83, 102, 114, 83, 98 94, 110, 110, 104, 98, 104, 90, 92 92, 114, 90, 108, 94, 96, 100, 104 108, 96, 104, 88, 108, 83, 100, 117 102, 88, 88, 117, 104, 90, 117, 110 94, 100, 96, 104, 108, 108, 85, 85 92, 92, 121, 104, 98, 98, 96, 114 108, 110, 112, 108, 104, 86, 125, 83 108, 83, 104, 96, 102, 98, 96, 88 102, 83, 98, 96, 104, 98, 123, 106 96, 102, 112, 96, 100, 114, 100, 96 96, 88, 110, 110, 106, 86, 98, 106 98, 106, 88, 106, 90, 86, 102, 102 114, 102, 100, 98, 90, 108, 114, 102 102, 102, 104, 112, 94, 98, 114, 92 108, 106, 121, 117, 85, 100, 106, 86 108, 106, 98, 104, 100, 110, 98, 104 119, 114, 102, 121, 102, 81, 100, 117 114, 108, 92, 110, 117, 110, 96, 117 104, 98, 106, 88, 108, 96, 106, 88 106, 104, 114, 110, 125, 119, 108, 104 94, 108, 117, 112, 106, 108, 132, 121 102, 108, 112, 104, 110, 108, 100, 108 104, 112, 121, 119, 90, 86, 94, 102 112, 106, 102, 112, 94, 119, 106, 117 119, 98, 108, 104, 112, 104, 100, 110 98, 108, 108, 98, 104, 119, 123, 132 100, 117, 104, 98, 130, 112, 100, 112 102, 100, 117, 117, 130, 114, 106, 123 117, 94, 112, 128, 106, 132, 119, 102 110, 94, 110, 104, 119, 102, 102, 90 117, 137, 130, 125, 121, 142, 121, 123 106, 108, 135, 112, 112, 121, 121, 146 119, 117, 142, 100, 130, 119, 117, 119 130, 121, 123, 125, 137, 125, 102, 123 139, 119, 119, 130, 121, 123, 139, 123 149, 132, 135, 117, 128, 123, 121, 123 154, 114, 137, 132, 142, 146, 144, 123 149, 121, 144, 132, 128, 132, 132, 166 114, 142, 142, 123, 132, 149, 146, 154 164, 142, 149, 139, 149, 142, 144, 139 164, 144, 149, 169, 159, 156, 144, 164 164, 169, 149, 142, 164, 154, 151, 161 149, 164, 137, 156, 161, 132, 144, 128 142, 128, 144, 144, 161, 130, 149, 132 128, 123, 149, 125, 151, 123, 159, 130 132, 139, 146, 125, 125, 142, 142, 139 128, 137, 139, 125, 137, 132, 154, 154 112, 144, 144, 137, 128, 154, 130, 154 132, 142, 149, 139, 139, 123, 119, 128 135, 156, 154, 114, 130, 142, 117, 119 137, 146, 137, 128, 149, 137, 137, 142 123, 144, 108, 128, 121, 123, 130, 128 154, 149, 149, 139, 123, 139, 119, 146 159, 139, 146, 135, 135, 137, 123, 139 130, 117, 135, 159, 156, 117, 123, 156 154, 169, 159, 159, 149, 123, 137, 135 139, 125, 139, 123, 132, 137, 137, 137 151, 137, 135, 144, 123, 114, 139, 144 161, 135, 132, 144, 169, 146, 151, 121 146, 132, 121, 139, 146, 144, 146, 123 146, 144, 128, 156, 151, 151, 156, 123 164, 144, 151, 154, 154, 149, 154, 137 159, 161, 161, 149, 159, 139, 149, 146 180, 149, 164, 159, 146, 182, 161, 177 174, 166, 169, 174, 182, 185, 190, 185 169, 154, 177, 166, 177, 169, 174, 196 210, 196, 174, 193, 188, 174, 219, 164 193, 185, 190, 185, 202, 182, 196, 219 180, 174, 182, 190, 185, 196, 180, 180 190, 185, 177, 182, 177, 177, 202, 193 185, 185, 177, 172, 196, 190, 202, 196 172, 185, 202, 172, 174, 188, 185, 169 185, 144, 204, 161, 185, 177, 172, 177 177, 216, 196, 182, 199, 182, 174, 174 193, 193, 196, 169, 185, 185, 182, 174 207, 196, 174, 182, 169, 185, 204, 193 188, 193, 193, 222, 182, 182, 207, 196 193, 177, 207, 202, 231, 204, 193, 213 231, 231, 207, 250, 256, 279, 246, 243 234, 286, 262, 216, 213, 231, 246, 234 231, 225, 202, 199, 204, 222, 199, 193 231, 188, 196, 164, 207, 182, 199, 188 185, 204, 202, 204, 193, 193, 202, 210 202, 199, 213, 196, 159, 202, 204, 174 196, 182, 202, 196, 199, 193, 196, 202 193, 182, 185, 185, 180, 182, 210, 180 204, 190, 193, 188, 210, 193, 188, 199 185, 196, 202, 190, 210, 199, 166, 207 202, 188, 190, 202, 204, 204, 202, 180 180, 188, 190, 196, 188, 177, 193, 169 193, 193, 193, 177, 199, 169, 177, 188 213, 172, 207, 182, 164, 190, 193, 196 180, 174, 222, 172, 210, 196, 185, 180 222, 193, 216, 219, 188, 154, 188, 207 213, 196, 210, 196, 202, 204, 204, 213 188, 210, 219, 204, 199, 196, 202, 199 185, 222, 193, 182, 196, 196, 207, 204 199, 199, 196, 219, 207, 193, 196, 210 210, 204, 193, 213, 237, 172, 228, 202 202, 196, 199, 190, 219, 196, 213, 210 196, 207, 172, 210, 213, 204, 199, 210 188, 196, 185, 188, 196, 196, 188, 196 225, 207, 196, 202, 204, 185, 253, 202 222, 188, 207, 182, 210, 196, 190, 219 207, 199, 202, 188, 225, 182, 180, 213 243, 210, 213, 225, 213, 210, 202, 225 222, 219, 210, 202, 222, 199, 213, 213 237, 204, 222, 213, 193, 216, 228, 193 222, 225, 202, 199, 228, 210, 240, 199 210, 216, 231, 180, 199, 190, 225, 213 202, 228, 225, 210, 213, 216, 216, 222 199, 202, 219, 228, 207, 225, 202, 210 240, 253, 185, 213, 219, 234, 207, 256 216, 240, 196, 237, 228, 190, 228, 222 237, 240, 180, 202, 199, 231, 246, 222 219, 234, 207, 193, 246, 240, 207, 243 216, 199, 246, 240, 286, 237, 243, 199 216, 253, 222, 213, 219, 228, 250, 219 243, 222, 266, 250, 216, 246, 234, 222 243, 240, 231, 282, 246, 219, 237, 228 269, 237, 231, 240, 246, 228, 237, 256 240, 250, 262, 256, 253, 240, 216, 246 246, 282, 253, 231, 266, 259, 266, 250 296, 279, 292, 279, 282, 262, 276, 296 282, 269, 269, 292, 286, 324, 296, 317 342, 339, 306, 310, 342, 331, 339, 350 350, 365, 365, 376, 428, 396, 404, 408 437, 433, 424, 471, 471, 502, 488, 566 493, 586, 566, 586, 640, 635, 600, 605 581, 666, 610, 625, 671, 605, 610, 586 590, 600, 600, 557, 538, 506, 529, 493 454, 445, 497, 497, 424, 424, 365, 420 396, 408, 346, 388, 380, 339, 380, 384 357, 357, 328, 376, 331, 313, 328, 353 320, 328, 328, 335, 317, 313, 317, 324 346, 313, 310, 289, 299, 279, 292, 292 303, 299, 313, 282, 292, 296, 292, 292 276, 262, 276, 279, 259, 303, 286, 299 276, 256, 272, 276, 276, 286, 266, 279 269, 246, 266, 269, 266, 269, 240, 276 279, 256, 243, 269, 228, 282, 286, 259 231, 279, 262, 262, 262, 259, 240, 253 246, 237, 231, 272, 259, 246, 266, 250 266, 243, 262, 256, 246, 282, 240, 266 225, 246, 246, 289, 253, 266, 289, 253 266, 259, 256, 253, 246, 240, 266, 246 250, 259, 262, 279, 272, 286, 253, 266 269, 256, 246, 272, 310, 286, 279, 272 276, 306, 292, 292, 313, 310, 313, 303 324, 292, 299, 306, 324, 331, 350, 346 365, 437, 437, 454, 467, 462, 493, 484 557, 576, 488, 557, 562, 571, 620, 571 552, 534, 515, 441, 449, 424, 445, 441 365, 396, 372, 361, 369, 350, 339, 335 346, 335, 350, 342, 328, 272, 313, 320 310, 299, 279, 299, 306, 286, 299, 317 282, 289, 303, 331, 306, 286, 266, 276 269, 269, 292, 286, 292, 292, 250, 262 272, 266, 243, 269, 279, 286, 276, 296 286, 246, 269, 282, 250, 253, 266, 259 237, 272, 292, 286, 286, 279, 272, 296 279, 276, 289, 292, 317, 286, 292, 310 296, 296, 276, 310, 296, 279, 276, 299 279, 292, 276, 282, 303, 262, 303, 272 276, 272, 279, 276, 269, 262, 246, 272 246, 276, 266, 269, 269, 269, 276, 292 250, 259, 269, 228, 259, 246, 292, 262 276, 262, 299, 272, 262, 279, 272, 276 276, 292, 286, 272, 289, 262, 256, 243 262, 243, 269, 259, 253, 276, 243, 246 262, 246, 253, 266, 256, 296, 253, 269 250, 279, 219, 237, 237, 262, 246, 253 243, 250, 234, 272, 253, 253, 262, 240 266, 256, 262, 253, 259, 246, 243, 246 231, 225, 246, 250, 234, 266, 246, 204 240, 240, 250, 210, 246, 246, 237, 234 246, 240, 213, 219, 219, 246, 256, 225 250, 222, 253, 219, 237, 222, 243, 231 234, 237, 256, 213, 228, 234, 253, 243 240, 250, 259, 222, 243, 243, 256, 246 237, 240, 237, 210, 250, 216, 228, 234 228, 228, 213, 210, 207, 234, 240, 225 243, 225, 216, 228, 225, 231, 231, 262 202, 228, 234, 237, 207, 250, 207, 228 237, 253, 207, 262, 219, 213, 243, 222 234, 202, 213, 228, 216, 243, 213, 188 234, 243, 231, 228, 234, 243, 207, 207 225, 234, 240, 253, 231, 207, 199, 250 240, 213, 202, 213, 256, 231, 216, 228 219, 243, 246, 246, 234, 207, 237, 196 228, 240, 216, 250, 213, 219, 199, 225 234, 237, 243, 219, 213, 228, 216, 210 219, 219, 228, 237, 234, 213, 228, 216 216, 269, 246, 222, 228, 207, 237,/