SampleIdent,928A21H3 76-78,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,15-mar-1994 15:05,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 228, 237, 246, 219, 246, 216, 219, 213 216, 199, 210, 213, 213, 202, 180, 228 207, 199, 204, 213, 196, 185, 202, 193 202, 210, 216, 231, 193, 216, 204, 207 225, 225, 228, 207, 207, 204, 199, 222 196, 190, 210, 228, 196, 190, 202, 213 228, 204, 219, 213, 190, 199, 210, 204 202, 213, 219, 213, 193, 193, 190, 204 207, 225, 219, 185, 174, 196, 190, 182 199, 193, 177, 180, 174, 182, 196, 193 185, 225, 188, 188, 228, 182, 188, 199 188, 193, 190, 193, 180, 202, 210, 180 188, 185, 193, 177, 177, 188, 185, 190 190, 185, 172, 188, 199, 210, 210, 190 216, 202, 207, 193, 182, 190, 193, 177 172, 185, 185, 196, 216, 174, 199, 190 177, 210, 166, 204, 193, 210, 207, 216 202, 196, 210, 182, 213, 190, 172, 188 202, 216, 188, 188, 193, 199, 182, 185 190, 219, 180, 202, 219, 182, 182, 231 196, 199, 207, 185, 190, 161, 210, 193 174, 196, 180, 216, 196, 210, 188, 231 225, 185, 166, 216, 204, 219, 177, 222 196, 188, 199, 188, 177, 210, 190, 196 199, 196, 231, 210, 193, 190, 213, 213 202, 199, 182, 193, 213, 204, 207, 193 210, 199, 216, 199, 202, 196, 185, 196 193, 196, 156, 196, 172, 207, 210, 182 185, 207, 199, 199, 222, 202, 193, 213 199, 207, 202, 193, 204, 202, 202, 188 207, 199, 210, 196, 237, 199, 228, 222 234, 204, 193, 246, 216, 193, 207, 219 228, 188, 213, 188, 210, 219, 202, 204 228, 213, 222, 216, 202, 177, 210, 199 193, 193, 216, 207, 216, 202, 231, 202 182, 199, 216, 222, 219, 210, 202, 231 193, 246, 210, 196, 190, 210, 199, 228 202, 190, 243, 222, 222, 204, 204, 207 190, 228, 216, 210, 207, 213, 240, 228 219, 202, 199, 216, 207, 207, 207, 216 219, 207, 237, 243, 225, 225, 210, 243 219, 243, 237, 207, 199, 240, 243, 225 234, 228, 228, 231, 219, 237, 237, 216 246, 234, 216, 219, 225, 266, 204, 237 246, 222, 234, 237, 234, 225, 250, 222 231, 225, 207, 231, 240, 204, 219, 204 225, 246, 240, 246, 250, 225, 250, 228 237, 246, 219, 240, 231, 243, 213, 234 256, 202, 246, 262, 228, 234, 228, 237 222, 219, 231, 234, 228, 228, 210, 231 269, 240, 231, 237, 234, 210, 231, 237 216, 256, 240, 231, 210, 207, 222, 222 237, 216, 240, 237, 210, 237, 222, 240 213, 216, 216, 202, 216, 240, 207, 222 240, 246, 213, 207, 216, 225, 193, 210 222, 213, 219, 228, 234, 207, 207, 210 222, 222, 199, 210, 202, 202, 196, 204 199, 202, 193, 196, 196, 207, 207, 207 225, 225, 202, 177, 188, 185, 199, 199 210, 210, 193, 204, 225, 231, 210, 202 188, 199, 210, 210, 188, 199, 204, 182 185, 196, 188, 188, 174, 188, 199, 193 188, 180, 196, 174, 193, 207, 204, 202 204, 193, 174, 190, 196, 196, 188, 193 188, 202, 193, 172, 180, 185, 174, 196 182, 193, 180, 196, 190, 177, 161, 207 174, 177, 193, 196, 185, 169, 172, 196 172, 193, 188, 159, 188, 185, 182, 188 177, 174, 180, 159, 151, 169, 210, 169 177, 196, 161, 182, 174, 177, 182, 196 166, 169, 166, 174, 172, 142, 164, 185 177, 180, 185, 159, 177, 185, 185, 188 188, 159, 185, 149, 166, 164, 159, 159 174, 146, 146, 174, 166, 166, 161, 193 169, 159, 151, 149, 159, 154, 156, 188 172, 174, 161, 174, 161, 159, 149, 159 144, 164, 164, 154, 161, 144, 166, 164 151, 144, 130, 164, 180, 172, 149, 156 169, 151, 164, 159, 139, 156, 159, 159 149, 159, 166, 149, 149, 144, 149, 164 139, 166, 159, 159, 149, 156, 174, 149 139, 172, 159, 164, 164, 156, 151, 174 161, 151, 146, 151, 174, 137, 159, 164 144, 164, 146, 144, 188, 146, 159, 161 154, 193, 159, 161, 164, 180, 169, 164 166, 188, 151, 139, 154, 159, 144, 164 172, 132, 164, 169, 151, 135, 156, 161 144, 130, 159, 130, 130, 128, 137, 137 149, 137, 130, 159, 137, 146, 154, 121 154, 121, 149, 137, 121, 132, 142, 137 112, 123, 139, 130, 137, 128, 108, 135 106, 114, 144, 132, 119, 121, 121, 114 132, 128, 121, 128, 119, 106, 121, 104 137, 125, 144, 123, 132, 125, 114, 121 137, 110, 110, 94, 121, 110, 121, 132 123, 106, 123, 132, 108, 132, 112, 117 121, 102, 96, 121, 114, 130, 106, 119 102, 110, 104, 92, 128, 119, 139, 110 98, 137, 108, 128, 102, 132, 117, 104 117, 104, 114, 128, 121, 123, 119, 94 121, 108, 128, 102, 102, 102, 121, 112 110, 128, 102, 98, 108, 114, 119, 121 100, 94, 110, 92, 92, 114, 106, 137 106, 117, 117, 102, 123, 94, 112, 96 112, 108, 112, 125, 106, 114, 121, 108 102, 112, 104, 100, 110, 112, 112, 108 94, 100, 108, 102, 96, 137, 92, 114 98, 106, 114, 110, 106, 86, 102, 108 104, 110, 108, 121, 112, 98, 125, 98 114, 110, 121, 114, 137, 114, 123, 110 104, 102, 110, 130, 121, 98, 117, 102 104, 114, 117, 117, 108, 110, 121, 108 117, 128, 123, 130, 121, 121, 112, 106 121, 100, 108, 123, 114, 114, 112, 108 106, 123, 125, 106, 114, 121, 123, 142 114, 119, 128, 119, 110, 119, 117, 88 139, 114, 123, 130, 123, 112, 137, 117 117, 128, 119, 123, 119, 123, 146, 132 154, 142, 146, 149, 137, 94, 128, 128 132, 132, 137, 121, 123, 121, 132, 114 114, 146, 159, 159, 121, 130, 142, 146 154, 154, 154, 159, 137, 146, 161, 177 149, 151, 174, 177, 174, 188, 185, 182 202, 177, 174, 188, 193, 193, 185, 182 231, 207, 234, 234, 246, 246, 243, 234 243, 237, 276, 262, 296, 317, 292, 320 388, 328, 331, 376, 357, 372, 400, 380 424, 380, 424, 437, 458, 462, 449, 480 534, 480, 493, 493, 454, 471, 471, 502 480, 502, 458, 412, 384, 400, 369, 376 350, 350, 331, 313, 303, 266, 292, 272 246, 228, 259, 219, 202, 202, 190, 216 196, 207, 164, 149, 169, 190, 159, 146 164, 164, 161, 154, 146, 151, 139, 156 137, 108, 125, 130, 130, 130, 106, 130 128, 132, 130, 81, 102, 108, 121, 137 123, 96, 119, 117, 110, 119, 106, 119 114, 106, 110, 121, 119, 96, 106, 112 117, 102, 104, 114, 100, 121, 94, 106 117, 117, 98, 121, 110, 102, 104, 104 96, 106, 100, 102, 100, 88, 98, 119 110, 90, 108, 106, 92, 90, 90, 94 92, 77, 106, 104, 108, 96, 98, 106 90, 94, 100, 114, 114, 108, 98, 102 112, 90, 106, 92, 98, 86, 85, 90 108, 96, 79, 112, 90, 117, 102, 94 112, 102, 108, 100, 104, 102, 88, 98 79, 121, 110, 81, 90, 108, 108, 106 79, 102, 119, 88, 83, 104, 104, 83 108, 83, 90, 100, 74, 88, 76, 100 98, 98, 79, 98, 98, 98, 102, 96 86, 86, 96, 96, 96, 106, 88, 94 92, 92, 86, 110, 90, 96, 112, 104 83, 104, 86, 88, 96, 96, 90, 98 130, 96, 79, 110, 85, 94, 90, 92 96, 90, 83, 100, 85, 81, 81, 98 83, 100, 90, 85, 104, 98, 110, 85 102, 100, 108, 100, 100, 85, 76, 88 92, 94, 100, 94, 104, 94, 88, 121 76, 79, 88, 90, 100, 88, 106, 102 92, 104, 79, 85, 98, 96, 88, 86 100, 106, 100, 94, 94, 92, 96, 88 92, 85, 72, 98, 112, 88, 96, 72 96, 98, 114, 102, 90, 98, 104, 92 106, 98, 114, 96, 108, 94, 98, 96 86, 98, 86, 100, 94, 92, 85, 96 98, 92, 85, 88, 94, 94, 83, 94 130, 114, 110, 100, 92, 108, 94, 86 110, 94, 90, 92, 104, 92, 106, 90 98, 94, 94, 100, 94, 112, 96, 98 92, 96, 102, 90, 98, 106, 98, 79 104, 106, 98, 108, 98, 92, 94, 94 88, 85, 98, 104, 94, 121, 92, 108 85, 92, 106, 102, 86, 98, 98, 117 85, 83, 92, 86, 104, 114, 96, 104 98, 112, 90, 108, 90, 92, 100, 104 104, 110, 96, 110, 90, 100, 88, 88 81, 94, 100, 98, 86, 114, 94, 100 112, 104, 114, 94, 98, 104, 88, 90 100, 94, 106, 96, 104, 102, 77, 106 108, 102, 86, 112, 104, 117, 112, 104 121, 100, 100, 112, 94, 106, 100, 108 88, 94, 110, 106, 98, 90, 102, 106 110, 98, 130, 117, 114, 117, 119, 98 94, 102, 102, 125, 102, 117, 94, 117 121, 106, 100, 94, 114, 121, 108, 100 121, 121, 108, 100, 104, 114, 130, 114 121, 108, 121, 121, 130, 110, 96, 128 104, 102, 98, 108, 104, 121, 117, 106 121, 117, 142, 106, 112, 121, 117, 119 96, 125, 121, 112, 121, 112, 130, 123 121, 114, 117, 121, 123, 110, 108, 112 117, 100, 128, 106, 121, 123, 106, 135 117, 114, 123, 106, 110, 119, 117, 135 119, 130, 108, 114, 114, 117, 128, 121 135, 125, 128, 125, 130, 132, 123, 121 123, 146, 130, 132, 144, 130, 130, 142 123, 149, 128, 149, 121, 130, 121, 119 121, 139, 132, 128, 123, 137, 132, 139 121, 121, 117, 159, 119, 110, 137, 114 121, 114, 128, 104, 132, 104, 100, 117 110, 146, 123, 102, 121, 119, 117, 130 125, 132, 125, 119, 119, 92, 117, 104 92, 123, 104, 110, 104, 108, 106, 114 108, 110, 121, 121, 137, 121, 130, 121 102, 121, 128, 114, 104, 114, 130, 96 121, 117, 130, 149, 106, 119, 121, 121 121, 137, 121, 108, 98, 123, 135, 110 114, 137, 132, 117, 117, 121, 114, 121 106, 104, 135, 125, 98, 104, 117, 132 121, 102, 121, 125, 110, 135, 106, 117 119, 144, 121, 108, 132, 96, 114, 106 119, 117, 121, 121, 130, 114, 117, 146 137, 137, 121, 137, 128, 128, 128, 130 130, 121, 108, 123, 121, 164, 135, 130 112, 137, 125, 123, 130, 137, 121, 130 139, 144, 154, 156, 146, 144, 144, 144 130, 149, 146, 119, 132, 144, 149, 142 149, 154, 139, 142, 164, 156, 169, 166 161, 169, 144, 169, 154, 193, 174, 172 199, 185, 204, 190, 210, 193, 196, 196 199, 234, 202, 210, 204, 222, 222, 190 228, 199, 225, 222, 219, 213, 228, 228 222, 222, 222, 213, 234, 219, 222, 190 231, 222, 207, 222, 193, 182, 207, 213 216, 190, 213, 182, 193, 174, 190, 196 177, 174, 210, 199, 210, 182, 182, 188 210, 196, 196, 207, 213, 196, 213, 185 199, 196, 188, 188, 188, 159, 207, 199 190, 188, 196, 188, 207, 193, 182, 185 199, 199, 185, 182, 204, 177, 190, 207 204, 199, 213, 185, 177, 185, 190, 185 190, 207, 190, 199, 188, 185, 207, 213 185, 207, 216, 222, 213, 210, 243, 213 210, 250, 269, 262, 266, 282, 243, 266 272, 289, 279, 286, 289, 253, 246, 231 272, 243, 234, 246, 196, 213, 222, 202 207, 210, 202, 202, 219, 193, 228, 193 182, 228, 204, 188, 190, 193, 207, 193 190, 177, 202, 207, 182, 202, 210, 219 196, 207, 204, 222, 204, 188, 202, 210 193, 213, 202, 199, 196, 188, 196, 177 231, 196, 202, 204, 190, 190, 222, 196 199, 210, 250, 199, 207, 204, 219, 188 199, 182, 190, 185, 185, 190, 234, 174 193, 210, 190, 182, 199, 225, 207, 196 193, 182, 180, 193, 204, 196, 182, 196 193, 193, 188, 196, 188, 202, 193, 182 188, 196, 193, 174, 219, 202, 182, 190 202, 177, 182, 172, 190, 188, 213, 204 196, 210, 190, 182, 202, 193, 185, 164 202, 199, 182, 182, 199, 177, 222, 185 185, 180, 159, 202, 174, 182, 172, 202 199, 164, 188, 202, 188, 177, 177, 210 182, 210, 193, 190, 210, 210, 202, 185 190, 182, 180, 190, 234, 174, 169, 190 188, 185, 185, 204, 207, 190, 182, 185 216, 222, 207, 182, 204, 193, 207, 190 196, 190, 169, 185, 207, 188, 185, 216 207, 219, 196, 188, 207, 193, 193, 185 182, 204, 174, 188, 193, 210, 185, 202 204, 196, 199, 225, 193, 185, 213, 199 199, 234, 193, 193, 204, 188, 196, 199 219, 174, 204, 202, 193, 193, 193, 202 210, 193, 196, 196, 199, 174, 169, 185 185, 169, 193, 213, 188, 193, 174, 219 190, 207, 182, 213, 219, 180, 182, 185 188, 216, 199, 213, 182, 199, 216, 196 202, 222, 190, 219, 199, 193, 210, 207 202, 207, 202, 216, 225, 207, 202, 202 216, 207, 196, 222, 228, 199, 222, 204 234, 216, 188, 190, 231, 188, 222, 216 213, 219, 219, 188, 228, 231, 210, 222 222, 188, 204, 231, 204, 225, 240, 222 246, 204, 228, 210, 231, 199, 210, 231 246, 213, 213, 219, 196, 210, 234, 222 243, 188, 231, 228, 222, 231, 202, 207 207, 231, 231, 243, 266, 269, 246, 240 231, 240, 262, 266, 279, 262, 246, 253 266, 222, 259, 222, 259, 246, 272, 262 262, 262, 269, 269, 282, 246, 303, 339 324, 266, 310, 324, 335, 324, 350, 380 346, 384, 369, 372, 416, 369, 416, 433 428, 400, 396, 497, 488, 493, 543, 534 524, 576, 557, 520, 557, 610, 600, 640 666, 635, 615, 660, 610, 625, 655, 635 586, 562, 600, 586, 595, 543, 524, 529 497, 488, 475, 458, 433, 441, 408, 392 384, 404, 384, 396, 404, 361, 353, 384 313, 342, 339, 350, 313, 306, 331, 303 339, 320, 331, 313, 350, 306, 313, 324 299, 272, 276, 286, 299, 296, 286, 289 272, 299, 296, 246, 286, 282, 306, 262 259, 289, 256, 269, 269, 266, 225, 272 276, 282, 231, 276, 231, 246, 222, 207 243, 266, 246, 250, 243, 246, 266, 246 262, 243, 219, 250, 234, 228, 246, 234 240, 234, 240, 256, 266, 237, 225, 213 231, 234, 216, 207, 231, 219, 237, 237 225, 216, 225, 240, 228, 222, 253, 246 246, 231, 243, 237, 250, 231, 253, 243 228, 216, 231, 276, 225, 240, 228, 262 228, 243, 246, 286, 259, 246, 207, 256 269, 262, 272, 262, 262, 253, 246, 253 231, 272, 279, 266, 266, 250, 259, 310 276, 292, 299, 292, 292, 357, 317, 346 335, 392, 467, 493, 493, 520, 534, 586 571, 635, 625, 697, 640, 692, 635, 605 552, 586, 557, 493, 520, 428, 416, 388 365, 361, 380, 346, 346, 317, 313, 292 328, 306, 299, 286, 286, 276, 276, 279 320, 276, 272, 253, 253, 276, 292, 282 262, 276, 269, 259, 259, 259, 225, 262 289, 262, 237, 269, 256, 243, 246, 250 272, 282, 213, 269, 250, 246, 225, 231 240, 253, 253, 246, 231, 250, 253, 266 243, 246, 259, 231, 256, 250, 279, 237 240, 266, 240, 246, 246, 272, 282, 237 266, 259, 269, 256, 279, 219, 296, 256 246, 237, 262, 250, 246, 213, 250, 256 256, 231, 269, 250, 243, 231, 246, 266 250, 253, 246, 228, 272, 259, 246, 240 253, 262, 240, 243, 246, 269, 269, 266 286, 256, 246, 231, 262, 246, 262, 231 231, 243, 246, 243, 253, 240, 259, 231 246, 231, 276, 225, 204, 225, 240, 219 231, 250, 225, 256, 199, 231, 225, 253 222, 207, 253, 222, 243, 259, 213, 234 243, 213, 204, 231, 240, 231, 225, 246 225, 210, 210, 216, 243, 210, 250, 222 234, 225, 225, 213, 207, 219, 225, 234 210, 225, 196, 196, 234, 213, 228, 216 207, 213, 228, 207, 219, 231, 228, 207 204, 199, 202, 216, 228, 225, 202, 210 237, 231, 231, 216, 193, 190, 202, 225 228, 237, 193, 225, 219, 216, 207, 210 219, 243, 228, 196, 213, 202, 219, 213 216, 193, 196, 210, 196, 234, 213, 216 237, 234, 216, 243, 207, 213, 204, 231 202, 225, 193, 231, 199, 193, 210, 228 193, 222, 219, 199, 204, 231, 225, 190 210, 213, 210, 185, 185, 199, 199, 202 204, 210, 180, 202, 213, 202, 210, 219 213, 213, 202, 202, 216, 204, 202, 196 193, 231, 219, 188, 216, 193, 213, 210 199, 207, 196, 213, 216, 210, 210, 190 193, 219, 213, 246, 231, 225, 190, 213 210, 207, 202, 231, 213, 196, 228, 225 207, 222, 207, 219, 216, 240, 243, 213 219, 219, 199, 228, 228, 193, 219,/