SampleIdent,928A 22H1 22-24,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,15-mar-1994 16:04,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 269, 286, 269, 262, 250, 269, 266, 266 253, 259, 282, 299, 266, 266, 286, 269 256, 272, 276, 292, 286, 243, 234, 282 289, 259, 250, 253, 253, 276, 234, 286 259, 269, 262, 279, 266, 276, 282, 282 253, 289, 262, 262, 276, 262, 269, 250 246, 228, 266, 262, 256, 262, 253, 289 259, 250, 286, 237, 266, 266, 237, 246 262, 269, 228, 222, 253, 234, 237, 276 256, 279, 292, 262, 253, 243, 240, 266 266, 222, 225, 262, 237, 256, 262, 262 231, 282, 269, 256, 216, 256, 266, 269 253, 250, 259, 262, 207, 272, 246, 259 237, 250, 269, 246, 231, 272, 225, 210 240, 256, 240, 225, 262, 225, 259, 228 259, 240, 246, 246, 266, 279, 243, 256 262, 250, 253, 256, 259, 246, 279, 253 250, 256, 243, 246, 262, 240, 256, 262 256, 276, 243, 228, 237, 250, 243, 259 286, 282, 269, 250, 250, 272, 231, 243 262, 256, 259, 240, 246, 246, 246, 256 243, 259, 246, 243, 253, 262, 256, 272 276, 269, 256, 253, 225, 276, 272, 231 253, 269, 269, 262, 250, 276, 231, 266 250, 246, 306, 266, 259, 276, 228, 266 276, 243, 246, 266, 259, 256, 256, 289 231, 272, 269, 253, 269, 253, 276, 231 266, 276, 259, 282, 286, 246, 292, 240 289, 256, 266, 276, 246, 269, 250, 282 282, 262, 272, 279, 289, 259, 259, 276 266, 276, 276, 279, 286, 269, 266, 259 286, 246, 276, 324, 272, 292, 289, 276 282, 279, 266, 306, 259, 286, 269, 282 256, 292, 276, 303, 269, 313, 269, 310 282, 266, 292, 262, 292, 306, 269, 256 279, 313, 299, 262, 299, 279, 282, 306 289, 306, 286, 262, 328, 296, 296, 276 266, 286, 299, 313, 292, 339, 328, 282 296, 306, 306, 328, 289, 303, 320, 320 310, 292, 292, 279, 317, 310, 299, 306 303, 303, 303, 313, 262, 306, 313, 313 306, 339, 299, 303, 276, 310, 324, 331 310, 313, 320, 292, 310, 306, 299, 306 296, 306, 303, 317, 346, 289, 335, 320 296, 331, 324, 320, 331, 310, 335, 306 292, 313, 299, 339, 292, 320, 324, 289 299, 306, 324, 286, 299, 365, 310, 303 313, 306, 303, 320, 320, 320, 299, 276 299, 339, 306, 292, 279, 279, 292, 299 320, 299, 286, 292, 303, 292, 342, 313 286, 299, 306, 272, 296, 313, 282, 272 328, 286, 279, 296, 313, 282, 299, 299 276, 306, 276, 279, 292, 282, 310, 272 296, 269, 276, 292, 286, 262, 286, 279 272, 289, 279, 250, 282, 253, 256, 262 262, 253, 292, 253, 279, 246, 262, 262 292, 272, 243, 240, 213, 243, 246, 246 228, 231, 259, 250, 210, 253, 250, 262 243, 234, 234, 237, 272, 219, 237, 246 250, 246, 250, 246, 237, 243, 216, 262 219, 231, 225, 225, 237, 231, 243, 256 222, 225, 253, 237, 222, 240, 234, 231 225, 219, 225, 207, 204, 253, 202, 222 222, 219, 210, 219, 228, 222, 225, 202 202, 219, 219, 225, 207, 225, 237, 210 225, 250, 207, 193, 193, 228, 204, 222 210, 207, 222, 207, 202, 190, 207, 202 234, 204, 199, 202, 231, 188, 213, 207 210, 193, 185, 202, 202, 193, 204, 188 210, 177, 216, 159, 182, 228, 222, 177 190, 177, 202, 199, 190, 202, 188, 210 196, 222, 185, 174, 190, 182, 188, 174 164, 199, 199, 185, 177, 193, 190, 169 182, 185, 193, 199, 202, 216, 177, 185 177, 196, 169, 172, 188, 182, 199, 172 188, 193, 196, 177, 177, 185, 174, 196 199, 210, 166, 177, 199, 180, 190, 174 210, 190, 216, 222, 193, 216, 196, 182 216, 182, 182, 182, 210, 182, 213, 193 174, 193, 196, 193, 202, 193, 188, 185 182, 207, 180, 174, 196, 182, 202, 182 199, 166, 177, 204, 210, 188, 193, 196 193, 193, 185, 182, 174, 199, 219, 190 188, 185, 199, 196, 199, 213, 204, 199 185, 190, 177, 166, 207, 182, 213, 182 182, 180, 174, 159, 182, 172, 172, 182 132, 159, 177, 156, 151, 149, 132, 166 146, 139, 166, 159, 161, 144, 149, 139 146, 149, 149, 149, 149, 149, 144, 144 174, 135, 142, 128, 144, 135, 154, 146 135, 135, 149, 132, 130, 144, 132, 137 130, 156, 137, 135, 151, 139, 137, 149 144, 130, 128, 135, 149, 128, 128, 144 125, 128, 132, 130, 139, 106, 128, 112 119, 98, 137, 121, 135, 110, 117, 119 130, 149, 121, 112, 121, 139, 154, 132 142, 117, 135, 128, 137, 132, 123, 94 130, 110, 130, 130, 112, 125, 114, 114 112, 114, 130, 119, 128, 112, 128, 130 121, 98, 125, 137, 128, 130, 121, 121 130, 121, 132, 128, 121, 119, 125, 125 85, 106, 130, 142, 110, 114, 135, 139 98, 125, 106, 121, 130, 110, 125, 119 100, 106, 108, 121, 104, 104, 123, 114 114, 88, 123, 94, 130, 128, 117, 130 106, 123, 117, 117, 108, 125, 114, 117 117, 130, 106, 108, 119, 104, 106, 123 135, 125, 108, 128, 125, 121, 119, 117 98, 125, 123, 106, 121, 125, 144, 132 121, 117, 102, 121, 144, 125, 98, 108 125, 110, 104, 94, 121, 110, 130, 108 108, 128, 121, 125, 130, 125, 125, 151 119, 117, 106, 114, 130, 104, 117, 117 135, 110, 121, 132, 119, 108, 112, 132 128, 123, 110, 119, 114, 106, 117, 130 130, 123, 132, 137, 135, 132, 146, 123 139, 142, 135, 146, 128, 135, 154, 139 137, 128, 121, 119, 137, 149, 149, 146 130, 114, 142, 151, 121, 130, 146, 142 159, 169, 132, 130, 144, 164, 132, 132 149, 154, 142, 159, 146, 177, 185, 144 177, 174, 177, 190, 177, 190, 202, 193 193, 190, 196, 210, 216, 210, 219, 222 204, 222, 231, 237, 222, 256, 289, 289 306, 282, 299, 310, 317, 320, 342, 353 346, 361, 384, 357, 428, 384, 404, 404 441, 467, 471, 493, 520, 488, 475, 543 515, 615, 590, 562, 600, 562, 586, 548 562, 552, 548, 502, 506, 471, 416, 396 376, 380, 369, 339, 317, 317, 317, 339 282, 296, 250, 246, 243, 231, 207, 216 210, 210, 185, 193, 225, 210, 204, 196 166, 166, 149, 161, 177, 174, 164, 156 151, 139, 144, 137, 161, 164, 144, 137 144, 137, 146, 137, 137, 130, 132, 137 132, 142, 128, 123, 128, 104, 106, 110 123, 121, 135, 121, 106, 104, 110, 102 90, 121, 100, 114, 117, 114, 123, 108 100, 125, 114, 106, 108, 128, 108, 128 100, 112, 128, 130, 114, 125, 108, 100 117, 112, 98, 100, 98, 114, 108, 114 92, 92, 104, 108, 114, 94, 110, 100 112, 100, 85, 102, 100, 119, 110, 106 108, 128, 96, 86, 79, 119, 96, 106 106, 110, 98, 96, 108, 121, 88, 102 83, 104, 94, 112, 112, 100, 117, 90 100, 98, 100, 90, 96, 106, 81, 104 90, 94, 92, 100, 98, 112, 104, 86 117, 96, 108, 106, 102, 102, 90, 108 98, 104, 108, 112, 110, 114, 100, 98 100, 94, 100, 108, 100, 108, 119, 64 110, 90, 110, 100, 92, 98, 92, 96 86, 102, 85, 96, 100, 92, 102, 88 121, 98, 98, 90, 110, 106, 104, 85 94, 117, 102, 98, 96, 90, 104, 110 102, 110, 114, 92, 102, 85, 92, 94 85, 100, 106, 90, 119, 108, 96, 94 102, 104, 88, 94, 90, 106, 90, 88 92, 92, 106, 98, 88, 104, 85, 110 96, 88, 96, 100, 108, 117, 106, 100 119, 96, 104, 104, 98, 117, 98, 108 96, 90, 96, 88, 94, 88, 100, 108 117, 112, 106, 90, 83, 94, 86, 114 104, 104, 98, 104, 94, 88, 100, 90 96, 85, 96, 92, 102, 98, 92, 86 112, 90, 100, 98, 100, 104, 106, 96 94, 94, 123, 106, 104, 102, 108, 94 88, 94, 94, 96, 100, 100, 83, 79 100, 90, 90, 121, 102, 110, 86, 108 112, 102, 110, 117, 102, 96, 108, 92 108, 112, 98, 98, 94, 114, 98, 88 85, 114, 104, 88, 102, 92, 98, 94 96, 121, 92, 121, 94, 96, 104, 112 96, 100, 121, 100, 90, 112, 117, 106 112, 114, 102, 100, 98, 110, 96, 112 86, 86, 106, 104, 112, 108, 98, 96 96, 114, 121, 112, 106, 100, 112, 88 119, 92, 102, 108, 102, 112, 108, 108 96, 92, 117, 112, 106, 108, 125, 119 114, 96, 98, 106, 121, 121, 128, 102 119, 104, 90, 119, 121, 108, 100, 121 100, 108, 100, 112, 117, 110, 94, 94 119, 108, 130, 110, 121, 106, 119, 104 96, 92, 96, 108, 106, 108, 117, 121 96, 112, 135, 108, 110, 117, 86, 100 98, 112, 114, 114, 98, 106, 119, 125 96, 104, 121, 117, 123, 102, 104, 117 119, 102, 102, 100, 121, 123, 104, 83 108, 98, 132, 83, 119, 121, 102, 119 114, 121, 132, 98, 117, 106, 114, 104 106, 128, 130, 121, 114, 121, 114, 112 144, 112, 142, 119, 137, 114, 132, 139 132, 125, 125, 121, 130, 128, 135, 102 128, 132, 112, 137, 121, 117, 146, 130 139, 142, 159, 142, 142, 137, 132, 161 130, 144, 144, 154, 159, 159, 161, 149 164, 135, 149, 135, 137, 123, 164, 154 123, 146, 125, 114, 102, 135, 139, 139 128, 132, 132, 121, 135, 125, 137, 104 100, 119, 112, 108, 125, 117, 123, 98 132, 114, 135, 119, 132, 139, 119, 121 125, 110, 121, 123, 130, 123, 110, 125 121, 125, 114, 121, 130, 146, 130, 125 121, 135, 100, 119, 92, 114, 102, 132 123, 119, 100, 114, 112, 108, 108, 119 130, 130, 125, 121, 125, 130, 114, 114 121, 121, 130, 128, 119, 119, 135, 123 142, 119, 102, 128, 142, 123, 106, 132 106, 125, 142, 132, 117, 112, 121, 98 102, 135, 108, 112, 114, 130, 119, 114 128, 110, 114, 121, 108, 114, 102, 128 106, 132, 149, 106, 98, 130, 123, 108 130, 130, 154, 106, 104, 125, 128, 96 108, 128, 114, 123, 135, 139, 130, 144 121, 128, 121, 112, 130, 137, 135, 132 132, 123, 139, 144, 142, 132, 121, 139 154, 161, 125, 144, 137, 137, 172, 149 144, 156, 130, 161, 154, 161, 130, 169 156, 156, 164, 169, 172, 151, 196, 169 188, 166, 190, 182, 174, 174, 182, 188 193, 177, 166, 188, 185, 219, 204, 210 210, 177, 199, 199, 202, 225, 216, 196 188, 228, 216, 210, 228, 219, 210, 207 196, 199, 196, 202, 159, 188, 202, 199 174, 202, 188, 193, 159, 180, 210, 207 210, 196, 188, 166, 182, 169, 204, 210 199, 169, 182, 164, 188, 172, 190, 193 177, 190, 169, 202, 180, 159, 177, 188 202, 166, 182, 151, 185, 159, 156, 174 190, 177, 174, 177, 172, 199, 159, 174 188, 180, 193, 188, 196, 169, 161, 185 193, 174, 199, 202, 172, 204, 172, 196 164, 174, 182, 185, 180, 199, 204, 174 207, 243, 228, 219, 222, 262, 243, 237 269, 289, 296, 262, 269, 286, 250, 234 256, 259, 216, 228, 172, 174, 174, 210 185, 210, 188, 177, 196, 180, 202, 166 185, 188, 159, 174, 172, 182, 185, 180 135, 190, 164, 188, 190, 159, 166, 182 177, 190, 204, 185, 190, 199, 193, 199 199, 199, 188, 180, 166, 193, 182, 196 172, 188, 182, 196, 180, 174, 149, 180 185, 207, 180, 180, 172, 149, 166, 190 169, 188, 164, 164, 182, 172, 154, 177 177, 172, 193, 190, 177, 207, 182, 159 156, 190, 188, 169, 172, 180, 156, 154 169, 169, 161, 149, 177, 190, 193, 182 166, 166, 159, 185, 180, 196, 159, 202 164, 199, 199, 185, 182, 174, 164, 180 169, 190, 185, 188, 199, 185, 174, 196 188, 166, 174, 182, 182, 164, 199, 185 166, 188, 174, 169, 161, 161, 154, 172 166, 199, 185, 154, 185, 202, 182, 185 196, 188, 204, 182, 164, 185, 182, 193 169, 188, 161, 159, 190, 174, 159, 185 188, 177, 161, 159, 188, 149, 190, 149 193, 166, 182, 199, 180, 174, 182, 188 185, 180, 202, 166, 190, 190, 196, 182 182, 166, 193, 166, 182, 166, 193, 161 164, 199, 190, 202, 188, 174, 172, 180 177, 202, 185, 188, 185, 196, 169, 199 185, 210, 169, 196, 190, 177, 177, 196 199, 196, 199, 177, 185, 193, 182, 182 177, 188, 193, 182, 188, 210, 182, 182 174, 169, 188, 188, 202, 174, 193, 185 177, 204, 199, 182, 199, 185, 207, 190 204, 207, 199, 180, 159, 169, 180, 199 204, 193, 182, 193, 196, 213, 213, 202 202, 202, 188, 196, 204, 199, 219, 210 180, 199, 202, 213, 219, 188, 190, 174 199, 185, 199, 204, 202, 213, 193, 202 185, 202, 213, 222, 204, 193, 225, 202 190, 219, 219, 196, 193, 193, 237, 216 202, 207, 222, 210, 196, 231, 185, 231 213, 207, 196, 246, 219, 213, 234, 246 234, 222, 256, 207, 234, 193, 204, 250 253, 228, 256, 240, 222, 240, 240, 225 234, 240, 207, 269, 240, 243, 259, 250 256, 282, 250, 246, 250, 256, 266, 262 272, 272, 266, 253, 276, 306, 296, 306 289, 353, 317, 296, 317, 320, 342, 339 350, 369, 361, 365, 372, 384, 416, 416 396, 424, 449, 458, 462, 511, 506, 562 571, 595, 562, 557, 620, 655, 635, 655 650, 655, 718, 650, 708, 655, 692, 660 686, 692, 620, 635, 635, 600, 562, 534 543, 502, 467, 416, 445, 454, 475, 400 365, 376, 369, 396, 357, 416, 380, 361 350, 361, 339, 353, 320, 317, 350, 353 342, 372, 339, 353, 335, 317, 320, 317 296, 289, 282, 324, 296, 306, 303, 286 286, 286, 303, 276, 269, 256, 259, 243 276, 279, 276, 256, 240, 276, 282, 256 266, 272, 259, 279, 246, 266, 250, 243 253, 225, 256, 246, 253, 243, 240, 262 243, 243, 282, 213, 234, 240, 250, 243 246, 225, 219, 240, 269, 240, 250, 228 219, 250, 237, 216, 234, 234, 222, 246 246, 228, 253, 250, 228, 231, 237, 222 246, 246, 237, 243, 222, 213, 222, 231 222, 246, 246, 240, 240, 231, 216, 250 276, 253, 222, 246, 262, 253, 279, 237 240, 250, 246, 250, 240, 272, 299, 282 282, 276, 250, 272, 253, 259, 266, 266 286, 289, 296, 313, 303, 346, 324, 372 372, 412, 376, 428, 458, 511, 640, 650 692, 740, 740, 740, 829, 812, 778, 767 734, 718, 610, 586, 488, 529, 493, 471 392, 361, 361, 365, 357, 342, 328, 328 320, 320, 320, 289, 289, 320, 282, 320 286, 262, 328, 299, 253, 276, 306, 246 272, 286, 282, 292, 240, 266, 262, 253 269, 282, 231, 262, 253, 276, 276, 272 240, 253, 266, 276, 262, 250, 266, 276 292, 276, 269, 243, 259, 262, 234, 266 286, 237, 250, 262, 259, 262, 262, 266 262, 279, 231, 282, 266, 266, 262, 303 272, 269, 259, 266, 279, 253, 253, 279 253, 246, 276, 292, 225, 250, 256, 243 262, 259, 246, 243, 253, 250, 253, 256 269, 246, 243, 262, 240, 243, 237, 259 259, 272, 262, 282, 262, 250, 266, 259 262, 240, 250, 279, 266, 269, 250, 259 276, 272, 219, 259, 240, 234, 243, 256 246, 243, 231, 259, 219, 234, 237, 216 240, 210, 216, 228, 225, 240, 250, 234 222, 243, 234, 228, 250, 237, 237, 216 202, 253, 237, 243, 231, 243, 213, 225 213, 237, 222, 259, 207, 240, 219, 222 199, 243, 213, 199, 231, 222, 228, 256 199, 213, 216, 225, 210, 216, 231, 202 210, 231, 219, 196, 234, 204, 219, 222 228, 225, 225, 213, 193, 196, 210, 216 216, 259, 237, 199, 225, 193, 231, 216 231, 243, 196, 225, 202, 228, 216, 240 246, 207, 237, 216, 193, 207, 237, 210 190, 216, 213, 225, 250, 202, 185, 225 207, 213, 216, 199, 213, 185, 231, 225 196, 199, 204, 210, 204, 225, 231, 188 210, 190, 204, 219, 207, 185, 202, 213 204, 243, 193, 213, 222, 231, 199, 193 210, 207, 193, 202, 188, 207, 240, 193 219, 193, 219, 196, 219, 207, 231, 210 216, 225, 193, 216, 222, 210, 196, 193 199, 210, 193, 219, 196, 213, 210, 196 199, 202, 210, 202, 213, 199, 234, 213 231, 237, 234, 199, 210, 188, 228, 207 216, 219, 219, 199, 202, 182, 202, 222 213, 222, 196, 199, 216, 182, 213, 199 202, 196, 216, 210, 207, 216, 204,/