SampleIdent,929A 1H1 36-38,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-mar-1994 8:53,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 262, 246, 246, 228, 250, 228, 219, 262 240, 231, 256, 210, 272, 246, 250, 246 231, 240, 240, 225, 243, 246, 228, 225 231, 266, 253, 231, 231, 234, 243, 259 216, 240, 259, 272, 240, 231, 256, 240 250, 256, 243, 237, 231, 250, 279, 292 276, 231, 228, 259, 246, 234, 253, 256 250, 246, 259, 246, 269, 269, 266, 266 246, 269, 256, 266, 262, 240, 276, 250 266, 266, 266, 269, 262, 256, 276, 253 269, 272, 262, 266, 219, 262, 256, 259 231, 276, 237, 269, 246, 262, 296, 272 253, 289, 253, 266, 231, 253, 276, 310 250, 269, 246, 276, 279, 225, 272, 276 253, 269, 286, 279, 276, 276, 272, 282 276, 286, 269, 269, 286, 289, 282, 253 296, 282, 296, 303, 269, 246, 272, 276 292, 282, 289, 276, 259, 262, 282, 259 306, 292, 279, 292, 272, 253, 313, 282 292, 292, 292, 313, 313, 289, 306, 296 289, 286, 269, 286, 279, 324, 266, 282 276, 282, 313, 289, 299, 303, 324, 306 313, 286, 292, 331, 253, 296, 296, 279 320, 310, 328, 292, 306, 303, 299, 296 306, 299, 313, 324, 306, 299, 303, 324 317, 299, 310, 324, 313, 365, 324, 296 328, 324, 313, 320, 331, 306, 339, 339 313, 306, 342, 303, 324, 313, 353, 335 342, 303, 342, 328, 353, 342, 331, 331 331, 384, 339, 313, 361, 335, 365, 365 320, 388, 350, 335, 357, 339, 392, 357 365, 388, 372, 353, 357, 380, 372, 357 396, 400, 365, 365, 372, 372, 380, 396 384, 372, 420, 380, 369, 350, 372, 388 392, 380, 384, 392, 388, 384, 388, 388 400, 408, 412, 376, 369, 361, 428, 396 372, 392, 404, 433, 458, 376, 416, 416 416, 396, 392, 365, 384, 420, 420, 420 445, 408, 480, 408, 428, 388, 404, 441 441, 416, 454, 428, 433, 449, 449, 458 420, 420, 462, 515, 437, 467, 454, 454 441, 488, 480, 449, 475, 454, 441, 502 497, 449, 475, 471, 467, 441, 534, 520 488, 497, 497, 488, 480, 511, 475, 467 529, 538, 502, 488, 502, 520, 488, 511 552, 524, 520, 515, 534, 524, 529, 538 586, 529, 529, 506, 524, 548, 548, 538 520, 515, 562, 506, 538, 506, 552, 552 543, 529, 520, 543, 571, 538, 562, 571 625, 557, 562, 534, 524, 562, 562, 506 595, 538, 552, 595, 515, 552, 534, 493 566, 562, 534, 571, 581, 566, 543, 515 562, 562, 524, 543, 520, 520, 511, 520 502, 511, 480, 475, 488, 493, 484, 529 502, 488, 471, 493, 484, 467, 454, 475 458, 484, 480, 471, 428, 437, 454, 471 475, 462, 441, 437, 480, 433, 449, 433 449, 412, 445, 445, 437, 445, 437, 420 408, 433, 454, 404, 437, 388, 396, 416 445, 428, 372, 392, 380, 408, 441, 396 384, 384, 388, 369, 408, 384, 404, 324 404, 357, 376, 400, 392, 361, 384, 404 376, 396, 392, 376, 372, 361, 369, 412 400, 412, 380, 369, 357, 357, 408, 380 331, 369, 392, 376, 357, 350, 342, 388 380, 324, 342, 350, 357, 384, 376, 320 331, 357, 353, 357, 361, 350, 335, 342 357, 335, 335, 331, 310, 310, 369, 320 357, 346, 328, 296, 331, 306, 339, 357 335, 350, 313, 292, 331, 292, 335, 346 357, 342, 328, 328, 317, 346, 331, 324 339, 269, 317, 289, 306, 365, 289, 292 289, 331, 342, 328, 299, 292, 324, 313 317, 353, 313, 331, 324, 324, 335, 279 317, 328, 299, 299, 303, 299, 299, 296 292, 282, 282, 299, 306, 296, 299, 320 292, 324, 303, 303, 286, 276, 320, 303 331, 276, 282, 310, 317, 299, 279, 303 299, 306, 342, 279, 313, 310, 299, 306 306, 328, 299, 306, 292, 306, 279, 310 292, 299, 342, 289, 292, 310, 335, 324 331, 310, 328, 339, 342, 335, 317, 324 353, 339, 320, 342, 342, 342, 346, 365 369, 331, 365, 376, 404, 412, 412, 400 396, 428, 441, 416, 484, 433, 471, 475 471, 471, 515, 471, 467, 449, 428, 424 392, 388, 376, 342, 328, 324, 303, 266 328, 266, 292, 282, 246, 276, 303, 266 276, 250, 237, 262, 234, 253, 266, 240 234, 222, 216, 246, 210, 231, 237, 207 237, 225, 210, 193, 204, 202, 216, 213 210, 222, 164, 204, 222, 207, 193, 190 196, 202, 190, 210, 216, 199, 182, 204 177, 202, 196, 207, 177, 177, 182, 207 216, 202, 193, 182, 196, 188, 164, 180 199, 213, 193, 199, 204, 185, 177, 166 161, 182, 207, 169, 185, 180, 154, 164 161, 154, 180, 177, 172, 177, 174, 174 182, 172, 169, 174, 164, 144, 159, 164 177, 151, 144, 182, 166, 180, 159, 174 144, 172, 151, 149, 154, 180, 185, 164 164, 159, 159, 166, 151, 149, 154, 144 154, 164, 174, 149, 166, 156, 139, 156 159, 146, 159, 144, 159, 164, 164, 159 169, 164, 180, 180, 154, 151, 177, 159 146, 172, 154, 169, 151, 146, 166, 188 177, 149, 166, 151, 174, 174, 164, 142 159, 142, 146, 164, 156, 164, 177, 166 174, 154, 156, 164, 146, 169, 166, 154 161, 159, 188, 166, 172, 151, 154, 159 159, 144, 161, 146, 164, 180, 159, 169 164, 142, 174, 174, 154, 174, 169, 151 146, 154, 182, 185, 180, 177, 188, 177 164, 154, 159, 154, 177, 159, 169, 185 151, 154, 164, 169, 156, 177, 166, 174 161, 177, 177, 164, 166, 151, 174, 182 161, 169, 169, 164, 174, 161, 204, 185 193, 169, 196, 196, 193, 169, 193, 188 185, 174, 182, 210, 180, 185, 174, 174 174, 196, 177, 190, 193, 228, 182, 188 177, 196, 213, 193, 204, 196, 199, 213 222, 228, 225, 234, 213, 199, 222, 225 225, 216, 222, 228, 237, 246, 219, 266 240, 228, 228, 246, 276, 276, 269, 231 272, 299, 259, 306, 256, 310, 320, 320 306, 331, 372, 320, 339, 339, 372, 365 372, 441, 400, 454, 441, 449, 462, 437 493, 511, 458, 548, 557, 605, 600, 595 590, 645, 635, 697, 724, 718, 762, 790 773, 795, 751, 724, 751, 734, 686, 666 635, 566, 586, 506, 538, 543, 548, 475 475, 467, 462, 441, 441, 404, 365, 328 299, 317, 250, 286, 246, 240, 253, 216 225, 199, 216, 193, 202, 216, 207, 188 199, 204, 174, 190, 164, 174, 193, 146 164, 180, 159, 172, 161, 159, 154, 151 161, 156, 151, 166, 146, 159, 154, 154 137, 135, 119, 130, 149, 121, 142, 135 132, 156, 142, 123, 137, 114, 146, 128 156, 117, 144, 125, 137, 132, 121, 110 117, 128, 156, 117, 121, 125, 132, 108 121, 121, 130, 132, 110, 128, 123, 123 106, 130, 100, 114, 128, 135, 125, 114 104, 125, 114, 112, 108, 121, 123, 114 121, 102, 112, 112, 119, 123, 110, 106 117, 121, 110, 114, 135, 117, 117, 104 119, 121, 108, 121, 119, 108, 114, 119 123, 117, 117, 117, 146, 114, 112, 100 112, 121, 106, 112, 114, 119, 125, 104 110, 121, 106, 114, 106, 104, 121, 119 110, 108, 108, 119, 121, 114, 108, 92 130, 106, 132, 121, 121, 114, 128, 114 108, 121, 117, 112, 108, 106, 102, 90 112, 106, 108, 121, 114, 112, 114, 102 128, 102, 112, 94, 104, 112, 108, 96 106, 100, 104, 94, 92, 123, 88, 92 94, 102, 106, 110, 96, 104, 92, 86 114, 104, 123, 114, 110, 110, 112, 98 125, 106, 86, 106, 112, 106, 112, 92 96, 121, 96, 123, 123, 106, 114, 90 106, 94, 132, 90, 104, 114, 100, 108 119, 123, 100, 86, 102, 110, 110, 92 112, 121, 117, 102, 90, 96, 94, 121 102, 100, 102, 102, 106, 108, 123, 102 112, 108, 96, 114, 110, 125, 94, 104 112, 110, 110, 104, 94, 108, 104, 106 121, 92, 112, 92, 102, 100, 98, 100 104, 96, 112, 102, 102, 112, 94, 106 119, 117, 114, 123, 117, 98, 121, 108 102, 102, 110, 117, 94, 96, 112, 92 102, 100, 102, 114, 96, 119, 102, 108 90, 125, 102, 114, 104, 106, 100, 108 110, 106, 102, 121, 110, 123, 96, 132 108, 121, 98, 98, 119, 112, 112, 114 98, 125, 121, 117, 112, 96, 128, 123 114, 114, 110, 106, 121, 121, 88, 106 114, 102, 114, 100, 123, 123, 125, 114 108, 119, 102, 128, 106, 110, 125, 108 108, 108, 110, 117, 130, 104, 119, 108 119, 121, 108, 100, 125, 106, 123, 94 98, 114, 128, 108, 117, 121, 110, 123 104, 135, 106, 117, 112, 139, 137, 128 130, 117, 108, 125, 119, 114, 125, 123 135, 130, 96, 110, 123, 137, 135, 132 121, 110, 144, 128, 123, 149, 130, 123 128, 144, 125, 130, 123, 130, 128, 123 119, 135, 110, 135, 149, 149, 144, 137 135, 130, 128, 137, 149, 130, 139, 123 135, 125, 123, 151, 159, 142, 144, 137 130, 146, 142, 132, 159, 130, 149, 142 135, 144, 146, 142, 144, 142, 154, 156 144, 169, 199, 164, 190, 182, 161, 151 164, 182, 164, 182, 188, 174, 180, 159 177, 193, 177, 207, 207, 196, 207, 216 193, 219, 199, 246, 202, 243, 225, 276 262, 292, 299, 331, 289, 310, 328, 346 339, 365, 384, 412, 408, 396, 424, 449 396, 353, 376, 350, 331, 328, 303, 289 306, 259, 262, 253, 269, 231, 182, 231 240, 199, 219, 204, 193, 199, 210, 202 228, 190, 188, 216, 182, 172, 188, 177 210, 202, 185, 188, 185, 185, 144, 182 174, 180, 169, 193, 185, 190, 193, 164 174, 193, 207, 188, 188, 185, 169, 161 193, 172, 164, 185, 180, 161, 164, 177 185, 164, 172, 174, 174, 154, 182, 172 164, 149, 177, 164, 177, 177, 144, 166 149, 202, 185, 172, 172, 188, 193, 169 196, 188, 190, 196, 207, 172, 199, 199 196, 166, 216, 193, 213, 182, 210, 216 182, 185, 216, 185, 172, 159, 156, 159 149, 149, 137, 137, 121, 142, 137, 125 132, 121, 154, 128, 117, 128, 144, 139 149, 125, 137, 139, 144, 121, 121, 130 142, 114, 117, 119, 144, 132, 164, 137 146, 112, 128, 121, 166, 128, 130, 149 128, 137, 137, 137, 142, 135, 112, 121 139, 130, 119, 144, 130, 121, 125, 137 149, 117, 128, 130, 132, 137, 121, 137 146, 112, 169, 151, 146, 154, 139, 135 149, 142, 132, 151, 137, 154, 137, 137 159, 146, 159, 156, 159, 166, 146, 154 161, 193, 169, 156, 174, 156, 144, 164 185, 154, 151, 151, 169, 142, 169, 156 159, 164, 166, 149, 182, 161, 159, 139 154, 156, 142, 137, 156, 132, 142, 144 146, 142, 164, 142, 144, 151, 128, 137 149, 154, 149, 149, 146, 144, 169, 154 137, 137, 139, 154, 154, 146, 137, 142 156, 142, 146, 146, 125, 130, 154, 130 130, 125, 154, 139, 164, 119, 154, 128 121, 139, 159, 123, 159, 161, 130, 161 149, 114, 135, 144, 156, 137, 169, 149 151, 156, 174, 182, 172, 196, 188, 164 219, 225, 243, 246, 259, 289, 286, 339 342, 424, 437, 396, 433, 396, 335, 339 331, 289, 289, 262, 213, 234, 196, 180 159, 174, 177, 174, 169, 174, 144, 144 159, 169, 154, 154, 159, 159, 156, 159 154, 161, 172, 174, 154, 144, 177, 154 177, 161, 185, 154, 190, 135, 164, 169 185, 210, 182, 182, 151, 169, 156, 169 177, 159, 169, 156, 146, 169, 144, 166 164, 139, 156, 159, 130, 164, 164, 164 144, 149, 159, 151, 149, 159, 164, 172 151, 139, 180, 135, 156, 139, 146, 151 144, 159, 161, 159, 146, 144, 144, 156 144, 169, 161, 142, 169, 144, 144, 151 169, 180, 172, 182, 149, 164, 177, 188 204, 174, 164, 177, 177, 166, 177, 177 193, 210, 161, 174, 166, 188, 159, 172 164, 210, 177, 142, 166, 159, 164, 146 159, 135, 144, 156, 169, 174, 172, 164 142, 144, 154, 144, 164, 146, 151, 174 166, 172, 154, 164, 161, 159, 169, 130 174, 144, 151, 146, 159, 135, 132, 139 166, 154, 125, 166, 159, 169, 164, 169 159, 156, 149, 139, 135, 174, 132, 142 174, 174, 156, 156, 154, 172, 174, 156 166, 169, 154, 166, 159, 154, 166, 154 169, 144, 137, 139, 154, 199, 177, 174 164, 164, 159, 154, 174, 185, 166, 159 166, 169, 188, 151, 180, 151, 172, 196 172, 149, 190, 156, 180, 166, 169, 174 166, 174, 159, 151, 169, 190, 177, 164 164, 202, 177, 161, 196, 180, 190, 193 177, 180, 164, 177, 193, 188, 156, 193 185, 177, 188, 177, 185, 180, 159, 202 196, 164, 190, 216, 174, 174, 196, 199 228, 219, 188, 210, 213, 225, 210, 185 180, 188, 199, 204, 222, 207, 207, 190 204, 188, 202, 202, 193, 199, 180, 199 182, 190, 207, 196, 207, 207, 202, 193 202, 188, 213, 199, 193, 207, 207, 225 219, 199, 225, 219, 234, 210, 219, 182 228, 234, 225, 219, 231, 231, 213, 210 234, 219, 231, 216, 250, 225, 219, 243 240, 234, 231, 253, 237, 279, 231, 228 240, 243, 246, 262, 286, 279, 253, 269 276, 269, 243, 299, 259, 289, 246, 272 303, 310, 269, 276, 272, 286, 299, 328 324, 289, 342, 339, 317, 331, 342, 384 350, 380, 376, 357, 388, 433, 384, 428 424, 462, 480, 454, 480, 529, 566, 502 562, 620, 610, 681, 751, 767, 778, 812 790, 829, 824, 900, 930, 924, 900, 980 961, 888, 876, 847, 767, 784, 745, 718 702, 708, 655, 557, 605, 586, 610, 595 581, 581, 557, 586, 538, 534, 586, 543 610, 566, 595, 557, 590, 600, 557, 562 534, 475, 571, 458, 475, 462, 475, 428 428, 433, 392, 392, 376, 376, 416, 388 331, 380, 369, 328, 350, 346, 328, 339 346, 299, 328, 353, 339, 320, 346, 313 346, 286, 335, 328, 313, 335, 328, 313 310, 299, 328, 299, 299, 306, 286, 282 289, 269, 282, 320, 279, 292, 306, 279 279, 279, 240, 266, 310, 310, 299, 262 289, 286, 292, 279, 279, 279, 292, 282 279, 282, 289, 289, 282, 296, 276, 276 276, 324, 320, 313, 331, 310, 296, 292 306, 289, 306, 279, 282, 286, 282, 259 317, 310, 306, 350, 324, 328, 328, 313 342, 313, 353, 328, 353, 365, 346, 350 346, 380, 380, 372, 365, 428, 428, 400 433, 458, 529, 506, 538, 529, 548, 576 615, 702, 697, 740, 847, 949, 1082, 1183 1274, 1482, 1772, 1823, 2016, 2043, 1989, 2043 1840, 1789, 1714, 1665, 1568, 1560, 1444, 1340 1246, 1163, 1116, 1122, 1050, 992, 980, 942 894, 876, 812, 835, 807, 784, 713, 630 610, 586, 586, 506, 538, 502, 506, 471 462, 441, 454, 404, 404, 449, 416, 433 400, 380, 400, 449, 388, 380, 412, 372 388, 350, 376, 339, 392, 350, 392, 339 369, 353, 331, 384, 369, 328, 388, 365 365, 346, 384, 384, 369, 392, 412, 392 396, 384, 412, 408, 400, 416, 412, 437 392, 404, 404, 433, 437, 420, 404, 404 392, 392, 365, 400, 388, 384, 384, 380 357, 361, 392, 353, 392, 388, 408, 428 416, 424, 376, 404, 433, 400, 433, 424 388, 424, 408, 400, 420, 428, 441, 416 437, 433, 408, 467, 506, 506, 511, 520 475, 475, 506, 445, 467, 433, 445, 441 420, 369, 353, 353, 365, 365, 324, 328 317, 335, 306, 310, 306, 313, 289, 286 328, 292, 320, 279, 303, 310, 276, 306 296, 250, 299, 272, 289, 279, 296, 286 253, 296, 282, 253, 286, 289, 282, 266 262, 269, 286, 272, 256, 296, 282, 299 266, 279, 253, 282, 289, 256, 276, 266 276, 272, 282, 269, 279, 276, 276, 282 243, 243, 256, 286, 256, 216, 286, 231 262, 240, 234, 243, 262, 262, 253, 262 237, 243, 231, 234, 246, 222, 246, 266 253, 256, 234, 256, 243, 276, 253, 253 243, 272, 253, 259, 286, 246, 253, 286 286, 269, 259, 262, 282, 250, 282, 289 250, 269, 276, 262, 202, 240, 262, 231 231, 237, 234, 250, 250, 246, 213, 250 225, 246, 240, 250, 225, 234, 225, 225 190, 231, 228, 225, 243, 228, 213, 222 234, 216, 219, 225, 213, 231, 216, 240 231, 246, 222, 228, 216, 207, 234, 234 231, 225, 231, 219, 231, 219, 219, 222 213, 210, 240, 243, 222, 237, 202, 234 213, 253, 250, 246, 240, 225, 234, 237 240, 210, 243, 202, 259, 225, 213, 246 207, 222, 216, 240, 219, 216, 196,/