SampleIdent,929A 1H3 130-132,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,14-mar-1994 6:25,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 346, 328, 313, 317, 350, 303, 346, 324 320, 317, 324, 317, 306, 328, 331, 335 320, 306, 339, 317, 331, 306, 339, 357 306, 286, 299, 296, 313, 310, 303, 331 313, 328, 324, 328, 331, 350, 317, 299 313, 299, 299, 299, 331, 292, 303, 310 331, 317, 317, 299, 331, 286, 313, 365 331, 320, 303, 310, 276, 310, 320, 292 335, 320, 303, 306, 346, 310, 313, 328 342, 324, 339, 320, 324, 289, 296, 324 324, 299, 331, 317, 292, 324, 328, 346 320, 313, 331, 320, 324, 306, 317, 306 324, 296, 303, 292, 331, 324, 320, 306 313, 331, 320, 320, 350, 324, 328, 313 324, 350, 328, 299, 331, 303, 346, 324 310, 296, 289, 324, 346, 303, 320, 324 317, 317, 324, 286, 331, 320, 376, 353 310, 369, 324, 346, 313, 331, 365, 320 350, 320, 339, 324, 310, 342, 342, 365 361, 320, 320, 324, 369, 342, 320, 365 328, 324, 357, 372, 328, 342, 331, 357 357, 365, 357, 335, 361, 365, 376, 388 353, 353, 353, 372, 335, 369, 361, 372 339, 369, 369, 380, 372, 380, 342, 342 346, 357, 380, 376, 416, 317, 353, 400 408, 376, 350, 380, 342, 388, 376, 380 365, 369, 388, 361, 365, 400, 339, 369 376, 342, 342, 396, 350, 400, 361, 342 376, 380, 428, 392, 420, 392, 392, 437 400, 412, 404, 380, 404, 376, 404, 372 428, 420, 408, 412, 369, 441, 384, 441 384, 424, 420, 408, 416, 416, 396, 408 365, 424, 424, 376, 445, 376, 404, 388 462, 458, 408, 428, 441, 475, 424, 416 433, 424, 441, 412, 437, 462, 428, 424 449, 471, 428, 445, 433, 437, 488, 441 441, 471, 433, 475, 471, 458, 454, 475 471, 454, 506, 467, 441, 484, 493, 454 445, 467, 480, 493, 493, 471, 467, 462 480, 493, 480, 467, 520, 497, 520, 520 529, 524, 529, 534, 529, 576, 511, 534 520, 538, 506, 566, 543, 511, 543, 534 566, 511, 520, 515, 548, 548, 538, 566 471, 529, 586, 538, 595, 566, 562, 586 557, 557, 538, 538, 557, 552, 534, 586 571, 581, 576, 566, 576, 590, 552, 595 586, 590, 595, 645, 635, 581, 615, 576 595, 581, 581, 605, 625, 581, 576, 576 595, 600, 605, 610, 645, 595, 635, 610 650, 620, 635, 581, 645, 586, 620, 620 630, 605, 635, 557, 625, 600, 605, 586 650, 625, 620, 610, 600, 586, 605, 635 595, 605, 581, 595, 605, 557, 552, 576 543, 543, 615, 576, 557, 548, 529, 557 524, 557, 548, 511, 497, 529, 534, 520 515, 506, 520, 511, 511, 524, 524, 506 506, 543, 502, 515, 493, 538, 475, 493 497, 462, 506, 467, 497, 488, 484, 493 484, 524, 458, 506, 497, 480, 433, 445 449, 475, 454, 488, 502, 493, 497, 449 475, 416, 462, 480, 458, 420, 488, 428 437, 404, 445, 408, 445, 454, 441, 445 404, 428, 424, 412, 454, 458, 416, 428 449, 437, 412, 396, 396, 408, 384, 380 412, 412, 392, 392, 441, 408, 416, 416 388, 424, 408, 416, 408, 404, 420, 404 420, 408, 400, 396, 388, 380, 392, 380 392, 384, 400, 369, 372, 365, 365, 365 357, 388, 353, 353, 357, 392, 365, 380 342, 357, 365, 369, 353, 350, 353, 372 353, 342, 357, 380, 353, 310, 353, 350 339, 365, 339, 331, 357, 317, 306, 317 388, 335, 331, 369, 369, 317, 353, 380 357, 328, 331, 317, 328, 331, 310, 313 339, 350, 346, 335, 342, 324, 335, 331 328, 328, 365, 328, 328, 361, 346, 342 328, 328, 313, 306, 342, 313, 331, 342 328, 346, 357, 339, 335, 310, 339, 335 324, 313, 342, 339, 331, 320, 317, 306 331, 353, 310, 306, 320, 350, 324, 328 335, 331, 303, 342, 350, 361, 339, 350 339, 346, 335, 357, 361, 396, 369, 353 369, 396, 346, 384, 380, 392, 388, 384 404, 380, 404, 441, 412, 441, 420, 428 424, 497, 493, 467, 475, 543, 548, 484 543, 475, 515, 475, 471, 458, 388, 372 353, 342, 346, 303, 303, 292, 292, 292 303, 296, 299, 303, 272, 259, 243, 237 279, 269, 250, 250, 253, 246, 253, 234 234, 225, 240, 222, 253, 231, 225, 199 216, 222, 219, 202, 199, 199, 199, 188 207, 210, 174, 199, 210, 188, 193, 188 180, 210, 207, 207, 196, 190, 207, 210 188, 190, 174, 199, 196, 222, 202, 174 180, 193, 202, 177, 188, 188, 185, 185 188, 188, 169, 166, 193, 182, 172, 156 182, 164, 174, 151, 188, 177, 190, 164 182, 169, 199, 169, 172, 149, 185, 154 182, 149, 169, 159, 154, 182, 161, 185 180, 177, 164, 149, 159, 180, 161, 169 188, 182, 149, 174, 174, 161, 137, 156 151, 182, 164, 169, 139, 169, 151, 177 166, 159, 174, 154, 154, 154, 174, 144 154, 151, 174, 166, 169, 190, 151, 149 151, 151, 166, 159, 169, 169, 166, 177 166, 180, 193, 144, 172, 188, 166, 169 137, 159, 154, 182, 154, 166, 172, 121 156, 154, 151, 177, 172, 169, 164, 154 166, 172, 154, 159, 151, 164, 156, 151 166, 146, 154, 154, 174, 161, 164, 169 146, 137, 161, 177, 164, 159, 174, 174 169, 154, 169, 169, 172, 161, 154, 144 174, 154, 161, 149, 169, 177, 159, 166 156, 156, 161, 185, 142, 146, 172, 166 161, 161, 164, 161, 174, 154, 159, 166 172, 182, 166, 144, 180, 161, 151, 159 172, 202, 172, 188, 177, 172, 169, 174 180, 193, 172, 174, 185, 177, 180, 172 166, 182, 174, 154, 182, 219, 196, 174 207, 185, 207, 196, 225, 188, 225, 210 193, 213, 234, 237, 174, 250, 193, 216 219, 210, 213, 222, 243, 250, 231, 253 240, 253, 246, 237, 246, 276, 246, 246 262, 246, 266, 279, 292, 296, 262, 331 328, 328, 296, 306, 317, 331, 365, 353 361, 350, 400, 388, 392, 384, 433, 471 420, 462, 445, 511, 488, 511, 524, 586 562, 566, 610, 640, 660, 681, 660, 692 745, 756, 756, 847, 829, 795, 858, 894 767, 807, 745, 713, 697, 713, 620, 635 620, 581, 524, 529, 506, 529, 484, 424 471, 475, 416, 396, 400, 376, 342, 269 259, 276, 272, 246, 256, 228, 240, 240 210, 216, 213, 246, 196, 177, 196, 202 188, 177, 166, 174, 169, 177, 172, 172 139, 172, 154, 130, 159, 130, 139, 159 130, 128, 135, 130, 159, 144, 130, 139 154, 117, 130, 144, 142, 104, 121, 119 128, 137, 121, 117, 121, 135, 128, 117 135, 123, 112, 117, 135, 135, 104, 123 142, 114, 90, 135, 117, 104, 121, 130 130, 114, 135, 104, 125, 137, 112, 135 130, 125, 100, 100, 117, 128, 102, 121 106, 110, 125, 100, 98, 100, 110, 135 98, 121, 100, 90, 121, 112, 110, 117 112, 130, 106, 132, 112, 119, 90, 121 102, 100, 114, 121, 110, 108, 121, 114 108, 114, 102, 98, 98, 100, 117, 114 128, 100, 106, 98, 121, 94, 106, 90 110, 121, 106, 104, 114, 108, 92, 130 100, 92, 110, 104, 92, 102, 121, 96 90, 112, 100, 123, 90, 94, 108, 108 117, 112, 125, 108, 94, 98, 121, 117 106, 112, 92, 104, 96, 104, 121, 83 123, 104, 92, 117, 102, 94, 104, 104 100, 102, 110, 119, 110, 96, 102, 92 94, 108, 92, 94, 94, 86, 100, 92 117, 100, 90, 114, 114, 108, 106, 108 86, 94, 90, 96, 108, 83, 85, 114 117, 100, 104, 98, 96, 104, 104, 121 106, 90, 92, 100, 100, 88, 83, 86 85, 94, 92, 85, 102, 94, 123, 100 98, 92, 83, 114, 117, 114, 81, 104 92, 108, 100, 117, 108, 100, 79, 86 94, 104, 72, 117, 83, 110, 94, 96 88, 114, 123, 83, 88, 90, 96, 117 110, 100, 106, 76, 119, 106, 106, 100 102, 92, 98, 96, 100, 104, 119, 125 83, 96, 88, 102, 106, 96, 112, 121 108, 92, 108, 112, 88, 98, 100, 108 102, 94, 94, 102, 110, 94, 117, 98 106, 112, 104, 98, 88, 85, 102, 114 96, 81, 77, 110, 100, 108, 117, 98 117, 104, 121, 110, 90, 92, 108, 90 74, 110, 98, 104, 125, 108, 88, 114 94, 106, 98, 96, 106, 86, 104, 112 108, 102, 100, 83, 112, 96, 106, 100 98, 102, 108, 119, 102, 106, 130, 114 102, 121, 94, 98, 106, 96, 108, 108 106, 98, 94, 104, 114, 104, 106, 114 114, 106, 130, 100, 96, 121, 117, 125 100, 104, 108, 123, 106, 119, 121, 119 100, 110, 117, 119, 106, 112, 102, 117 125, 121, 121, 119, 137, 106, 104, 130 104, 114, 121, 104, 106, 123, 108, 102 130, 119, 110, 112, 108, 92, 137, 125 110, 108, 128, 112, 117, 135, 114, 114 142, 132, 135, 112, 123, 146, 100, 117 139, 142, 117, 132, 110, 137, 125, 146 137, 135, 125, 135, 137, 117, 142, 112 130, 117, 144, 142, 139, 135, 144, 139 142, 144, 149, 144, 137, 164, 164, 139 149, 128, 164, 146, 172, 151, 185, 164 166, 177, 164, 172, 199, 164, 196, 199 193, 213, 210, 196, 222, 222, 216, 237 292, 246, 276, 296, 272, 357, 361, 331 331, 357, 335, 357, 369, 372, 324, 317 310, 328, 286, 276, 289, 289, 253, 231 219, 213, 204, 204, 213, 228, 182, 204 196, 193, 180, 216, 182, 196, 177, 161 174, 188, 188, 188, 177, 156, 182, 174 164, 161, 188, 174, 169, 156, 185, 151 159, 169, 137, 149, 161, 177, 174, 177 166, 169, 172, 174, 177, 174, 166, 154 164, 169, 166, 169, 185, 159, 169, 164 139, 154, 146, 180, 149, 172, 166, 142 164, 159, 164, 159, 161, 149, 156, 161 149, 154, 164, 146, 149, 164, 182, 156 169, 164, 161, 154, 149, 169, 161, 149 185, 154, 169, 159, 185, 210, 166, 161 169, 185, 185, 164, 174, 149, 151, 137 112, 142, 119, 128, 121, 121, 135, 130 128, 119, 128, 119, 123, 130, 144, 117 108, 114, 108, 121, 123, 125, 123, 110 137, 121, 121, 114, 106, 125, 128, 132 123, 130, 128, 130, 119, 137, 125, 123 149, 144, 128, 130, 123, 112, 106, 121 130, 119, 121, 121, 121, 123, 128, 117 132, 119, 128, 123, 142, 130, 121, 146 119, 117, 121, 125, 146, 125, 130, 132 135, 123, 132, 146, 130, 151, 156, 151 135, 139, 149, 137, 146, 154, 139, 154 164, 164, 154, 149, 139, 164, 169, 154 154, 137, 164, 149, 164, 156, 161, 154 151, 144, 154, 154, 154, 137, 135, 137 146, 132, 149, 142, 125, 142, 128, 123 137, 142, 142, 159, 130, 137, 139, 135 135, 130, 128, 135, 139, 144, 130, 161 125, 144, 164, 121, 137, 132, 164, 135 146, 156, 177, 142, 130, 146, 121, 161 130, 125, 137, 142, 135, 164, 132, 121 137, 151, 159, 137, 144, 159, 132, 132 154, 144, 137, 149, 159, 159, 169, 172 166, 202, 164, 182, 193, 202, 207, 202 237, 225, 259, 269, 324, 299, 324, 404 380, 384, 400, 376, 424, 361, 350, 317 331, 282, 250, 213, 190, 177, 177, 172 164, 185, 174, 151, 149, 149, 164, 146 139, 159, 135, 154, 142, 161, 149, 139 146, 144, 159, 151, 146, 144, 144, 149 149, 156, 135, 177, 135, 130, 142, 161 151, 159, 154, 149, 151, 130, 137, 154 139, 142, 159, 172, 132, 151, 139, 137 159, 156, 154, 159, 135, 130, 132, 128 135, 139, 164, 151, 137, 142, 117, 161 159, 121, 149, 117, 135, 121, 146, 130 139, 132, 125, 149, 151, 125, 142, 166 142, 142, 125, 151, 130, 125, 159, 149 137, 156, 146, 149, 159, 154, 161, 177 151, 149, 154, 139, 144, 159, 159, 154 159, 142, 161, 154, 159, 144, 159, 151 130, 132, 149, 154, 149, 154, 182, 146 169, 156, 180, 149, 137, 154, 149, 164 164, 112, 144, 137, 149, 144, 154, 154 166, 164, 139, 144, 151, 166, 142, 139 151, 161, 156, 137, 142, 154, 139, 161 149, 144, 139, 159, 151, 142, 164, 154 159, 142, 149, 149, 142, 166, 164, 149 137, 154, 151, 149, 146, 154, 169, 149 151, 159, 164, 151, 149, 137, 169, 144 156, 164, 161, 164, 154, 164, 139, 149 161, 159, 166, 185, 174, 154, 149, 177 169, 159, 154, 149, 161, 132, 172, 159 166, 151, 161, 151, 185, 156, 139, 172 174, 182, 156, 169, 164, 174, 154, 177 161, 156, 154, 164, 164, 164, 193, 159 174, 177, 172, 166, 159, 164, 190, 166 159, 142, 174, 193, 193, 149, 174, 161 180, 169, 164, 193, 169, 188, 204, 193 180, 207, 193, 188, 202, 213, 210, 210 210, 204, 196, 188, 199, 202, 202, 202 182, 185, 188, 207, 210, 196, 185, 166 182, 202, 207, 207, 219, 177, 199, 202 207, 182, 185, 216, 204, 225, 222, 231 196, 199, 204, 188, 199, 196, 204, 204 228, 243, 204, 219, 216, 237, 210, 210 234, 210, 228, 240, 246, 237, 231, 210 231, 231, 240, 262, 246, 266, 199, 253 262, 256, 269, 246, 262, 269, 282, 259 262, 282, 262, 279, 289, 282, 279, 276 272, 272, 313, 306, 306, 339, 282, 320 303, 339, 306, 310, 350, 357, 388, 361 361, 396, 396, 437, 404, 441, 449, 449 462, 437, 497, 493, 471, 529, 581, 571 590, 615, 650, 702, 724, 778, 812, 790 824, 864, 870, 858, 930, 980, 888, 847 882, 801, 876, 778, 762, 756, 650, 666 620, 605, 645, 666, 557, 557, 548, 557 562, 520, 562, 534, 534, 552, 511, 538 571, 520, 511, 480, 538, 524, 511, 529 471, 454, 462, 480, 454, 372, 454, 384 388, 408, 404, 388, 372, 376, 353, 339 384, 346, 357, 324, 299, 292, 313, 328 328, 328, 320, 320, 306, 313, 306, 306 313, 313, 306, 320, 310, 313, 289, 282 320, 289, 286, 289, 299, 272, 292, 282 272, 286, 266, 256, 296, 286, 292, 282 266, 282, 269, 259, 292, 266, 276, 282 250, 269, 282, 279, 272, 250, 324, 269 259, 282, 253, 272, 282, 313, 262, 292 276, 272, 306, 276, 299, 299, 303, 303 299, 299, 289, 331, 279, 262, 279, 303 320, 296, 299, 306, 328, 328, 292, 286 306, 324, 335, 335, 310, 372, 350, 346 324, 353, 380, 380, 384, 433, 424, 428 384, 467, 433, 506, 552, 600, 605, 635 708, 756, 824, 949, 1076, 1109, 1318, 1444 1505, 1568, 1739, 1866, 1945, 1945, 1954, 1858 1722, 1714, 1521, 1444, 1340, 1369, 1260, 1122 1050, 1005, 1005, 967, 894, 858, 835, 807 784, 762, 686, 708, 650, 625, 610, 529 548, 520, 534, 454, 484, 454, 458, 408 449, 458, 428, 416, 420, 428, 416, 400 380, 365, 376, 372, 361, 412, 331, 376 350, 369, 365, 357, 335, 376, 357, 388 353, 353, 342, 320, 376, 342, 331, 365 357, 353, 357, 392, 376, 365, 369, 372 357, 392, 412, 408, 404, 428, 408, 369 416, 404, 416, 396, 408, 357, 376, 380 384, 335, 380, 353, 365, 392, 361, 380 361, 404, 342, 376, 372, 353, 388, 449 408, 404, 400, 380, 380, 376, 388, 376 388, 424, 408, 424, 534, 548, 552, 566 581, 557, 502, 538, 488, 562, 520, 534 529, 497, 437, 467, 420, 428, 412, 376 361, 353, 342, 384, 328, 339, 324, 331 306, 313, 303, 286, 306, 320, 303, 282 331, 324, 339, 296, 310, 259, 289, 269 320, 279, 292, 286, 282, 250, 259, 262 306, 299, 292, 266, 259, 292, 313, 279 259, 266, 262, 262, 262, 250, 276, 256 296, 272, 276, 246, 256, 289, 256, 246 272, 296, 246, 269, 253, 246, 272, 256 256, 246, 266, 231, 240, 231, 259, 243 222, 253, 246, 272, 243, 250, 246, 228 237, 259, 250, 225, 246, 250, 231, 253 269, 269, 243, 256, 259, 243, 272, 234 237, 266, 256, 272, 266, 266, 253, 243 259, 266, 286, 250, 256, 276, 272, 240 250, 259, 231, 240, 246, 256, 262, 225 269, 222, 259, 243, 237, 234, 225, 237 246, 246, 222, 228, 240, 231, 222, 222 228, 225, 234, 243, 225, 219, 222, 234 225, 210, 199, 199, 222, 237, 207, 207 190, 219, 219, 225, 231, 234, 228, 202 213, 228, 216, 250, 222, 207, 188, 210 190, 204, 202, 213, 210, 253, 237, 219 237, 219, 234, 231, 243, 222, 240, 243 228, 234, 237, 199, 216, 213, 240, 228 222, 216, 237, 228, 225, 228, 213,/