SampleIdent,929A 3H2 50-52 GLY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-mar-1994 9:16,/ DataAngleRange, 2.0000, 34.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 166, 185, 182, 174, 202, 177, 164, 164 156, 159, 164, 146, 161, 166, 149, 149 149, 154, 169, 151, 174, 166, 137, 146 149, 137, 154, 123, 132, 151, 146, 169 151, 164, 121, 142, 161, 132, 146, 146 137, 139, 132, 146, 130, 135, 139, 161 125, 135, 144, 128, 125, 130, 119, 128 146, 132, 137, 149, 117, 123, 130, 135 130, 117, 154, 121, 106, 117, 132, 121 132, 149, 125, 128, 117, 135, 130, 130 128, 135, 130, 123, 117, 110, 123, 104 144, 139, 130, 139, 119, 139, 137, 130 128, 135, 117, 130, 112, 146, 128, 135 110, 128, 132, 112, 135, 132, 123, 151 144, 139, 121, 154, 135, 166, 139, 132 135, 156, 128, 139, 146, 146, 132, 137 154, 144, 137, 142, 128, 144, 144, 144 137, 139, 146, 156, 164, 149, 159, 144 144, 149, 130, 149, 144, 149, 139, 188 156, 154, 172, 144, 151, 166, 202, 169 164, 161, 159, 193, 169, 169, 177, 185 161, 151, 172, 174, 177, 166, 190, 172 164, 185, 185, 185, 185, 190, 185, 166 204, 180, 188, 174, 207, 180, 182, 188 188, 188, 207, 182, 193, 202, 193, 185 188, 204, 164, 196, 172, 219, 193, 193 210, 185, 196, 199, 188, 207, 188, 210 210, 177, 190, 182, 177, 213, 210, 196 207, 207, 216, 234, 188, 210, 193, 199 222, 193, 222, 216, 225, 199, 253, 196 240, 216, 222, 225, 231, 216, 240, 234 213, 231, 222, 225, 222, 246, 266, 213 266, 246, 246, 234, 237, 234, 246, 240 237, 269, 222, 256, 231, 243, 234, 231 259, 269, 256, 269, 250, 276, 250, 272 272, 253, 262, 276, 262, 272, 279, 262 246, 299, 246, 279, 253, 250, 231, 269 262, 262, 266, 272, 282, 292, 276, 259 262, 292, 296, 282, 286, 279, 299, 306 269, 266, 272, 310, 296, 299, 276, 253 269, 276, 289, 279, 292, 292, 282, 306 324, 299, 276, 262, 259, 289, 253, 282 286, 276, 292, 250, 282, 269, 310, 243 272, 246, 262, 240, 276, 243, 246, 266 282, 269, 292, 269, 243, 269, 250, 276 256, 237, 234, 269, 250, 262, 219, 231 250, 250, 246, 272, 216, 256, 269, 243 262, 213, 243, 219, 225, 216, 222, 228 246, 228, 240, 240, 237, 237, 231, 240 207, 266, 256, 246, 259, 234, 256, 256 222, 219, 225, 213, 222, 222, 228, 202 216, 188, 240, 228, 237, 210, 243, 237 204, 228, 202, 234, 222, 228, 207, 202 204, 213, 202, 202, 185, 222, 172, 190 210, 202, 177, 185, 164, 199, 190, 180 213, 193, 193, 190, 207, 199, 188, 202 185, 180, 172, 190, 196, 182, 193, 202 182, 188, 185, 180, 177, 169, 169, 166 174, 196, 196, 166, 169, 177, 182, 174 196, 188, 164, 210, 159, 174, 188, 159 185, 154, 185, 222, 161, 156, 159, 159 169, 185, 172, 144, 169, 164, 164, 154 151, 180, 177, 188, 156, 185, 164, 169 174, 151, 193, 164, 169, 177, 164, 172 159, 161, 132, 154, 137, 142, 156, 146 169, 164, 137, 146, 169, 156, 166, 154 142, 154, 164, 142, 156, 154, 166, 164 154, 161, 142, 174, 159, 161, 149, 144 169, 159, 149, 139, 156, 151, 161, 159 142, 137, 139, 161, 142, 156, 149, 132 159, 125, 164, 159, 159, 144, 182, 117 177, 139, 154, 169, 149, 154, 172, 135 154, 156, 142, 137, 161, 151, 166, 159 154, 164, 132, 169, 139, 151, 159, 164 146, 154, 151, 180, 146, 164, 156, 151 146, 144, 156, 177, 144, 164, 156, 132 128, 146, 137, 154, 144, 164, 169, 166 169, 151, 174, 154, 156, 132, 164, 169 146, 177, 151, 151, 142, 166, 161, 154 149, 174, 159, 146, 188, 161, 169, 177 156, 166, 180, 177, 164, 166, 156, 166 193, 190, 182, 185, 169, 185, 174, 188 193, 199, 202, 243, 202, 213, 213, 210 228, 219, 222, 231, 234, 228, 259, 259 259, 253, 282, 266, 276, 286, 272, 269 250, 259, 246, 253, 269, 234, 231, 219 207, 216, 216, 199, 199, 210, 159, 169 193, 177, 169, 177, 182, 196, 185, 180 146, 174, 154, 166, 154, 154, 177, 174 159, 172, 149, 177, 164, 156, 182, 151 182, 159, 159, 144, 132, 164, 144, 135 169, 151, 149, 156, 149, 156, 166, 154 161, 139, 154, 139, 161, 137, 149, 144 161, 151, 177, 161, 146, 114, 151, 139 154, 137, 159, 137, 180, 169, 149, 130 142, 135, 154, 112, 144, 132, 159, 142 159, 144, 135, 154, 142, 137, 169, 142 154, 156, 135, 146, 139, 142, 144, 137 156, 142, 137, 144, 146, 135, 128, 154 128, 144, 159, 151, 144, 156, 149, 137 149, 135, 144, 164, 125, 135, 151, 125 121, 130, 142, 135, 149, 139, 137, 161 144, 154, 135, 144, 125, 132, 154, 142 128, 125, 154, 146, 149, 144, 139, 154 156, 164, 142, 121, 144, 137, 130, 161 146, 135, 144, 132, 154, 125, 137, 149 149, 137, 139, 146, 132, 128, 130, 149 142, 132, 135, 142, 146, 149, 130, 121 125, 149, 142, 142, 156, 149, 137, 137 112, 121, 135, 144, 132, 125, 117, 139 125, 144, 164, 135, 146, 128, 142, 137 123, 106, 135, 128, 135, 121, 149, 149 128, 159, 151, 164, 121, 132, 135, 119 132, 121, 135, 144, 132, 146, 137, 130 135, 130, 132, 119, 135, 164, 137, 137 130, 130, 135, 135, 125, 128, 130, 128 123, 123, 123, 149, 135, 130, 146, 156 125, 119, 137, 130, 135, 144, 142, 146 130, 132, 132, 100, 149, 139, 142, 151 121, 139, 149, 139, 151, 132, 149, 132 125, 139, 142, 139, 144, 164, 159, 159 139, 149, 149, 169, 128, 154, 154, 164 154, 149, 196, 180, 142, 130, 182, 166 149, 161, 196, 174, 182, 182, 169, 172 188, 188, 180, 199, 199, 196, 222, 219 213, 225, 219, 240, 213, 222, 250, 246 246, 262, 253, 259, 279, 276, 240, 292 282, 276, 292, 320, 335, 346, 346, 350 369, 328, 306, 376, 357, 365, 342, 380 342, 369, 365, 328, 365, 328, 303, 310 310, 306, 313, 272, 276, 243, 282, 262 253, 240, 240, 207, 216, 219, 228, 234 185, 185, 174, 161, 188, 156, 185, 154 139, 139, 169, 151, 164, 123, 164, 139 144, 117, 137, 132, 142, 119, 121, 128 117, 110, 106, 125, 135, 112, 119, 121 149, 100, 112, 119, 106, 106, 121, 121 114, 102, 114, 102, 112, 102, 121, 130 79, 96, 104, 119, 112, 96, 114, 114 102, 94, 117, 110, 106, 102, 130, 106 106, 98, 94, 96, 110, 94, 108, 110 98, 100, 86, 92, 104, 106, 123, 104 119, 102, 92, 110, 108, 102, 110, 98 96, 104, 106, 102, 77, 100, 117, 86 94, 100, 121, 104, 102, 100, 114, 85 106, 110, 86, 117, 77, 106, 86, 123 100, 112, 117, 86, 88, 92, 94, 88 114, 110, 98, 100, 139, 112, 106, 100 90, 96, 98, 83, 110, 112, 110, 96 104, 104, 88, 102, 102, 121, 92, 90 94, 83, 104, 94, 106, 85, 104, 100 88, 100, 119, 88, 104, 114, 106, 110 77, 86, 92, 92, 90, 86, 106, 106 85, 108, 86, 102, 106, 98, 108, 96 90, 98, 92, 96, 85, 90, 85, 98 96, 108, 90, 102, 96, 100, 98, 117 85, 98, 102, 104, 90, 96, 77, 102 108, 104, 96, 94, 83, 102, 81, 83 86, 98, 90, 85, 100, 94, 90, 94 85, 81, 104, 92, 102, 90, 86, 96 76, 88, 106, 96, 85, 96, 92, 90 92, 104, 106, 77, 108, 88, 110, 77 104, 88, 94, 98, 94, 90, 119, 98 92, 83, 98, 92, 90, 88, 121, 114 72, 77, 92, 90, 96, 83, 90, 88 100, 98, 96, 98, 96, 94, 98, 102 98, 79, 83, 98, 112, 94, 92, 92 90, 98, 102, 117, 88, 96, 98, 106 86, 98, 96, 104, 92, 117, 110, 112 94, 100, 106, 112, 112, 114, 108, 108 90, 112, 106, 94, 108, 96, 102, 123 98, 92, 96, 104, 96, 94, 119, 90 94, 112, 112, 125, 125, 106, 92, 121 106, 100, 88, 102, 123, 119, 110, 128 98, 108, 102, 114, 114, 117, 104, 121 108, 108, 94, 108, 108, 119, 102, 90 102, 108, 108, 94, 100, 104, 98, 94 98, 92, 130, 76, 119, 121, 119, 106 123, 114, 110, 112, 104, 92, 110, 112 100, 102, 94, 123, 110, 123, 104, 100 98, 104, 110, 112, 114, 110, 104, 106 96, 106, 110, 86, 100, 108, 104, 92 96, 108, 112, 114, 108, 108, 117, 125 106, 114, 102, 119, 102, 125, 102, 110 92, 119, 119, 100, 90, 114, 119, 104 144, 96, 100, 108, 102, 119, 112, 128 121, 108, 110, 114, 100, 106, 121, 117 123, 106, 128, 119, 106, 128, 128, 119 106, 117, 114, 128, 110, 110, 128, 100 114, 102, 119, 114, 123, 137, 100, 108 110, 117, 110, 108, 117, 117, 119, 112 98, 114, 108, 125, 102, 117, 151, 137 119, 130, 121, 114, 137, 130, 130, 121 135, 130, 135, 135, 119, 149, 121, 154 137, 161, 156, 169, 139, 149, 182, 159 177, 182, 193, 193, 182, 193, 202, 169 196, 202, 188, 219, 216, 210, 204, 207 210, 174, 196, 188, 172, 174, 188, 169 169, 156, 164, 154, 154, 139, 151, 144 130, 151, 149, 137, 110, 146, 135, 132 121, 112, 137, 117, 128, 110, 114, 137 149, 130, 139, 137, 119, 137, 114, 121 146, 128, 125, 130, 114, 130, 139, 119 128, 135, 128, 149, 128, 130, 142, 104 142, 125, 130, 119, 132, 130, 135, 146 137, 142, 114, 119, 128, 156, 142, 149 125, 117, 149, 144, 132, 125, 121, 142 154, 139, 144, 128, 130, 121, 137, 149 146, 169, 144, 128, 149, 123, 144, 144 156, 164, 128, 144, 123, 146, 151, 125 128, 159, 139, 125, 149, 142, 117, 135 139, 125, 151, 121, 117, 130, 123, 110 119, 139, 121, 112, 112, 125, 121, 121 121, 121, 142, 104, 128, 119, 149, 104 144, 119, 142, 110, 125, 117, 104, 121 130, 135, 112, 128, 114, 125, 110, 142 128, 128, 123, 128, 117, 135, 110, 130 112, 108, 123, 108, 112, 135, 114, 144 123, 146, 121, 123, 139, 135, 161, 119 130, 164, 123, 135, 137, 149, 123, 156 142, 156, 154, 128, 142, 139, 128, 172 144, 156, 146, 185, 149, 169, 166, 190 169, 169, 156, 137, 154, 146, 180, 139 185, 161, 177, 174, 193, 159, 132, 204 156, 177, 174, 149, 185, 174, 156, 154 144, 144, 154, 174, 146, 144, 142, 149 164, 144, 159, 154, 159, 151, 135, 146 130, 166, 151, 132, 156, 166, 139, 151 146, 164, 132, 159, 144, 137, 154, 125 137, 154, 130, 137, 137, 137, 146, 149 130, 161, 164, 149, 149, 166, 159, 146 139, 164, 146, 137, 121, 159, 182, 139 169, 166, 135, 159, 146, 182, 169, 174 196, 169, 164, 207, 193, 213, 185, 207 250, 243, 292, 310, 279, 286, 306, 313 339, 335, 306, 350, 346, 339, 296, 357 289, 292, 269, 256, 259, 234, 222, 207 196, 182, 159, 164, 156, 177, 174, 177 159, 161, 146, 137, 159, 159, 185, 172 151, 172, 169, 166, 144, 188, 180, 159 154, 161, 142, 169, 172, 174, 161, 142 154, 159, 166, 156, 169, 172, 174, 154 132, 149, 159, 151, 144, 172, 135, 144 164, 177, 166, 159, 174, 146, 149, 159 182, 180, 156, 130, 159, 144, 146, 177 156, 169, 144, 146, 146, 144, 159, 139 159, 164, 159, 172, 159, 142, 161, 156 154, 164, 154, 169, 154, 156, 174, 149 169, 151, 151, 144, 172, 169, 161, 156 159, 149, 177, 151, 177, 193, 177, 169 151, 180, 174, 180, 190, 177, 144, 172 164, 182, 182, 154, 151, 159, 188, 154 193, 180, 174, 166, 166, 156, 159, 172 161, 161, 156, 156, 139, 159, 151, 144 151, 169, 177, 154, 193, 161, 149, 159 144, 164, 154, 159, 164, 159, 177, 177 146, 169, 164, 135, 182, 161, 149, 174 146, 180, 161, 161, 169, 161, 188, 156 188, 144, 164, 164, 190, 185, 177, 177 142, 172, 174, 188, 182, 166, 164, 156 139, 185, 185, 146, 159, 182, 185, 164 169, 188, 166, 174, 159, 161, 161, 177 190, 188, 169, 185, 169, 185, 169, 188 193, 185, 169, 174, 164, 188, 182, 156 202, 166, 172, 166, 182, 174, 156, 196 172, 156, 161, 188, 156, 164, 172, 151 156, 193, 156, 169, 142, 169, 174, 172 169, 188, 190, 169, 172, 185, 190, 188 172, 169, 193, 177, 190, 199, 216, 174 190, 190, 182, 207, 228, 202, 188, 216 199, 204, 243, 202, 188, 185, 180, 199 199, 199, 196, 199, 202, 199, 166, 193 188, 180, 216, 196, 196, 188, 199, 182 204, 193, 231, 182, 174, 188, 193, 213 185, 202, 169, 213, 210, 207, 172, 202 216, 199, 199, 177, 199, 196, 193, 231 202, 188, 216, 222, 225, 219, 196, 216 216, 216, 213, 222, 213, 219, 222, 246 253, 256, 253, 262, 266, 266, 250, 276 243, 266, 253, 266, 250, 231, 246, 234 213, 237, 246, 237, 246, 228, 256, 246 240, 279, 259, 292, 276, 272, 256, 292 296, 279, 266, 250, 256, 313, 317, 279 350, 328, 335, 328, 365, 357, 416, 396 380, 433, 408, 437, 449, 484, 493, 467 515, 467, 529, 524, 484, 557, 506, 524 502, 538, 484, 488, 475, 493, 475, 488 458, 480, 433, 408, 424, 441, 445, 449 388, 400, 388, 408, 412, 372, 388, 380 392, 412, 408, 428, 376, 380, 400, 384 388, 365, 400, 335, 346, 365, 353, 376 335, 384, 328, 328, 350, 350, 339, 317 342, 317, 320, 317, 296, 342, 324, 282 320, 286, 266, 299, 266, 262, 292, 313 296, 286, 306, 266, 269, 289, 282, 292 299, 286, 299, 299, 292, 269, 262, 310 253, 282, 279, 272, 259, 266, 266, 266 276, 296, 279, 282, 282, 296, 282, 286 296, 259, 246, 279, 266, 282, 246, 292 292, 296, 292, 299, 313, 306, 292, 299 317, 282, 282, 310, 320, 299, 303, 303 272, 317, 303, 272, 313, 335, 339, 313 331, 313, 282, 313, 279, 335, 331, 335 342, 339, 376, 350, 335, 342, 361, 376 369, 372, 384, 467, 392, 420, 445, 480 449, 416, 497, 506, 538, 615, 620, 671 650, 767, 773, 888, 949, 1030, 1096, 1109 1267, 1274, 1347, 1369, 1513, 1452, 1482, 1490 1560, 1529, 1475, 1436, 1369, 1318, 1274, 1149 1102, 1018, 930, 824, 790, 708, 692, 702 635, 640, 615, 543, 515, 548, 543, 484 458, 445, 404, 428, 396, 376, 408, 365 365, 372, 331, 369, 342, 320, 331, 310 324, 282, 299, 303, 310, 331, 313, 313 292, 276, 306, 262, 279, 292, 282, 256 272, 303, 243, 276, 269, 279, 262, 282 262, 276, 282, 259, 310, 320, 256, 296 282, 317, 266, 317, 296, 279, 269, 292 282, 262, 296, 310, 296, 269, 276, 286 269, 289, 299, 272, 282, 289, 292, 282 279, 266, 292, 286, 269, 276, 286, 256 289, 276, 335, 342, 286, 310, 335, 306 342, 365, 380, 400, 412, 467, 475, 454 416, 441, 420, 412, 384, 471, 392, 372 380, 361, 376, 361, 339, 339, 353, 303 289, 320, 276, 292, 286, 276, 246, 266 240, 225, 231, 237, 219, 222, 237, 234 234, 204, 225, 216, 185, 204, 246, 240 210, 210, 196, 196, 213, 207, 210, 185 202, 204, 228, 174, 199, 213, 222, 210 225, 210, 213, 196, 213, 199, 219, 182 174, 185, 207, 182, 202, 174, 202, 185 182, 199, 207, 182, 213, 204, 210, 193 207, 182, 185, 161, 185, 174, 196, 185 204, 193, 188, 172, 207, 188, 169, 169 204, 188, 177, 172, 188, 185, 202, 177 169, 193, 182, 207, 177, 196, 188, 185 174, 182, 188, 169, 204, 190, 188, 185 193, 182, 190, 177, 196, 199, 190, 225 177, 199, 196, 196, 177, 202, 207, 180 177, 169, 207, 180, 169, 204, 177, 193 199, 174, 193, 204, 204, 182, 159, 202 185, 193, 182, 180, 210, 193, 177, 193 172, 199, 177, 216, 213, 219, 180, 196 177, 169, 172, 188, 202, 182, 185, 202 193, 196, 180, 193, 177, 196, 193, 231 190, 213, 199, 196, 185, 182, 199, 172 188, 250, 188, 213, 228, 219, 190, 202 210, 228, 199, 193, 222, 204, 193, 180 193, 210, 213, 207, 182, 199, 177, 213 193, 169, 177, 204, 177, 204, 193, 196 190, 166, 177, 169, 188, 216, 188, 180 188, 193, 182, 166, 193, 193, 182, 199 204, 202, 188, 169, 202, 199, 193, 216 188, 188, 174, 188, 199, 202, 188, 190 182, 207, 182, 228, 161, 196, 193, 207 210, 177, 196, 169, 185, 174, 185, 182 172, 188, 182, 193, 207, 172, 193, 190 185, 188, 182, 193, 190, 185, 182, 174 169, 177, 180, 204, 199, 196, 199, 190 177, 193, 193, 196, 174, 172, 180, 177 190, 159, 182, 216, 190, 177, 185, 188 193, 185, 185, 210, 188, 188, 182, 177 188, 204, 177, 199, 196, 169, 193, 225 182, 188, 180, 196, 202, 174, 196, 219 196, 216, 188, 210, 210, 225, 196, 190 213, 182, 207, 188, 185, 225, 202, 207 219, 199, 210, 193, 202, 204, 180, 202 199, 207, 210, 204, 182, 172, 182, 210 213, 185, 193, 213, 199, 188, 169, 204 207, 193, 185, 199, 204, 210, 204, 180 213, 199, 193, 196, 188, 188, 190, 199 188, 196, 188, 199, 180, 199, 193, 219 182, 182, 204, 182, 196, 190, 185, 202 225, 185, 219, 188, 190, 177, 180, 164 177, 219, 177, 199, 190, 159, 190, 216 202, 169, 196, 182, 207, 164, 169, 185 204, 180, 193, 166, 193, 169, 199, 207 180, 169, 164, 169, 188, 174, 188, 193 154, 174, 182, 177, 174, 156, 188, 164 169, 159, 172, 156, 164, 159, 156, 154 185, 166, 169, 164, 142, 185, 169, 146 159, 164, 172, 149, 135, 174, 159, 174 156, 172, 151, 164, 177, 142, 174, 164 180, 164, 142, 174, 172, 149, 164, 174 159, 177, 144, 166, 169, 169, 166, 182 164, 166, 166, 166, 177, 154, 172, 154 151, 159, 161, 159, 146, 169, 159, 169 188, 188, 164, 166, 164, 172, 172, 159 149, 177, 161, 137, 146, 159, 177, 149 169, 164, 177, 164, 169, 159, 151, 146 159, 161, 151, 151, 174, 169, 164, 151 151, 149, 159, 164, 149, 149, 149, 159 185, 177, 151, 149, 166, 125, 159, 135 166, 154, 139, 151, 159, 128, 161, 132 142, 149, 154, 156, 154, 142, 128, 137 137, 146, 130, 151, 151, 144, 164, 142 139, 139, 144, 135, 137, 135, 151, 135 149, 154, 142, 151, 146, 144, 139, 132 154, 149, 174, 159, 159, 154, 135, 135 154, 154, 144, 142, 154, 146, 166, 156 146, 137, 144, 154, 161, 166, 159, 142 149, 169, 156, 193, 132, 172, 180, 159 172, 199, 169, 144, 164, 172, 185, 188 169, 151, 174, 159, 139, 161, 156, 154 172, 146, 164, 161, 166, 156, 146, 154 139, 166, 161, 169, 182, 164, 159, 151 182, 164, 169, 174, 188, 174, 159, 199 188, 164, 169, 182, 185, 151, 169, 188 174, 182, 169, 177, 185, 190, 188, 180 174, 190, 207, 193, 204, 188, 169, 202 169, 185, 188, 207, 182, 174, 231, 156 188, 202, 199,/