SampleIdent,929A 3H3 50-52 CLAY,/ DiffrType,PW1710,/ DiffrNumber,1,/ Anode,Cu,/ DivergenceSlit,Automatic, 12,/ MonochromatorUsed,YES ,/ GeneratorVoltage, 40,/ TubeCurrent, 35,/ FileDateTime,18-mar-1994 5:55,/ DataAngleRange, 2.0000, 29.9800,/ ScanStepSize, 0.010,/ ScanType,CONTINUOUS,/ ScanStepTime, 1.00,/ RawScan 328, 346, 324, 328, 306, 286, 306, 313 320, 292, 310, 350, 320, 331, 369, 353 292, 328, 303, 346, 320, 317, 331, 328 324, 317, 365, 357, 380, 328, 357, 357 324, 361, 365, 350, 365, 372, 357, 328 350, 353, 335, 372, 335, 331, 350, 357 365, 369, 346, 380, 392, 342, 376, 365 388, 357, 372, 350, 365, 372, 384, 372 365, 376, 365, 365, 372, 380, 376, 380 353, 331, 380, 346, 369, 353, 376, 376 365, 380, 369, 396, 365, 357, 396, 376 357, 376, 350, 396, 365, 380, 369, 404 361, 388, 428, 404, 400, 376, 404, 372 392, 400, 400, 400, 380, 404, 404, 372 388, 392, 369, 376, 396, 420, 408, 392 408, 404, 384, 416, 392, 380, 433, 392 416, 433, 392, 416, 428, 392, 400, 412 424, 428, 416, 392, 408, 433, 408, 433 400, 445, 420, 433, 404, 480, 420, 445 433, 433, 445, 454, 449, 441, 404, 445 441, 458, 428, 454, 437, 437, 416, 441 428, 458, 420, 424, 454, 433, 433, 449 437, 437, 454, 458, 433, 437, 441, 458 404, 458, 488, 441, 475, 493, 437, 424 437, 475, 471, 493, 484, 497, 454, 475 462, 471, 471, 484, 467, 449, 515, 497 493, 462, 484, 480, 467, 458, 502, 506 515, 502, 484, 458, 502, 502, 471, 497 480, 493, 475, 511, 493, 480, 502, 493 524, 511, 529, 484, 529, 515, 515, 562 515, 511, 529, 488, 511, 520, 543, 552 515, 529, 524, 520, 552, 552, 502, 557 529, 548, 534, 488, 571, 538, 590, 557 529, 566, 548, 562, 595, 586, 557, 576 497, 552, 552, 506, 595, 600, 538, 538 548, 586, 543, 557, 586, 605, 615, 625 655, 615, 576, 586, 562, 576, 615, 562 571, 645, 620, 615, 615, 645, 586, 600 630, 562, 660, 610, 635, 605, 571, 620 640, 630, 635, 645, 645, 640, 615, 615 630, 635, 630, 655, 645, 600, 650, 692 660, 676, 666, 671, 681, 635, 620, 660 671, 650, 660, 671, 655, 635, 660, 686 681, 635, 681, 729, 676, 645, 650, 666 697, 702, 650, 692, 708, 645, 676, 702 724, 724, 681, 724, 692, 692, 745, 734 708, 740, 718, 751, 734, 666, 756, 724 718, 718, 729, 697, 692, 734, 724, 676 702, 724, 708, 724, 713, 718, 729, 745 686, 734, 729, 697, 745, 666, 676, 778 734, 767, 745, 724, 734, 702, 724, 756 745, 713, 708, 790, 812, 784, 740, 767 745, 745, 718, 708, 762, 702, 686, 718 676, 692, 734, 692, 702, 630, 708, 692 615, 620, 671, 635, 671, 702, 630, 625 655, 671, 645, 635, 645, 630, 660, 655 620, 605, 600, 600, 650, 630, 625, 640 586, 660, 600, 605, 625, 610, 635, 605 605, 620, 595, 605, 543, 552, 581, 625 557, 581, 581, 557, 595, 576, 581, 581 605, 586, 581, 590, 571, 571, 576, 581 538, 595, 534, 605, 576, 520, 600, 562 566, 571, 557, 576, 571, 538, 557, 493 605, 543, 548, 552, 520, 566, 552, 520 502, 552, 538, 529, 543, 548, 534, 493 493, 467, 520, 488, 506, 543, 529, 467 511, 506, 511, 502, 471, 480, 511, 493 511, 502, 484, 471, 471, 493, 480, 529 493, 467, 475, 506, 462, 449, 471, 441 493, 511, 506, 475, 462, 471, 493, 475 484, 488, 467, 441, 441, 441, 493, 480 475, 484, 475, 484, 449, 454, 462, 454 471, 484, 441, 441, 497, 475, 454, 467 437, 433, 433, 428, 475, 449, 462, 449 420, 420, 506, 454, 449, 433, 467, 441 467, 462, 488, 458, 462, 454, 454, 454 471, 475, 416, 458, 449, 480, 449, 449 433, 458, 449, 441, 441, 480, 458, 428 449, 471, 454, 471, 467, 458, 454, 458 445, 493, 471, 467, 484, 502, 488, 480 437, 497, 488, 502, 506, 480, 506, 484 475, 493, 497, 548, 515, 543, 506, 562 538, 576, 552, 576, 571, 571, 650, 605 576, 615, 605, 640, 625, 724, 605, 650 666, 718, 686, 697, 697, 671, 650, 676 615, 655, 557, 581, 562, 506, 529, 462 488, 480, 428, 437, 424, 400, 416, 384 380, 424, 384, 369, 384, 324, 353, 396 331, 306, 328, 328, 331, 306, 299, 324 339, 310, 320, 320, 320, 282, 317, 286 250, 276, 276, 272, 250, 262, 262, 286 282, 269, 259, 262, 276, 276, 272, 272 259, 222, 240, 253, 276, 231, 262, 282 259, 240, 250, 272, 259, 279, 276, 256 262, 237, 231, 210, 231, 240, 213, 210 216, 250, 234, 231, 219, 246, 213, 237 222, 204, 243, 234, 216, 225, 219, 204 216, 202, 210, 219, 213, 202, 204, 219 204, 213, 199, 204, 202, 199, 225, 213 202, 193, 202, 204, 213, 185, 199, 213 193, 202, 202, 185, 196, 202, 204, 207 193, 202, 196, 219, 210, 182, 199, 188 196, 202, 193, 182, 196, 199, 196, 204 204, 216, 219, 196, 202, 204, 225, 207 231, 193, 216, 210, 204, 196, 185, 207 174, 219, 204, 219, 213, 207, 202, 190 204, 207, 180, 213, 188, 193, 216, 219 193, 207, 193, 188, 196, 180, 185, 182 207, 219, 188, 180, 196, 202, 169, 193 210, 190, 182, 207, 210, 222, 196, 199 193, 207, 207, 202, 202, 210, 177, 207 204, 185, 204, 196, 196, 185, 177, 199 228, 202, 185, 207, 213, 193, 177, 228 199, 219, 210, 210, 222, 188, 196, 196 207, 213, 234, 188, 213, 210, 193, 219 225, 231, 213, 222, 216, 213, 219, 228 228, 202, 210, 231, 231, 216, 219, 246 240, 222, 225, 210, 234, 234, 237, 256 266, 210, 231, 234, 250, 243, 256, 234 262, 256, 256, 272, 282, 269, 286, 256 256, 279, 259, 276, 272, 276, 306, 279 303, 317, 303, 313, 313, 292, 296, 313 317, 331, 328, 342, 320, 361, 339, 357 361, 441, 384, 384, 404, 428, 404, 441 400, 433, 467, 454, 488, 520, 562, 506 557, 524, 576, 605, 581, 615, 635, 655 692, 702, 740, 729, 740, 824, 870, 864 930, 924, 973, 906, 986, 1037, 1043, 1043 1096, 1082, 1136, 1136, 1204, 1211, 1142, 1129 1156, 1050, 1069, 1005, 942, 918, 900, 918 882, 847, 835, 745, 795, 724, 756, 660 595, 605, 557, 497, 488, 416, 454, 416 361, 369, 346, 299, 339, 335, 306, 296 286, 286, 279, 250, 256, 228, 213, 237 240, 250, 207, 225, 213, 216, 207, 169 219, 202, 202, 185, 169, 185, 213, 193 151, 185, 149, 164, 169, 174, 193, 182 164, 164, 190, 154, 159, 149, 142, 151 142, 142, 144, 164, 159, 144, 125, 159 164, 154, 142, 151, 135, 172, 135, 130 135, 154, 130, 112, 130, 128, 154, 125 135, 117, 132, 130, 114, 137, 130, 132 130, 125, 125, 132, 121, 119, 159, 130 144, 121, 114, 130, 119, 159, 142, 110 151, 114, 151, 108, 102, 121, 128, 114 119, 130, 112, 108, 142, 137, 125, 110 110, 128, 125, 128, 142, 117, 139, 121 135, 98, 121, 123, 135, 123, 123, 114 137, 125, 114, 119, 130, 106, 112, 128 123, 92, 119, 119, 125, 114, 117, 125 123, 117, 121, 96, 112, 130, 130, 117 106, 100, 121, 117, 110, 114, 119, 123 119, 112, 110, 112, 128, 128, 117, 119 104, 117, 121, 104, 114, 117, 119, 88 104, 106, 114, 102, 123, 100, 108, 98 104, 102, 121, 108, 102, 114, 104, 114 98, 106, 112, 119, 102, 110, 108, 102 117, 90, 117, 108, 128, 104, 132, 117 119, 106, 121, 106, 106, 96, 117, 104 106, 117, 108, 104, 110, 96, 106, 100 96, 132, 108, 117, 98, 104, 112, 117 112, 117, 106, 110, 108, 121, 130, 117 112, 100, 135, 102, 106, 106, 92, 117 114, 112, 121, 121, 106, 121, 114, 98 106, 108, 121, 128, 121, 112, 125, 114 100, 114, 102, 106, 114, 102, 108, 114 104, 106, 112, 119, 102, 119, 108, 135 110, 94, 128, 94, 96, 104, 104, 121 117, 94, 117, 98, 104, 117, 132, 119 102, 110, 114, 110, 90, 108, 110, 132 106, 119, 123, 128, 100, 106, 94, 110 114, 112, 137, 104, 106, 112, 121, 112 117, 96, 108, 112, 98, 94, 123, 119 100, 137, 102, 123, 117, 117, 117, 119 125, 132, 110, 121, 119, 123, 121, 108 106, 98, 117, 117, 137, 114, 117, 114 102, 125, 112, 121, 96, 137, 121, 128 139, 108, 117, 114, 112, 98, 123, 110 128, 119, 139, 119, 114, 121, 110, 123 139, 121, 108, 123, 139, 121, 123, 112 137, 121, 132, 106, 139, 106, 130, 146 108, 132, 114, 144, 121, 137, 123, 123 142, 106, 125, 128, 132, 121, 123, 139 125, 137, 137, 112, 128, 130, 130, 151 121, 121, 130, 149, 121, 137, 128, 123 156, 139, 142, 135, 151, 164, 164, 130 137, 135, 144, 146, 154, 144, 132, 128 159, 151, 144, 137, 151, 144, 164, 125 144, 151, 159, 151, 154, 174, 144, 154 196, 144, 164, 169, 144, 146, 159, 185 182, 169, 164, 177, 166, 177, 164, 174 169, 172, 182, 213, 169, 216, 207, 231 202, 204, 213, 193, 210, 222, 210, 237 240, 207, 243, 266, 237, 276, 286, 317 296, 324, 279, 320, 342, 372, 369, 369 404, 400, 392, 424, 416, 428, 454, 428 428, 420, 462, 437, 424, 404, 428, 388 372, 342, 328, 306, 303, 310, 317, 296 262, 266, 276, 250, 262, 246, 246, 228 253, 246, 240, 259, 240, 240, 228, 246 216, 213, 204, 199, 231, 204, 213, 222 204, 207, 202, 210, 216, 210, 222, 237 207, 196, 216, 202, 199, 207, 199, 216 225, 202, 222, 225, 196, 219, 210, 213 188, 185, 185, 196, 219, 216, 188, 204 207, 180, 222, 207, 161, 166, 193, 207 213, 204, 202, 199, 182, 216, 207, 216 202, 199, 216, 240, 222, 231, 210, 204 240, 228, 222, 231, 253, 240, 237, 225 240, 243, 243, 259, 246, 234, 207, 199 204, 182, 210, 185, 154, 188, 174, 149 156, 164, 164, 139, 149, 144, 132, 144 149, 137, 128, 149, 139, 182, 151, 144 146, 146, 132, 166, 130, 132, 125, 128 135, 137, 142, 139, 144, 149, 121, 137 125, 123, 130, 135, 142, 142, 144, 125 128, 130, 146, 121, 142, 125, 154, 114 119, 128, 114, 119, 132, 110, 117, 130 125, 149, 121, 125, 137, 146, 117, 108 119, 130, 151, 130, 123, 142, 142, 139 159, 121, 149, 149, 128, 144, 128, 144 137, 128, 151, 142, 144, 139, 149, 137 146, 159, 146, 123, 156, 144, 135, 149 142, 144, 149, 142, 142, 130, 128, 151 142, 114, 151, 139, 149, 130, 149, 121 108, 130, 154, 121, 154, 121, 146, 130 119, 119, 130, 132, 135, 132, 130, 102 130, 137, 112, 121, 139, 110, 125, 121 132, 144, 135, 146, 130, 142, 144, 108 117, 98, 128, 117, 130, 137, 130, 121 104, 123, 123, 132, 100, 108, 132, 117 123, 142, 123, 139, 146, 125, 132, 119 149, 132, 164, 139, 137, 151, 161, 159 164, 154, 164, 169, 188, 196, 225, 225 240, 292, 306, 353, 306, 313, 350, 320 353, 350, 320, 306, 225, 256, 243, 199 210, 177, 169, 146, 169, 159, 142, 132 149, 137, 135, 128, 130, 146, 139, 142 146, 156, 149, 144, 144, 154, 125, 144 149, 144, 161, 142, 149, 123, 144, 166 139, 166, 159, 144, 146, 164, 142, 132 159, 166, 159, 144, 144, 132, 137, 137 142, 146, 146, 146, 130, 114, 144, 128 128, 146, 144, 135, 139, 144, 149, 146 130, 135, 130, 106, 137, 137, 137, 132 110, 149, 144, 112, 130, 128, 123, 119 121, 132, 114, 128, 130, 130, 135, 156 123, 139, 128, 121, 146, 130, 123, 137 121, 156, 149, 144, 146, 137, 139, 130 161, 154, 166, 151, 144, 154, 151, 169 130, 151, 132, 130, 139, 121, 139, 142 130, 137, 123, 119, 169, 128, 132, 154 144, 123, 142, 135, 123, 137, 139, 137 137, 146, 135, 119, 154, 128, 137, 117 110, 144, 142, 135, 137, 164, 142, 149 159, 139, 137, 137, 146, 159, 142, 146 125, 142, 146, 130, 137, 132, 139, 128 117, 149, 144, 166, 159, 137, 135, 142 137, 149, 123, 130, 146, 142, 123, 130 142, 151, 142, 139, 142, 151, 135, 151 151, 137, 144, 144, 169, 151, 154, 142 144, 144, 137, 149, 149, 161, 164, 149 154, 154, 144, 151, 161, 174, 156, 164 159, 154, 149, 159, 161, 174, 149, 132 169, 151, 159, 164, 139, 159, 146, 161 144, 174, 174, 149, 166, 144, 151, 169 156, 151, 151, 188, 182, 154, 180, 177 202, 177, 169, 180, 169, 177, 185, 199 188, 193, 193, 196, 204, 204, 199, 202 202, 204, 213, 199, 213, 207, 202, 202 250, 216, 185, 199, 210, 196, 188, 207 190, 219, 204, 188, 180, 202, 204, 190 207, 193, 207, 199, 190, 196, 188, 177 185, 188, 213, 216, 199, 164, 196, 190 231, 240, 213, 210, 196, 196, 231, 219 210, 202, 213, 199, 253, 228, 243, 234 243, 269, 262, 250, 237, 256, 250, 253 272, 253, 262, 296, 266, 276, 262, 303 310, 296, 331, 313, 276, 310, 310, 320 306, 292, 324, 342, 339, 357, 313, 369 353, 335, 369, 400, 369, 420, 396, 437 428, 441, 420, 437, 475, 458, 475, 506 529, 538, 552, 562, 620, 595, 692, 630 686, 762, 740, 740, 841, 864, 906, 930 980, 1063, 1063, 1156, 1211, 1183, 1232, 1204 1232, 1296, 1274, 1267, 1218, 1204, 1142, 1142 1096, 1136, 1063, 1063, 1005, 942, 924, 882 864, 864, 870, 882, 829, 829, 807, 870 812, 824, 818, 847, 756, 812, 835, 762 751, 745, 784, 718, 708, 708, 686, 635 660, 615, 552, 552, 529, 529, 571, 497 511, 454, 475, 488, 467, 416, 449, 416 437, 416, 420, 396, 408, 424, 400, 433 388, 396, 372, 420, 400, 416, 408, 380 372, 384, 376, 376, 361, 388, 353, 396 357, 361, 376, 339, 365, 369, 384, 376 372, 357, 342, 335, 357, 342, 372, 328 353, 369, 350, 365, 369, 361, 339, 310 357, 357, 342, 335, 350, 313, 357, 335 346, 339, 365, 357, 342, 357, 350, 392 303, 380, 357, 380, 369, 388, 365, 404 384, 408, 388, 404, 412, 376, 396, 396 420, 428, 458, 433, 361, 388, 384, 392 404, 475, 445, 480, 471, 437, 458, 520 538, 480, 557, 529, 576, 548, 620, 660 681, 729, 734, 762, 847, 801, 986, 999 1136, 1170, 1340, 1467, 1490, 1568, 1756, 1798 1806, 1901, 1998, 1954, 1945, 1823, 1849, 1781 1632, 1568, 1537, 1616, 1459, 1369, 1296, 1274 1274, 1183, 1190, 1156, 1076, 1082, 1005, 961 999, 973, 924, 876, 841, 790, 751, 729 708, 655, 671, 686, 595, 605, 595, 620 562, 590, 557, 552, 557, 538, 488, 557 502, 511, 543, 515, 511, 529, 511, 511 471, 515, 484, 480, 493, 471, 475, 462 449, 502, 511, 441, 454, 506, 484, 480 467, 497, 502, 449, 493, 529, 502, 488 502, 529, 502, 488, 506, 534, 488, 506 484, 484, 529, 454, 445, 454, 488, 454 475, 449, 400, 408, 458, 480, 467, 493 475, 454, 441, 449, 484, 462, 493, 497 493, 462, 441, 441, 493, 493, 506, 493 471, 471, 506, 524, 548, 502, 562, 566 543, 538, 543, 600, 529, 548, 520, 506 502, 506, 497, 471, 437, 424, 458, 400 400, 408, 376, 357, 392, 361, 346, 339 331, 369, 357, 361, 320, 353, 361, 328 331, 317, 342, 320, 331, 324, 328, 303 320, 310, 317, 320, 306, 324, 306, 299 335, 286, 320, 303, 342, 306, 289, 317 313, 296, 279, 292, 303, 310, 299, 259 296, 306, 286, 279, 296, 282, 289, 279 289, 269, 272, 246, 296, 282, 269, 262 299, 313, 259, 269, 266, 282, 266, 286 269, 256, 243, 282, 272, 253, 262, 246 276, 266, 253, 240, 259, 225, 262, 253 269, 243, 253, 262, 269, 262, 256, 228 306, 266, 279, 266, 253, 222, 282, 306 286, 262, 276, 266, 299, 266, 272, 256 259, 237, 259, 256, 250, 231, 237, 246 253, 269, 222, 237, 240, 231, 243, 219 246, 231, 216, 216, 193, 210, 213, 237 237, 213, 222, 219, 228, 213, 216, 213 222, 234, 219, 199, 216, 210, 193, 237 234, 231, 185, 222, 210, 204, 199, 219 225, 231, 228, 231, 231, 210, 213, 216 246, 210, 231, 240, 234, 228, 210, 202 237, 219, 207, 219, 231, 222, 207, 243 240, 204, 222, 207, 216, 228, 231, 228 210, 196, 174, 182, 213, 202, 246,/